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' I , ‘ . , ,“I I " * but *h‘Lo“ “in a “£3 4 .I . . ‘ a -- " [8 -,~. - 33!. .7 - . ._ . . . . u .I_" " ['0 '|" . "' . ' ' , O ‘ ,4 . ' . a ‘ I ,:o ‘I‘ 7‘ I, ' 0 ' I I I ‘ : .-. \ ' * " "19;: I. I | l I‘ III . I_‘ . 6': II ‘ ', I! ' ' h . IIVI‘O- ~' " ‘A . . Iv " I, I .I. . . -.- ‘ . . ' .‘ ' \‘f I ' ' ' ' ' ‘ '- \ ' I I ‘ ‘ II ‘ l l . \ ' ‘ . 's . ' . . . 1 -‘ . . ‘ . I v . ‘0 o l . 1 . . 1 l ‘ I I . I ' \._ :1 T wad-s HESIES This is to certify that the thesis entitled A Comparison of Two Laundering Procedures of knife Nylon blips presented hg beulah Loraine Davicson has been accepted towards fulfillment of the requirements for A. A. degree in Textiles & Ulothing ajor professor h! A COMPARISON OF TWO LAUNDERING PROCEDURES FOR WHITE NYLON SLIPS BY Beulah Loraine Davidson A THESIS Submitted to the School of Graduate Studies of Michigan State College of Agriculture and Applied Science in partial fulfillment of the requirements for the degree of MASTER OF ARTS Department of Textiles, Clothing, and Related Arts 1953 THESIS ACKNOWLEDGEMENTS The writer wishes to express her sincere appreciation to Miss Hazel B. Strahan, Head, Department of Textiles. Clothing and Related Arts, Michigan State College, for her guidance and supervision of this thesis; and to Miss Sarah Brier, instructor in research, for her willing assistance in the testing laboratory. (RIF, 7-7” (3’) 1 ‘ i. J- ' ‘ t ()1) ' an. I. II. III. IV. TABLE OF CONTENTS INTRODUCTION . . REVIEW OF LITERATURE . MATERIALS AND METHODS . A. ORGANIZATION OF THE STUDY . B. LABORATORY TESTS Twist . . . . . . . Denier . . . . . . Filament Count . Course Count Yarn Count Thickness . . . Weight per Square Yard Bursting Strength Breaking Strength . Elongation . . . . Abrasion . . . . Drapability . . Friction . . . . . Color . . . . . . DISCUSSION OF RESULTS . A. ANALYSIS OF ORIGINAL FABRICS B. PERFORMANCE TESTS ON ORIGINAL FABRICS C. ANALYSIS OF FABRICS AFTER LAUNDERING V. VI. VII. VIII . TABLE OF CONTENTS (Continued) CONCLUSIONS . SUMMARY . LITERATURE CITED APPEN DIX Table I. II. III. IV. V. VI. VII. VIII. IX. XI. XII. LIST OF TABLES Original Specifications . Original Performance Original Performance Coefficient of Kinetic Friction . Yarn Count . Weight per Square Yard Thickness in Inches and Per Cent Change Bursting Strength in Pounds Change . . Breaking Strength in Pounds and Per Cent Change . . Elongation in Per Cent Abrasion . . Drapability . O O O and Per Cent 32 34 55 37 39 41 45 54 59 60 62 64 Plate 1. II. III. IV. VI. VII. VIII. IX. XI. XII. LIST OF PLATES Satin Slip Fabrics . . TricotSlip Fabrics . . . Cutting Chart Satin . . Cutting Chart Satin . . . Cutting Chart Tricot . Cutting Chart Tricot . . Shrinkage in Inches After Launderings Satin . . . Shrinkage in Inches After Launderings Tricot . . Resistance to Abrasion of Laundered Satin . . . . Resistance to Abrasion of sat in O 0 O O 0 Q O O 0 Resistance to Abrasion of Tricot . . . . . . . . Resistance to Abrasion of Laundered Tricot . . . O O O O O 0 Thirty Five Thirty Five 0 O O O O O 0 Machine Hand Laundere Hand Laundered Machine Page 74 75 76 77 78 79 80 81 82 85 LIST OF FIGURES AND CHARTS Figures Page I. Per Cent Change in Course Count . . . . . . . 40 II. Weight in Per Cent Change . . . . . . . . . . 43 III. Per Cent Whiteness on Color Wheels-Satin . . 47 IV. Per Cent Whiteness on Color Wheels-Tricot . . 48 V. Average Per Cent Dimensional Change-Satin . . 52 VI. Average Per Cent Dimensional Change-Tricot . 53 VII. Breaking Strength . . . . . . . . . . . . . . 58 VIII. Abrasion . . . . . . . . . . . . . . . . . . 63 Charts I. Performance in Laundry . . . . . . . . . . . 86 II. Average Per Cent Dimensional Change in Slips After Laundry . . . . . . . . . . . . 90 III. Vertical Dimensional Change of Satin . . . . 91 IV. Horizontal Dimensional Change of Satin 92 V. Vertical Dimensional Change of Tricot . . . . 93 VI. Horizontal Dimensional Change of Tricot . . . 94 IN TR ODUCT I ON I. INTRODUCTION The many new true synthetic fibers such as orlon, acrilan, dynel, or nylon which we consumers enjoy today may be considered dividends from the previous years devoted to basic research. The technological deveIOp- ments in the earlier semi-synthetics, rayon and acetate; and much of the fundamental fiber research has been done since the close of World War I. Since 1918 rayon and acetate have undergone many improvements and have largely replaced silk in many products. Nylon became available, less than fifteen years ago and has, perhaps, had greater growth in total production and acceptance by the trade and consumer than any of the other fibers. The acceptance of nylon for its many diversified uses is unquestionably due to its inherent characteristics and performance in use. Nylon's superior strength, abrasion resistance, ease in care, retention of shape, draping qualities, and chemical resistance are significant reasons for its sensational rate of increase within a decade. Knit construction has been particularly well accepted because it permits evaporation of perSpiration better than the woven lingerie fabrics. Discoloration of white nylon lingerie washed with synthetic detergents has, however, been a common complaint among consumers. Repeated launderings seemed to result in progressive grey or yellowish discoloration. The purpose of this study was to investigate the effect of two laundering procedures on the extent of discoloration in white nylon tricot and white satin slips. Comparison of dimensional change in the slips by two methods of laundry; analysis and comparison of physical prOperties and performance characteristics of the new fabric with those same prOperties and character- istics after laundering, constituted the other objectives for this study. For a more valid determination of total serviceability expected from a garment, it would be desirable, in con— junction with laboratory analysis to carry out a wear study in which the garments would be subjected to normal use and care. Since perspiration, body strain and other factors affect serviceability and satisfaction in use, wear studies are more inclusive of the variables involved in a garment's performance and total serviceability. Because wear studies involve a much longer period of time for investigation, this study was limited to laboratory analysis for determination of the effect of two different methods of laundering on service qualities and color change in white nylon tricot knit and white nylon satin. REVIEW OF LITERATURE II. REVIEW OF LITERATURE The development of nylon evolved when Du Pont chemists began a new program of fundamental research in 1928. It is a classic case of a new material developed in little more than one decade. The new fabric did not receive the name “nylon“ until l958. It has won great favor because of its strength and lightness; its wash- 'ability and quick drying qualities; its resistance to wear; resilience and ability to hold its shape in use. (12) Du Pont, the sole producers of nylon yarn in the United States at the present time is manufacturing staple fiber and filament yarn at the combined rate of 145,000,000 pounds per year, thirty three per cent of which is going into military uses. Greater production is expected in the future since the demand for it has been greater than the available supply. (5) Not only has nylon been used extensively for woven lingerie but its use in tricot knit goods has increased tremenduously in popularity since the close of World War II. (34) By 1952 nylon has become the key word in the tricot field because finished nylon tricot fabrics have excellent stretch and recovery prOperties, softness, 5 drapability and porosity. (4) Tricot fabrics, prior to the close of world War II were manufactured on a limited scale. Celanese is generally credited with being the pioneer in the manufacture of tricot goods for the under- wear trade and mass market. The popularity of tricot knit is shown by the Operation of more than 2400 tricot machines in 1951, compared with 1100 in 1941. Nylon fibers are, in general, stronger and smoother running on the tricot machine than cotton or rayon. Nylon tricot cloth can now be made satisfactorily on the new high Speed machinery without the manufacturing defects which plagued the knit wear industry when they tried to use silk, cotton, rayon and acetate. Factors such as dimensional stability or resistance to distortion and creasing are the two most important prOperties associated with high quality performance in a textile material. In cotton goods, dimensional stability is accomplished by methods based upon com- pressive mechanical shrinkage. Regenerated cellulose rayons, on the other hand, do not reapond well to this type of treatment so some form of resin or chemical stabilization is generally adOpted. Loom-state nylon fabrics, like those made from other textile fibers; hawea tendency to shrink. This shrinkage may be eliminated by treatment with boiling aqueous liquors during processing or in the process of setting. This process of setting, besides imparting the required degree of dimensional stability, is also capable of imparting a permanent shape to nylon fabrics. This precludes the formation of permanent creases during processing and the finished fabric has resistance to distortion and quick recovery from creasing. The setting of nylon may be defined as the reduction or elimination of subsequent yarn shrinkage. It enables the yarn to assume the con- figuration in which it has been held during the setting treatment. The degree of set or stability which is achieved depends, to some extent, upon the degree of shrinkage allowed during the setting procedure. Converse- ly, subsequent yarn shrinkage after setting depends on the severity of the processing procedures in setting as well as the method of test for any subsequent shrinkage. (16) Studies relating to the service qualities of nylon fabrics of significance to this investigation are relative- ly few. Fletcher, Duensing, and Gilliam (8) of the Bureau of Human Nutrition and Home Economics studied sixteen fabrics, knitted to specification in the Bureau's laboratory. Medium staple cotton, wool, filament rayon 7 and filament nylon constituted the four groups studied. They found greatest dimensional change usually occurred in the first laundering. All fabrics except the plated nylon of forty courses per inch, exhibited considerable lengthwise shrinkage. The nylon fabrics changed the least in width of any of the four groups. Less length- wise shrinkage occurred in the knit fabrics of forty courses than those of thirty two courses per inch. (8) Also it was found that knitted fabrics usually shrank more in length than woven fabrics of similar fiber content. In another study, Fletcher and Roberts (9) observed the geometry of knit fabrics made of staple rayon and nylon and determined their relationships to shrinkage in laundering. These fabrics were knit of the different yarns under controlled conditions in the Textile Research Department of the American Viscose Corporation. They found nylon fabrics changed the least in both length and width. All “grey" fabrics shrank more than ten per cent in length in five launderings. All of the loosely knit "grey” materials, except the plain knit nylon, stretched excessively in width. Area shrinkage in all of the "grey" fabrics and the finished viscose fabrics increased with knitting stiffness. Area shrinkage in the finished 8 acetate-viscose, and nylon materials usually decreased as the knitting stiffness increased. Weiner (30) reported studies made on the effect of knitting and finishing variables on the shrinkage of typical Quartermaster Corps cotton underwear construction. Factors analyzed were yarn count, knitting stiffness, and stitch type in relation to reducing potential laundering shrinkage. Since the dimensional stability of woven fabrics is related to tightness of weave; fabrics with well packed warp and filling yarns are subject to less laundering shrinkage than the more Open weave structures. Similarly it was found the lengthwise shrinkage of knit fabrics was less severe when coarser yarns were used. However, the use of heavier yarns resulted in greater widthwise shrinkage. The improved control of lengthwise shrinkage that occurred when heavier yarns were used may be explained by the closer packing of the fibers and yarns which takes place; resulting in increased fabric density. Fabric weight was also increased by the use of the heavier yarns. Tests made with different knitting stiffness showed that those with the greater number of courses per inch were subject to less lengthwise shrinkage but to more shrinkage in width. For a given degree of improvement in laundering stability, increasing the 9 number of courses per inch resulted in much less change in width and weight of the fabric than increasing the size of the yarn. Alexandra and Sturley (1) investigated the influence of twist on breaking load and breaking extension of continuous multifilament nylon yarns and monofil. Com- mencing with three-four S twists per inch, curves showing twist against average breaking load for regular 50, 45, and 60 denier multifilament yarns exhibited an increase in breaking load to a maximum as additional twist was inserted. Further insertion of twist showed the breaking load decreased continuously to the limit of seventy twists per inch. Twist setting the three-four S twists per inch yarns, produced an increase in breaking load of approximately five per cent. The public relations department of E. I. Du Pont De Nemours and Company suggests that fabrics made entirely of nylon may be washed with the same soaps and synthetic detergents used for general laundering, provided the dyes and finishes are truly washable. Garments can either be washed in warm sudsy water by hand or in the washing machine. The latter method can be used satisfactorily where there is no hazard of fraying. They stress the fact that to keep white nylon white, it must be washed IO separately. Although colors in other garments may appear to be fast, they often leave enough discoloration to bring about an objectionable "off white" tinge to white nylon. When washing white nylon in hard water a soap which softens the water should be used to prevent the deposit of curds of insoluble soap on the fabric which give white garments a grey cast. (20) This grey cast particularly in cotton, has been found to result from soil redeposition. Tests have shown that many detergents have poor soil suspending characteristics and permit the retention of soil over a period of washings. In a study conducted by Roseberry and McKee (17). soil removal from nylon was observed in various procedures. The study proposed to determine the best conditions for washing nylon for maximum soil removal. Various detergents, concentration of detergents and temperature of water were used. They found that at a concentration of .075%, the detergents could be ranked from best to poorest in the following order: non-ionics, sulfonated amides, alcohol sulfates, soaps and alkyl aryl sulfonates. At a .15% concentration the order changed with soaps leading in soil removal followed by the alcohol sulfates and alkyl aryl sulfonates. At a .5% concentration the order is the same as that at .15%. At .075% concentration the soil ll removal power of a built soap and non-ionic detergent increases. Raising the temperature of the water from 120° to 130° F. resulted in significantly more soil . removal in the built soap but no increase resulted from further temperature increases. The effectiveness of the non-ionic detergent continued to increase as the temper- ature increased. Leonard and Schwartz (14) report that in 1956 Krueger made a microscopic study on the soiling of garments which had been worn and showed the contamination of cotton fibers in those garments by secretion from sweat glands and hair. It was concluded from these experiments with cotton fabrics of various constructions, that the degree of soilage and resistance to its removal depends on the solubility of the skin excretions and the nature of the fabric construction. Open weaves permit dirt to penetrate while surfaces that are close and even, and starched are resistant to contamination. They also found that fine fibers retain soil more readily than coarse fibers, and that fibers with uneven cross-sectional contours retain soil more readily than those with smooth circular contours. Nylon belongs to the latter group. Snell (22) reports the alky sulfates, sometimes termed fatty alcohol sulfates, paved the way for 12 broadening the field of detergents. By 1950 they were commercially successful. Coconut oil is the fat source commonly used since it has the desired average chain length of carbons. As with the alkyl aryl sulfonate, some sodium sulfate is produced as a natural step in manufacture. The cost of the active detergent is off- set by building with about seventy five per cent of other ingredients. This type also requires correction in building to give good detergency on cottons. The detergent used for this investigation contained about twenty five per cent of the alkyl sulfate built with sodium sulfate, a polyphOSphate and a few per cent of carboxymethyl cellulose. This compound commercially known as Tide is said to be a better detergent than soap for washing cottons. Alkyl sulfates are more resistant to hard water than alkyl aryl sulfonates. Snell further states that synthetic detergents must be used under Optimum conditions for the particular job to be done. For example, strong agitation promotes any detergent process. EXperimental work applying standard washing procedures has shown that mechanical action alone frequently does one-third to one half of the total scouring. 13 In another study Snell (25) reported that soap would always be used under the prOper conditions of water softness and alkalinity for washing cotton. However, in studies comparing soap with an alkyl aryl sulfonate, the latter proved to be somewhat less effective than soap in washing light weight silk dress fabrics, fiber glass textiles, nylon knit goods, cotton, rayon, and rayon given crease resistant finish. In some cases, differences were not great between the soap and the detergent. Nylon was washed easily by both. Furry, McLendon, and Aler (ll) conducted a study to determine the efficiency of soaps and synthetic detergents for use in home laundering. Fifteen soaps, one soap powder, and thirty five synthetics detergents were evaluated for their effectiveness for removing soil under standardized conditions. The change in light reflectance produced in the laundering of artificially soiled cotton fabric was used as a measure of the soil removing efficiency of the different detergents. Samples of the test fabric were laundered in the Launderometer at 127° F and 840 F for fifteen minutes in distilled water and in water of 150 and 500 parts per million hardness at five different concentrations of the detergent. It was found that the soaps removed 14 considerably more soil at 127° F in both distilled and hard water than at 84° F. In hard water the synthetic detergents, in a majority of cases, were more effective than the soaps, especially at concentrations lower than .55 per cent. Snell (24) states that most of the research on laundering textiles with synthetics detergents has been carried out on either cottons or wool. The fiber's physical nature enters into washing conditions in the selection of Optimum temperature and pH of the wash solution, but the fiber's chemical nature is more directly related to the action of a particular detergent. ”When synthetic textiles resemble neither the cellulose of cotton nor the protein of wool; research investigations, methods and conditions of scouring would be of great value." Relatively few serviceability studies on nylon slips have been conducted to the present time. However, in 1949 Kroll and Williams made a study of snagging in nylon tricot slips. They found that snagging in the slips studied resulted from the wearer shaving her legs. The stiff hairs pricked the nylon fibers. Why did the nylon tricot slip show this snagging condition when it did not appear in tricot slips made of other fibers? A 15 comparison of nylon with other fibers in knit tricot indicated that the lOOped effect caused by snagging in the nylon was a result of the strength and smoothness of the individual nylon which permitted a pulling action. With other fibers no lOOped conditions resulted because the obstructions causing the snag easily broke the individual filament. It was found, however, that snagging could be decreased by increasing the denier of the individual nylon filament to a point where the stiff hair bent rather than pulled the filament. With this thought in mind, slips were thereafter made of forty denier — thirteen filament yarns where previously they had been made of forty denier- thirty four filament yarn. In other words the yarn size was increased to overcome snagging. Several studies of rayon slips have been made. In 1946 Rann (22) made a laboratory study of four different brands of rayon crepe and rayon satin. The slips were laundered thirty times. She found maximum shrinkage occurred in the first laundering. Shrinkage was some- what more progressive than the crepe as laundering was continued. However, wider variation was found in the measurements after launderings, due to the bias cut of the garments. The results of her study indicated that 16 the measurements of a bias cut slip after laundering, are highly dependent upon both laundering and the ironing procedure. The average percent shrinkage which occurred was sufficiently high to materially affect the fit of the slip. Improved methods of shrinkage control were badly needed for woven rayon slips. Tensile strength con- sistently increased through the twentieth laundering. Thereafter slight decreases in strength were noted. Thompson (52) carried out a "wear" study on eighteen rayon slips. Thirty three rayon slips of one style and brand were purchased. Eighteen were worn by cooperators engaged in similar occupations for 750 hours. Twelve of them were laundered in the home and the other six laundered in the laboratory under controlled procedures. Six unworn slips were laundered in the laboratory and served as laundered controls. Thompson found that yarn count increased progressively through ten launderings and, in some cases through twenty, tending thereafter to stabilize or decrease. There was corresponding increase in weight per Square yard. Warp breaking strength loss was greater in the worn slips which were laundered by the COOperators. The worn slips showed significant evidence of deterioration; in fact a few of the slips were ready to be discarded after thirty 17 launderings. The greatest deterioration was observed on the inside of the double edge stitched bodice top, par- ticularly across the back and underarm sections. Bayor's (5) study compared the service qualities of thirteen slips each in three different brands of rayon warp knit. Two brands were two-bar tricot construction, the other a single atlas. The study was carried out to compare by laboratory tests, the physical properties affecting dimensional change and serviceability in repeated launderings. Inasmuch as shrinkage is a characteristic problem in knit fabrics, a comparison of fabric shrinkage and dimensional restorability by the use of three different drying procedures was the second aSpect of the study. There were obvious changes in the slips as the number of launderings increased. In each brand there was increase in wale and course count. Weight and thickness of the fabric increased through the fifteenth laundering and decreased thereafter. The same pattern of increase and decrease occurred in bursting strength. Two brands had a significant correlation with the number of launderings. MATERIALS AND METHODS 18 III. MATERIALS AND hETHODS A. ORGANIZATION 0“ THE STUDY Sglection of Slips Six white nylon satin slips and six nylon tricot slips were purchased in a local store in May, 1952, for this laboratory study. The tricot slips were all of the same design and ranged in sizes from 54 to 58. The satin slips were also alike in design of sizes ranging from 12 to 16. The Barbizon satin slips cost $5.95 each and the Vanity Fair tricot cost $4.95 each. The satin slips were cut on the bias with a four gore skirt construction. The side front and back were cut in one piece to eliminate the side seam. (See plate in appendix). The satin slips were lace trimmed and had lapped zig zag stitched seams with pinked edges. The tricot slips had a three gore skirt construction with one gore across the front and two for the sides and back. The seams used in the construction of the slips is referred to in the knitting trade as a serged seam. This over- edged seam is desirable for knitted garments because this stitch permits more stretch without breaking. The hens and tOp of the front and back bodice yoke were 19 double stitched. One slip of each type was kept as a control. One each of the satin and tricot were divided in half so that test samples for weight and color change could be withdrawn at Specified intervals for each method of laundering. The remaining eight slips were used for physical testing after laundering. (See plates I and II in appendix for samples of the original and laundered fabrics.) Four slips were withdrawn after ten launderings for physical testing. The four remaining slips were carried through thirty five launderings. The slips were soiled with a modified standard dry-soil mixture before laundering and after each five subsequent launderings. In order to make shrinkage determinations, each slip was marked at Specified points. At Specified laundering intervals, measurements were taken at these points and recorded to the nearest one sixteenth of an inch. The tricot slips were laundered according to a modified procedure used by Bayor (5) in her study, "Comparison of Some Physical Properties Affecting Service Qualities of Three Brands of Rayon Warp Knit Slips". The hand laundering procedure for the satin consisted of wetting out the slip for three minutes and then gently squeezing the suds through the fabric for three minutes. The soap solution was made of one half 20 cup of detergent to eight gallons of water of 1100 1.50 F. The water was gently squeezed from the slip, then rinsed for two minutes in clear water at 1000 F followed by a second and third two minute rinse. After the third rinse the slip was rolled in a towel to remove excess moisture and allowed to remain for thirty minutes. The slips were then ironed with the heat control set on rayon (225° to 275° F). The iron was raised and lowered, or rather, no pushing motion was used so as to minimize stretch. The slips were then placed on a flat surface and allowed to dry six hours before being measured. The tricot slips were similarly laundered but dried differently; that is. pulled to shape and freed of wrinkles then hung by the straps until dry. The machine laundering procedure was as follows: The slips were run for fifteen minutes in an agitator type washing machine. The same soap solution and amount of water were used in the machine as used in hand launder- ing. The temperature of the water, however, was 120°: 5° F. After gently squeezing the sudsy water from the slips, they were rinsed for two minutes in clear water at 1100 F. After the second rinse they were agitated for five minutes in clear water of the same temperature. They were dried in the same manner as the hand laundered tricot slips. 21 measurement of the Garments In order that shrinkage measurements be taken on the slips at the same location at each interval, thread markings were made at designated locations on each slip. Three horizontal measurements were taken in both the satin and tricot slips; namely, at the bust, waist and hip. Six vertical measurements were taken in the tricot center front, center back, side seams, and side front. The seven vertical measurements in the satin were taken at center front, side fronts, side seams, and side back. Measurements at these points were taken following each laundering through the fifth and again after the tenth, twentieth, and thirty fifth. To take the linear measure- ments the garment was placed over an ironing board. A firm measuring tape was then placed on the slip closely following the thread marked line. Care was taken not to move the slip during the measuring procedure. Measurement for that line was recorded and the slip shifted to the next line for measurement. The same procedure was followed for all linear measurements. Due to the fact that knit goods and garments cut on the bias stretch in handling; the width measurements were taken across one half of the slip while it was lying flat on the ironing board. This measurement was doubled and recorded as the measurement for that horizontal line. 22 B. LABORATORY TESTS The following tests were done under standard conditions of 65% i 2 relative humidity and temperature of 72° 1 2° F. Ifligp, The Suter Twist Tester was used to determine the number and direction of twist in warp and filling yarns according to the Flatt method. A five inch yarn ravelled from the fabric was fastened into the tester so that a three gram deflection load depressed it one eighth inch. One yarn was twisted until broken, a second yarn untwisted and then retwisted until broken. The following formula was used in determining the twist per inch. t - Nl - N2 :,2 2 L N2 = number of turns to twist to rupture N1 8 number of turns to untwist and retwist to rupture T = total of number of turns in yarns t 3 turns per inch L = length of yarn used An average of ten determinations each was computed as turns per inch for warp and filling yarns reSpectively. Dgnigr. The Universal Yarn Numbering Balance was used to determine the denier according to the method and procedure outlined in A. S. T. M. (2). Yarns ninety centimeters in length from warp and filling, were measured with a steel rule accompanying the instrument. Each yarn was then looped and hung on the balance by a Single yarn in such 25 a manner that it was not touching any other part of the instrument. The beam clamp was released and the index pointer rotated until the beam was in balance. The index pointer indicated denier. Ten determinations each for warp and filling were recorded and the averages computed. Filament Count. Filament count was made by placing a yarn on a piece of black velvet. Five filaments were counted and pinned to the velvet until the counting was completed. The number of pins multiplied by five plus any remaining filaments constituted the filament count for that yarn. The average of the count of five yarns from both warp and filling were recorded as filament count for warp and filling respectively. Course Cognt. The number of wales and courses per inch were determined by counting a Space of two inches from at least five different places on the fabric with a Lowinson micrometer. The material was laid on a table without tension while the wales and courses were counted. The arithmetical average of five determinations, with no two areas including the same set of courses or wales was recorded as wale and course count. Yarg Copnt. A Lowinson micrometer was used for counting the number of yarns in an inch for both warp and filling. Yarn count was recorded as the arithmetical average of 24 five determinations for each with the count taken from no two areas including the same set of yarns. Thickness. The thickness of each fabric was determined by the use of the Scheifer Compressometer. A foot, one inch in diameter, was lowered on the Specimen until one pound of pressure was exerted. The thickness of the fabric was recorded in inches. Three readings were taken on each Specimen and the average computed. The thickness was determined on the original, and again after the tenth and twentieth launderings. Wei ht in ces er S are Y r . Weight per Square yard was determined in accordance with the method outlined in A.S.T.M. (2). Five Specimens two inches square, were taken at random from the fabric and weighed on a chainomatic balance. The weight per Square yard was computed by the following formula: 45.71 grams Area in inches (20) = ounces per Square yard Egrsting Stgength. Bursting Strength was determined in accordance with the A.S.T.M. standard procedure. A Scott Tensile Testing machine equipped with the ball bursting attachment was the instrument of test. Five samples, ‘fOur and one fourth inches square were cut for determination 0f the dry bursting strength. The Specimens were inserted aDdheld securely in a clamp mechanism.under a tension 25 which was uniform in all directions. The clamp mechanism is 1.7500 inches in internal diameter. The center of the Specimen was pressed against a polished steel ball 1.0000 inches in diameter until the Specimen burst. The direction of the bursting motion of the ring clamp was at right angles to the Specimen being burst. Five wet Specimens after being immersed in water for two hours were burst in the same manner as the dry. The average bursting strength recorded for both wet and dry was the arithmetical mean of the results of five tests for each. Breaking Strength. Breaking Strength was determined on the Scott Tester by the ravel strip method outlined in A.S.T.M. (2). Ten Specimens each one and one fourth inches by twelve inches were cut for both warp and filling with the longer direction parallel to the yarns being tested. Each strip was ravelled to one inch in width with approximately the same number of yarns taken from each Side. Test Specimens were then cut into two six inch strips; one set for dry and the other for wet breaking strength determinations. No two Specimens for warp or filling contained the same set of yarns. The samples for wet breaking strength were broken after immersion in distilled water for a period of two hours. Specimens were broken within two minutes after their removal from the 26 water. Recordings were made to the nearest one half pound. The average of the ten readings each was recorded as the dry and wet breaking strength in pounds for warp and filling. Elongation. Elongation of the fabric was taken simultaneously with tensile strength by the autographic recording device on the Scott Tester. Elongation was calculated from the start of the line on the tensile gram and an average of ten determinations each for wet and try tests was recorded as the average percentage increase in length for warp and filling. Abrasion. Resistance to abrasion was determined on the Taber Abraser. Three Specimens five by five inches were abraded with CS 10 Calibrase wheels under 500 grams pressure. Specimens were abraded for determining first sign of wear, arbitrarily defined as the first yarn broken, and then to a hole; defined as the rupture of two yarns at right angles to each other. The remaining two Specimens were abraded to a constant number of cycles. The constant number was arbitrarily determined; falling within the maximum and minimum range of cycles for first Sign of wear and a hole. Drapgbility. The drapability of the fabrics was determined on an improvised drapemeter patterned after the one deveIOped by John H. Skinkle and Arthur J. Moreau (21). The drapemeter 27 consisted of two ring stands supporting a horizontal rod on which three, two and one half inch paper clips hung. A second ringstand with a clamp held a millimeter rule exactly 100 millimeters below the jaws of the paper clamps. Three Specimens 100 by 250 millimeters each for warp and filling with the short dimensions parallel to the set of yarns being tested were folded lengthwise with the face of the fabric on the convex side, and placed in the clamp one fourth inch below the end of the fabric. The fabric was allowed to hang undisturbed for two minutes. The millimeter scale was then moved to the two edges of the fabric on the concave side and the chord length read in millimeters. Since the Specimen was 100 millimeters in width, the reading would also be the percentage of the width. The arithmetical averages for each set of warp and filling yarns were determined and the geometric mean of each was computed and recorded. ngction. The instrument of test for determining the kinetic friction of the slip fabrics against another fabric, was the Dreby Friction Meter. Test method and procedure of the A.S.T.M. (2) was used. A sample of the fabric, four by twelve inches, was laid face down on the polished horizontal surface under a polished one pound weight, three by three and one half inches. A sample 28 of the same size as the other fabric was attached to the drum and withdrawn at a speed of about thirty inches per minute. 0n turning the drum, the lower sample was with- drawn imparting a frictional drag to the upper sample which was recorded on the dial. Readings from the dial were recorded as the unit coefficient of kinetic friction. 9212;, A disk colorimeter was used in color tests. The disks were made of two neutral colors and two other colors. For this problem, complimentary colors of the Munsell Color System were used. The disks were cut from Standard Munsell papers. These disks had a radial slit extending from a center perforation to the circumference, so that two or more discs might be interonen, with a portion of each remaining visible. The disks were placed on a motor and Spun rapidly enough to eliminate flicker. The color resulting from this mixture depended upon the relative amounts of the exposed areas of the several disks used. All colors which lie within the region bounded by the colors of the disks could be matched by the mixture. The measurement was recorded in terms of the exposed proportions of the disks in the matching mixture. Five readings for each sample were taken and the average calculated. Tests were made on the original fabric and after each five subsequent launderings. DISCUSSION OF RESULTS 29 IV. DISCUSSION OF RESULTS A. ANALYSIS OF ORIGINAL FABRICS An analysis of the results of physical testing of the new fabrics and those laundered both by hand and by machine was made to determine significant differences or Similarities in the two methods of laundry. The physical tests carried out on the new fabrics were yarn analysis consisting of denier, filament count, and twist; and fabric analysis for weight per square yard, yarn and course count, bursting strength, breaking strength and elongation, abrasion, friction, drapability and color change. Fiber Contegt MiSOrOSCOpic and chemical analysis were made to verify the fiber content of the slips. The fibers were immersed in a ninety per cent phenol solution in which nylon is soluble. From the reaction Obtained it was concluded both the slip fabrics were 100 per cent nylon. Xarn Analysis Analysis of the yarn of the satin slips included denier, filament count and number of twists per inch. Due to the construction of the fabric, it was not possible to analyze the yarns of the tricot. However, the tricot was sold as 50 having been made of thirty denier yarns. The warp and filling yarns in the satin were almost identical in denier and filament count; denier of forty four and forty six reSpectively in the warp and filling. Filament count was thirty four for the warp and thirty three in the filling yarns. In determination for twists per inch, it was found that the filling yarns had about five times as many twists as the warp with eighteen turns per inch. Both warp and filling were given a Z twist. Alexandra and Sturley (1) found that with an addition of twist the breaking Strength increased to a maximum but further insertion of twist resulted in breaking load decreases continuously to the limit of twist or seventy turns per inch. Yarn Coun§ The satin fabric was not a balanced construction; the ratio of warp to filling being one to two and one half; characteristic in satin constructions. The warp yarn count was 295; the filling 129 yarns per inch. Course Copnt In the tricot fabrics, there were almost twice as many wales as courses per inch. The original wale count was fifty five and the course count thirty per inch. 51 Weight in Ouncesgper Square Eggg The weight per square yard was calculated from samples which had been conditioned for at least four hours under Standard conditions for testing textiles. Original weights of both the satin and tricot were Similar, varying only one tenth of an ounce. The satin and tricot weighed two and one half ounces and two and four tenth ounces per square yard. Although the satin was slightly heavier in the original; that was due, in part, to soluble sizing. This assumption is later substantiated as the satin became progressively lighter after laundering while the tricot increased progressively in weight. Thickness Original thickness measurements Showed the tricot approximately forty per cent thicker than the satin. Original values were .0105 inches for the tricot and .0061 inches for the satin. This does not parallel weight differences Since both the tricot and satin were of approxi- mately the same weight. The satin was compact in structure with a high yarn count. The lOOped construction of tricot was reSponSible for its greater thickness. 52 mcoapwcfiaumpmc Mo meoapmcflammpmc m mcoapmdaanmpmc n no m M0 m meoapmcaammpoc mo mcoapwcfiaaoumd 0H mo meowpwaaanopmc 0H no mQOfipwqwanmpmc m Mo .m>4o .m>4m .m>¢e .m> Thirty Five Machine Launderings Back 50 :3--.t- Indicates location of linear measurements Indicates location of width measurements PLATE VIII 81 Shrinkage in Inches After Thirty Five Hand Launderings Tricot Front Waist Waist Hip Hip Hem Hem Thirty Five Machine Launderings Back 111 1.1.. _ -_-. Indicates location of linear measurements Indicates location of width measurements 82 PLATE IX Basistanee to Abrasion of Handlaundered satin at a Constant Number ef 500 eycie, PLATE X Resistance to Abrasion of.Machine Laundered Satin at a.constant number of 600 cycles After 10 - . launderings launderings PLATE XI 84 Resistance to Abrasion of Hand Laundered Tricot at a constant number of 500 cycles After 10 After 35 launderings launderings PLATE XII Resistance to Abrasion of Machine Laundere Tricot At a Constant Number of 500 Cycles After 10 . launderings launderings 86 b¢.Ha+ @000. mm.oH+ mb.¢H+ mb.¢a+ wm.H+ em.a+ ow.©+ ow.o+ HPOO. >00. >00. H000. mOHO. mOHO. OHHO. OHHO. MOHO. aaa.m. mao.a. moo. - cam. - ON.H3 war. n mm..1 mo.H1 mao.m+ mmm.o+ mmo.>+ mmm.m+ mum.m+ mmo.r+ ¢o>.o+ www.o+ mnmm.m mH.L on.H+ mmmm.m mnmw.m m¢.+ on.H1 mmmd.m mmov.m 0b.Hl.¢®.H+ Hmm¢.m Ombd.m 0%. + PH. 1 mmv¢.m mmm¢.N Hflom.m doom.m omam.m Nmb¢.m bomm.m mme.N HHHO.N nnom.m Nmn.m 0.0mfl w.©mm 0.00H N.mmm ®.Hma ¢.wmm 0.0mH m.mmm d.mNH O.mmm mm.a+ mm.e. mm.M+ mm.n+ mm.m+ Hm.m+ ow.m+ “5...”... O.mm O.mm m.Hw b.Hn n.0n mm ON ®.bm mm m.bm OH om.mm mm ON 0.00 OH m o.dm o mewsomz anew napam mdwgoma ease pooaaa .8 11MW11 3 m a memesoo means mmnmsoo wwamml;w Necesmq OHHAMM mammwmwmwl nma.uo mmmdeo w1.mm1w@d.oz madmno1w1 nodHIMumldmz ho 90 names: {3% page $.38 .oz comps: macnsmq QH moenanoenmm H Hm4*** meowpecfianmpou n no .m>4## meoapmdfiauepou m we .o>4# 00 00.00 00.00. 0.000 00.00- 0.000 00.00- 00 00 00.00 00.00. 00.000 00.00- 0.000 00.00- 00 00 00.00 00.000 0.000 0 2.5.50.0: 00 00.00 00.0. 0.000 00.0 - 0.000 00.0.- 00 00 00.00 00.0. 00.000 00.00.. 0.000 00.0 - 00 00 00.00 00.000 . 0.000 0 0000 00000 00 0 0.000 00.00.. 0.000 00.0.. 00 00 0 0.000 00.00.. 00.000 00.0 + 00 00 0 0.000 0.000 0 000000: 00 0 0.000 00.0 0 0.000 00.0 - 00 00 0 0.000 00.00.. 0.000 0.00.. 00 00 0 0.000 0.000 0 0000 000000 gum-00.111300- .00 0.0 w -3200 00% 0 000.03 3.0.00.0. 000000003 M .o eaom new: Ho no no 00000000 *xmwaaa0aman 0000 00000 .00 000000 11 the H mm“ % hacequ n0 condenouuom Avosnapeoov H amdmo 89 0.00 00.00- 0.00 00.00- 00 0.00 00.0 - 0.00 00.0 - 00 0.00 0.000 0 mc0£002 0.00 00.00- 0.00 00.00- 00 0.00 00.0 . 0.00 00.0 - 00 0.00 V. 0.000 0 0000 000000 .000- .0000, .000 wmwyw 0 0000000- 000000 000 000 00 00 Illa-0000.1 .30 041-002-0021... .00 000000 mucqsma GH mcnmspomnom 00000000000 0 00000 CHART II Average Per Cent Dimensional Change In Slips After Laundry No. of _ Vertical Horizontal _L: Satin Tricot Sa§;n Tricop 0 Hand Machine 1 Hand + .23 + .18 -1.52 1.04 Machine - .32 +.32 - .07 2.34 2 Hand ' 047 - 015 “1075 1078 maChine' - 087 " 015 ’1054 - 2059 3 Hand - .54 - .10 -l.36 1.76 Machine - .57 + .06 -1.17 2.10 4 Hand "' 051 "’ 007 ”1037 "' 1087 Machine - .44 - .44 -1.14 - 2.25 5 Hand .43 - .37 -l.24 2.32 ”80111118 - 050 - 048 -1026 " 2079 10 Hand - .48 - .39 -1.56 - 3.13 maChine " 046 - 039 - .84 "’ 2095 20 Hand - .02 " 027 - 085 2059 Machine + .08 + .01 -1.10 2.80 35 Hand - .02 - .51 - .98 3.47 Machine + .31 ...11 - .93 - 2.89 90 CHART III Vertical Dimensional Change of Satin* 91 Right Left Right Left Right Left No. Side Side Side Side Center Side Side of Seam Seam Front Front Front Back Back L 3‘5 Ch. fCh. fiCh. iCh. {cm 2. Ch. 2. CL (1) 1 Hand +066 * 048 +1.32 " .75 +-.25 " 018 - 019 MaChine O " 058 " 019 " 087 "’ .10 + 009 "' 057 (l) 2 Hand + 048 - .20 + 057 “1050 -1024 - .19 “1024 MBChine '1023 -1013 ""o66 '1065 " 087 + 018 "' .76 (l) 5 Hand + 048 O O -2027 " 048 " 066 " .86 Machine - .28 - .09 - .48 -1.23 -..68 - .67 - .57 (1) 4 Hand + .29 - .20 + .47 -l.22 - .27 - .37 - .86 Machine +-.28 - .66 - .10 -l.52 - .39 - .10 - .57 (1) 5 Hand - .09 - .29 + .47 -1.22 - .57 - .66 - .86 MaChine " 009 " .74 "' 038 “1060 " 019 "' 001 " .48 (1)10 Hand " 028 " .10 + .38 -1031 " 037 "' 085 "" .86 Machine - .38 - .38 - .57 -1.33 - .29 + .18 - .48 (2) 20 Hand * .95 + .76 i+2.65 -l.48 - .76 -1.31 - .95 Machine r .19 - .37 0 - .37 -+l.l5 +1.13 0 (2) 55 Hand + 057 + 057 +2065 “1030 ' .94 - 093 " 076 Madhine 0 - .34 0 - .55 *1.54 +1.51 0 *Measured to the nearest 1/16 inch (1) Average of two determinations (2) One determination CHART IV Horizontal Dimensional Change of Satin* Right Left Curved Bust Bust No. Bust Bust Under- Under- Bust of Front Front arm arm Back Hi Hem L g on. if Ch. fin. fen. Ken. 7.“‘cn. ?."cn. (1) 1 Hand -3.36 *#l.86 -3.45 -3.17 -4.58 '*1.06 +1.00 MEChine ' 025 "’ 053 - .96 -1080 -5030 {-5022 +1012 (1) 2 Hand -3.87 ‘+4.59 -3.48 -3.93 -2.21 - .18 + .87 MaChine -1050 ' 007 -5048 -3053 -5057 +1090 + 067 (l) 3 Hand -2.58 + .91 -3.57 -3.60 -3.24- + .47 +2.07 Machine - .51 - .48 -3.06 -3.53 -4.08 +3.05 r .42 (1) 4 Hand -2.58 - .02 -5.o7 -3.17 43.02 + .60 11.64 Machine + .54 - .55 -3.52 -3.56 -4.29 +2.89 + .53 (1) 5 Hand -2.32 + .91 -4.34 -2.69 -3.26 +1.07 +1.98 Machine + .54 -l.44 -3.51 —3.56 -4.29 '72.89 + .53 (1) 10 Hand -2.32 - .01 -3.93 -4.03 -3.74 +1.22 +1.88 MEChine 1' 057 O -2064 -2068 -4029 +2.60 4' 055 (2) 20 Hand -3.06 1‘3.70 -2.50 -3.45 -2.88 1-.89 +1.33 maChine " 051 O “2052 -1069 -5085 + 025 + .65 (2)35 Hand -2.04 +4.63 -3.33 -5.17 -3.85 +1.19 +1.70 MBChine -1001 +1078 “2052 “1069 -5085 f 023 f’ 056 fiMeasured to the nearest 1/16 inch (1) Average of two determinations (2) One determination 93 CHART V Vertical Dimensional Change of Tricot* Right Left Right Left No. Side Side Side Side Center Center of Seam Seam Front Front Front Back .l; % Ch. %Ch. % Ch. % Ch. % Ch. % Ch. (1) 1 Hand 0 + .09 1 .40 7.40 -r.18 + .001 Machine 7 .09 1-.45 +.69 .+,59 -+.36 - .26 (l) 2 Hand 0 .00 - .102 - .20 - .26 - .36 MEChine - .27 ‘* .0005 ‘I‘ .10 'I- 030 " 009 - 080 (l) 5 Hand - o 44 ‘F o 004 i 030 "’ 030 ‘ 055 + o 18 3550111118 - 056 ‘f .18 +060 '1' .10 + 056 " 053 + 010 "' 018 " 027 050 - 018 " 097 (1) 4 Hand - .oo4 - .09 0 Machine - .71 - .36 - .10 (l) 5 Hand - .70 " 044 - 050 1' .10 ‘ 026 " 062 MBChine " O76 " 036 - 010 " O49 " 018 " .97 (1)10 Hand "' 055 "" 060 + 010 "' 050 " 026 " .71 machine - .53 - .36 - .20 - .10 - .36 - .80 (2) 20 Hand 0 - .34 ..,2o - .40 - .88 - .18 Machine 0 + .36 4-.19 + .39 - .35 - .53 (2) 35 Hand - .7 - .52 +.2 - .4 -l.l - .54 MEChine "‘ 018 *018 +039 0 " 036 "’ 071 fiMeasured to the nearest 1/16 inch (1) Average of two determinations (2) One determination CHART VI Horizontal Dimensional Change of Tricotfi 94 . Top of Normal Curved No. Bust Slip Waist Waist Hip of Front Back Line ‘ Back Line Hem L i Ch. iCh. 2 Ch. % Ch. %Ch, Z Ch. (1) 1 Hand - .65 -1.96 — .37 -1.71 + .15 -l.69 MEChine ”2075 -2082 " 076 -5099 -1050 -2020 (1) 2 Hand -l.28 -4.o7 - .87 -l.69 o -2.80 Machine -2.40 ~3.6l -l.l3 -3.58 -2.41 -2.43 (l) 3 Hand - .63 -3.10 -l.40 -2.13 -1.27 -3.01 Machine -l.90 -1.03 -l.70 -2.58 -2.87 -2.55 (1) 4 Hand - .96 -2.91 -l.09 -2.64 - .47 ~3.14 maChine -;L038 -3001. -1070 -1099 -2071 -2071 (l) 5 Hand -1.46 -3.88 -l.94 -2.00 -1.30 ~3.37 Machine -2.24 -3.41‘ -1.70 -2.58 -3.59 -3.25 (1) 10 Hand -3.05 -4.66 -2.27 -3.18 -l.73 -3.87 Machine -2.75 -3.81 -1.70 ~2.58 -3.47 -3.25 (2) 20 Hand -5.o7 -4.58 - .33 -2.85 - .81 -3.88 Machine -2.08 ~3.66 -l.54 -3.54 -3.19 -*2.78 (2) 35 Hand -3.68 -5.34 -2.3 -3.56 -1.63 -4.31 Machine -2.42 -4.47 0 -3.54 -3.67 -3.24 *Measured to the nearest 1/16 inch (1) Average of two determinations (2) One determination ROOM 1155 ONLY, MICHIGAN STATE UNIV RSITY LIB E RARIES 7 6 0 904 3 1293 030