—_———— _——— _—————- _'_—— _.'——'- __—_———- _—_—-— _—__—— _———-—— _————— ___———- ————— .-————- ’- AN EXPERIMENTAL STUDY OF SALT CONSUMPTION IN THE EAST LANSING 'WATER PLANT Thesis for the Degree of B. 5. Floyd ' Vermette 1936 3“ .0 3:3 467% r? ' ' .e’f'l- -‘ .3. 'v . ‘- 5““-: 5 .fe‘~ L It? . 3' .H‘ I” A -‘(l p“: ’v (If; yh' 3: ,w‘ {1}... ' ‘- v - { ‘ 'L3w¢.v- 4.3" 0"" ‘ "In . «Jr-w 4m;- . . ‘ ‘ ‘5 ' ll: 3‘31." :3; ‘ .-. '€,"u""‘>‘ ‘ ‘ 0:4,”. 0 iv." .... A. a «a w. . . ..... E .. - . .“9 .l (v. A]: I21 . r ..r ....».OW.V 49%“. .uuhfi'fifle‘ Vx+1£ n. 1 .x. . FE. . , ... 0' fi‘l s 2. An mammal mm of Salt Consumption in The 2mm. mum; rWhen:- Plant A 'l‘honia Submitted to The Faculty of mourn-m STATE} Gamma or Anlztccmn J22: m: A3531) 30m: :2: T32! ! - ‘ Floyd :fimetto Omflidate for the Degree of Bachelor of Science ‘4 .r V J) .m: 19 9t; - 1'34}?th A 35.". 3371331305113“ I wish to take this opportunity of expressing my ap- preciation to Mr. Theron: for the cooperation and assis~ tanoo he has rendered me in my work on this thesis, and for the use of the necessary equipment. F. L. V. I 3““: 1!" (_ ,l-‘ . 1% 'Kli‘fi’ . K) 2.10.31; Mimi; Water mm Plant OBJECT The object of this thesis is to find by experiment the least amount of salt it is necessary to use in each of the five softening tanks of The East Lansing Water Plant, and to suggest any improvements which would make the plant 'Operate more economically. INTRODUCTION Zeolitc is a name given to a group of minerals com- monly found in cavities in igneous rocks, from which they are derived through secondary alteration. They include thompsonite, natrolite, scolecite, analcite, chabicite, gmelenite, phillipsite, harmotome, stillite and heulan~ dite. The name is derived from the boiling reaction be- fore the blowpipe. The engineer, though, defines a zeolite as any chemical compound so imperfectly bound together that its composition will change dependent upon the concentra- tion of chemicals in solution in its presence. Commercial zeolite is usually artificially manufac- tured because of its greater purity. Artificial sodium ze- olite (NaAlSiO4‘BHgO) known as ”permutite," is the material used in water softeners, because it will exchange its sod- ium for the calcium, magnesium, iron and aluminum of the hardness producing compounds in the water, thus leaving the water with as many chemicals in it but with zero hardness. When the calcium, magnesium, iron or aluminum zeolite is then placed in a solution containing a greater concentra— tion of sodium, the sodium replaces the previously mentioned elements and the original zeolite is obtained. In a zeolite softening plant the sand is contained in tanks - over a layer of gravel — through which the water to be softened is passed down until the non—hardness produc- ins substances of the zeolite have been exchanged for hard- ness producing substances of the water. The sand is then washed by running water upward through the tank to remove any particles of material and dirt which may have been caught in the sand. A standard sodium salt brine is then run through the tank in the same direction as is the water to be softened, until the reverse of the chemical reaction of softening takes place. The filter is then rinsed by passing raw water downward through it for a certain length of time. All effluent of the regenerating process is dis- charged into the sewer. A portion of the brine which has passed through the tanks is saved in some cases but its value is doubtful. Its practical value will be shown in this paper to be negative. The largest cost item in the operation of a zeolite water softening plant is for the salt necessary to regener- ate the zeolite sand; therefore, in order to operate most economically, the salt dose must be cut to a minimum. A ze» elite water softening plant has the advantage over other types of being able to produce zero hardness water if de- sired, and there is no sludge to dispose of as in other methods. A zeolite plant can also be made automatic so that it does not require the constant attention of an atten» dent, whereas it would be a much more difficult task to con» Struct a soda ash or lime treatment plant to be entirely au» tomatic. Other types of softening with coagulation, though, are more adapted to use with water which must be filtered, for the coagulant removing the hardness also serves to re- -5- move other objectionable insurities, but it requires more space than the zeolite plant and a method of disposing of sludge must be provided. In the United States and abroad, zeolite softeners have been used for more than twenty five years for soften— ing water from various supplies and for various consumers such as laundries, the textile industries, boiler feed, breweries, etc. At the present time there are over 150,000 installations of zeolite water softeners, both large and small, in the United States. Household installations, how- ever, are decreasing in number with the increased use of -municipal softening and treatment. .4... DESCRI?TION OF THE EAST LANSING WATER PLANT East Lansing's water treatment plant is on the east side of town, working with a total clear water storage of 110,000 gallons, 100,000 of which is effective. There is a 100,000 gallon storage tank at the site of the treatment plant and a 10,000 gallon tank on the west side of town, but some of the total capacity must be used for cushioning. This is small for a population of 8000, as East Lansing has, for it provides only a two hour average flow. The daily consumption of water ranges from approximately 350,000'ga1- lone in winter to 800,000 or 1,000,000 gallons in summer. The plant runs intermittently, alternately filling and al- lowing the tank at the site of the plant to be emptied. If the plant ran continuously it would have a capacity of hpQgOOO gallons per day. The water is drawn from two 12 inch diameter wells. Well number one is directly under the plant and is 390 feet deep, its casing sunk to a depth of 150 feet with a strainer 170 feet below the floor of the pumping pit. The floor of the pumping pit in 10 feet below the surface of the ground. Well number two is a little to the north of the plant and is automatically cut in only in case well number one is insufficient to supply the demand. Well number two is 392 feet 9 inches deep and equipped with a six stage centrifugal pump. Well number one has a five stage pump. The casing is sunk to a depth of 150 feet and the strainer is 170 feet down as in well number one. D . ' f. \ / \\ n fl / 2110.1;th vulva and Iii-Pins m 5.5 6 Control lane]. The water, as it comes from the wells, has a hardness of approximately;300 parts per million and is softened to about 70 parts per million by dividing the flow to go neard Ly onewfourth through two iron removal tanks, and the rest through five softening tanks. The iron removal tanks are the same size as the softening tanks, seven feet in diameter by nine feet in height. They each contain 103 cubic feet of manganese zeolite sand and reduce the iron content of the water from 1.0 part per million to 0.1 part per million. This amount of iron in water, although very small, is ob- Jeotionable because of the rust it produces on clothes washed in water containing as small an amount as 1.0 part per million of iron. manganese zeolite sand is made by treating sodium zeolite sand with manganese chloride, and then oxidizing it with sodium or.potassium permanganate. The reactions are: NaOZ + EhClg - mnoz s 2NaCl HnOZ + 2NaMnO4 - HaOZ e linOlli’ngo.7 In the latter reaction, the higher oxides of manganese formed are carried to the surface of the grains of zeolite. When water is then passed through the send, these oxides Bite up their oxygen to the iron of the water in the follow» in; reaction: Maps 9 unosngo7 . 4Pe(HCO3)2 . unoz e SMhO e 2re203 e 8003 e 4320 The ferric oxide thus formed is insoluble and is precipita- -g- ted on the grains of zeolite. These iron removal tanks are regenerated by hand with a m ngsnese salt solution each time attu'approximstely t,080,0C0 gallons of water has passed through each tank. The maximum rate of flow through the iron removal tanks is 105 gallons per minute per tank, and the maximum marking pressure is ?5 pounds per square inch. The five softening tanks are regenerated as previous- ly described. Their oporation.is automatic, being electric~ ally controlled by a tin: sequence switch capacially de- signed forthe purpose. The time sequence switch Operates the motor on the multiport valve to regenerate the tanks at the preper time. Each tank contains 203 cubic feet of sodium aeolite sand and uses about 14 inches of brine from the 18” 1 60a brine tank (055 gallons) for each regenera~ tion. The washing period of each softening tank is about 10 minutes with a flow of wash water of 250 gallons per minute. The brine is then run through the tank for approx- imately 15 minutes, depending on the salt dose used. Then wash water is run through the tank for about 20 minutes at liS'gallons per minute. The plant also embodies equipment for the use of re- covery brine, that which has been used but still contains a certain amount of salt. This brine, when used, is run through the regenerating tank before the new brine, to re— claim any of its value. -7- DROCEDURE The procedure was to decrease the salt dose for re“ generation a small amount at a time until it could be out no more without causing the tanks to deliver hard water he- !ore the time of their next regeneration. The soap tcst for herdness wrs run at intervals before regeneration to determine if and when the tank started to deliver hard eet~ er. The recovery brine was used at the beginning of the experimental work, but discontinued so that its practical value could be determined after the economical amount of salt to use was found. After this was done, the economi- cel amount of new salt brine was ietermined while using the recovery brine. Some unforeseen difficulties in the operation of the plant were encountered, which caused the experimental work to proceed less smoothly then it might have otherwise. The theoretical amount of flow of water to each soften» lag tank was confirmed by the economical amounts of salt necessary to regenerate each tank. RESULTS No attempt will be made in this paper to exglain the irregularities in amounts of soap solution necessary to pro- duce a lather in 40 cubic centimeters of the effluent from the various softening tanks as found at the beginning of the experimental work, for the operation of the plant at that time was very irregular, due to various causes. 0n occa- sions, at that time, regenerations were skipped and tank number five once got two doses of brine in one regeneration. The recovery brine was also being used then, thus introduc- ing two unknown quantities, a circumstance which usually makes any experimental work of little importance. Any ir- regularities experienced before the critical point in am— ount of brine used was reached were due to these or other similar causes. Another variable introduced at one time during the work was the cutting of the amount of water go- ing through the iron removal tanks, thus increasing that through the softening tanks, but this had to be discontinued. Tank numbers one, two and three delivered zero soft water during theiriéntire runs until the brine dose was out to 13 inches, indicating 13} inches as the least amount which would give proper results. These tanks were then de- livered 14 inches to provide a factor of safety. Tank numbers four and five went hard with 11 and 10} inches of brine respectively, thus indicating 115 and 11 ' inches as their economic values of salt dose. These lower figures for four and five were due to the decreased flow of water through these tanks. The decreased flow was caused by their 4 inch effluent pipe being too small. The economical amount of new brine to be used with the recovery brine in operation was found to be 16 inches for tanks one, two and three; and 14 and 15% inches with four and five, respectively. v H F140?! D 1912-;- we: \ r it v J V 4 V IL 0 [1 r 4% E If M xv % 1' H 4 ‘ Rm . .. .aumrummH-L mums“? WM“; L ”Wan; L1. .n-Hmth”. 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I r. 5 3 3 {‘3 {\3 t3 3‘!” i»t) Plant f $150 13 :5 in Plant Stop filimt Start 15 Plant {312.023 P312311; f ‘~. 'f-S Brine (Start 5 5 Us ff 1.: H) a a-n 51‘! mm dose out t 3 C), I)‘ - filo J 57: 4E 130:4:0 ):3{) 10-5" 110 O. 6" 33;, m brine 1:01; Date 5‘6-5 36 $34-$56 25-13-456 \. Lv 00 O. a. O. ,. 5 ‘ u d [I I) 3:14 35.9 t ‘g :' ‘11 ' I .23. .7 It .0 o. ,s“ \‘ '1 art 2.. U V" U 5: f? :}3LJ -~ ' .\::51’ («ml 8 :55 7:18 9‘ W.“ ":35 'f 3.41:}, " $.34; 2,3: 1:5 3534.)}: ."~ :130 9:12; “z: it’ 0:31. 9 :15“ 7:15 'fflh‘ 9:135 572‘HV3 33:12”: 8:43“. 8:53 9 :35 11:54.- 11:41) 11:58 J‘io: 2:. 3’."{. .i'x 0? {o P o." {o jxo.i" (1“,? L1: 2: 1 '- P3. 0 V‘ C. J . " ‘ ‘| . 1 VV " H.” ‘I r P 1,) U! 013! I): ' ‘A (con-timmd ) I 3‘31}: ' ' I I F "ew ‘90 V» U. PIA-ETC. Plant ‘ 4 ‘ i I ‘1: 5 3 C I. I IS {’5 I". W0 7% #0- 0L {11,831. 3 ".‘unk ' a as at (x 308.31 :1 31 r I r - l u , 1' If; 3:33 3 Wm}: ' '1‘.) 17;: La 3 and dronyinn; ho‘ntlo v -f' 33" Trina (low) «mt to start With 7'" 42 0“ Va 3 S 55 Pizmt Stop v13 1’1: :3 1% Stop 7" x) 7" .0- ”:5 1?. V 5: Stop I )[7 5n ‘ fYtilo lieu Date 5-1 " )--3-4 3 5-11-39": l'1b1o 3:53 5:02: 5:1“; 5:17 is :9. 5::15 5:40 5:50 625-8 (3 24:7 6:55 I’- :59 7:07 7:20 7:63 “:03 7:56 8:04, 8:27 :1 :39 8 :59 43:03 4.41:3 '7 :11 9 :10 9:11 9:130 9:133 53 :57 43:3 J r2 :07 41:11; 1"»:515 7:00 ’730'7 7:11? 7:13 7:37 7:535 was 8 :11": 8 :N‘. 23:59 12.5:011 12:09 DATA (0011151? 11 10d ) "fink ""szc "‘nnk '1' ml: ' ‘mfl: :-:ta. 0 Raw 341‘ 13' :5 :5 W; {3 7‘» 15 R I Plomt Stop :; 5 .L’lacfi; Start 6 '5 3 3 W5 3 I; It :5 H 3 1715 A031. l’lw'lt Start 23 3 it 3 ES {‘5 ‘37:? Poi-to 3 1‘5 '3} 3 5 E'Irine (1090 :2 1.51/4" to :34: :5 ”'3 Plant {Stop . Adi. 3655 53 {'7' 25 5 :31; .1113. 11'1") 33 2-1 3 i-‘Jto 3 1'5 13 3 S 24: S I'h'im close out. to :5 :‘3 1.91/16" starting With m; 5*." I]. :; 3 f 3 r3 :5 :5 :5 13:5 5% IS :33 ..-’1a.nt Stop J1. .3! .I’. L 3 3 2’5 2:5 5 I Brine 1'.sz filled up 1 L" too “'7 fill after i'} 1. I”: R :5 .1: W7 3 Flu.) 1t mum’s 1 ”3.:; 3 3 5 3 an 11a bate : “113—526 'T‘ine 0‘): If“: I 5-: :‘fi.’ 13 X.» 1:06 1:15 3:11 {5:15 3:36 3:35 “:30 6:53 63.39 8:45 13:5.“ ‘3 '.':. :5 " ::31) n .I'n .04; 9:1” . :26 9:37 10:69 11:05 11:12: ll::.“ '6} 124.5 3: 1'7 (13:33” figfl'? 5331."; fl 2: 3:3 6:40 DATA (Gantin'ued ) "'mfl: "Tani: ”H.313: Tam-t: “farm Etta. 2:“;in :4 l a“: 2 W 5 5:? 4 it" 5 T 14;]. /L3" 01' 1" 3.: brine to a-is‘: 4 E; 35 1; W5 5 3"le :1; Start. WIS l’lzu 11. {Start 3 'f I i 3 3 c \r' (-11) ’lrwt f‘ tart ., f3 1‘9““):3’3' b31116 1.0754: { R 1") 3 F3 15,"s[5:“ brine Plant 3130? 4:0 :1: h“ 1.3;. Plum sum, :5 S :5 1 ‘ '7 ‘..-.'>5 W1 . .. 1': 15 14," 03‘ brine to in a 53 i3 '7 {5 Plant. Stop ,1 15 3/43' of brine to 4 rs :s :s 5 :5 ms 1: 13 1/5" of 1’11 Lift Start brine 1'2; B 14" of brine 112-: :3 41mm .3100 ;: .3. 3 3 3 5 2.33: 23:31:48 mat at 14: 1/4.:"t0 start V! 1;.1171-3 i“ :‘3 Pump 3901:) ‘V I-J =3 :5 1 r’:.:" of brine l’lzmtf Stop "1.8.11; th‘r‘t Date r-lS-SG Time 6:45 6:55 7:00 " :11 7.01 11:49 9:01) 9:07 781.4: Adi- 7:25 7:55 7:41 8:09 {3:111 8:34 8:35 10 :34, 10:43 10:53 12:01) 13:14 13:30 12:3 13:é5 5:03 5:10 3:15 53 :15 5:34 8:34 31:40 6:57 7:05 7:13 7:131" l7 3:11!” Noon ii‘mfs: :31 D R 5 WI": 3 Pfiio S ‘1 .1. 1;: 1/2" Jnaigq. TI. q; [I 6) “Ynfl: 5-5:} {A 513 DAfiA (continued) Wm}: Tam: szk Stan Raw :5 5,1. 4. 5 '7 5 5 15 3 3 1'13 B 15" of hrine to1# 5 lflamm; Etc? 5 Brine tank B‘V’S 61/8" too after1#*5 R 13' of‘brtno £01? A F) 3 5 .3 V3 Fla.) It ntOP Tine dose 301; at 15 1/13" starts with =39 1 Plant Start {.3 5 :13 17:5 Planfi Start W3 33 12 1/2" of brine to R é'4 Plant Start 7 5 n3 W3 23 of brine to ‘fr 5 B ’30 8 1/2" 1300 :nudh.br1ne in tank after 1% 4, 33 12 1/2" of brine tO‘fi'fi R Plz.nt Stop 11 3 S 3 3 )ate 11:21: 11:87 JL].:‘%55 3:03 13:30 ILL) 2:3”; 13:155 12:52 10:14 10 :1315 10:13:} 10:11:11 11:50 11V? 11:56 13:26 12:5n [50350 ’.'.‘1 m}: W 3. YES .3 ‘ank a". i 1: Plant Plant n Plant 1. ’lwrb WT} 'i‘apk bu ’ '7 7? .) r)’ x) 1 ~. '9 .5 Stop c v? "5 \J 18 “Hi: i 13 .h. '5‘! y: #3! CR DATA (continued. ) P" V. M‘ a V1 n: 4.1 8 7 Q 12:" . ,, 13‘) of brine f K) a”? ‘. a I} 1) k 1.1:" of brine t04# 5 .3 Sta. Raw l to i: 1/"" of brine to 5 5 {“5 VS 4.- B 113' of brine to '7‘}? .1. It '. Q \7§§ 3 13" R 5 W6 3 12 m' of brine Rtoaéé 4 4: of ()‘A 4 Plant «'1 .13 Wm B 12‘ of‘brine Plant ._. .. x 1013 bring t0«# Stop Start toififi 6': DA".‘A (continued) '71 Date .. inc ”am: 'L‘zml: Tank Tank Tam}: Sta. Raw 5;: 1 5r}? :3 5:5 5 9'5 4 A 5 19:4"; 33.”. R Plant Stop {3:39 B Brim done measurodrtlfi 5/8n 2:5 R 3 3 :5 5 '31; 11:: 3:15 B {-3 33 3'33 7’13 3 :50 .73 42:01 R 420‘? Plant nton 5‘3 :58 - 5246 113” of brine to ~35 4 a“; 51;: 5 1393!. Of FWlfi-Oz'lfl 52:18 1 rpm-m 7:05 AM. town's "’ 53m 7::{3 4: 72:54- 5 4 7:41.63 M 7,395 :3 1:3" of brine to 5%? vi: 3:00 R (3:03 Flatt Stop 9:01 5 $3 5 S 3 9:31 “"4 924-). B 11 1/2" of n 924:8 R brine to a"? 5 10:13 ; 10:31 Salt (1033 set at 13" start With 3531 10::25 Plant Stop 11 1/13" of brine to 3:” 4 83:13:; Polio R 23:27 Plant Stop 524.1% S 5 4:18 "'5 42:38 E 11 11/23" of “24“ brine to a": :3 624:7 Plant Stop 3:355 S 96!:45 1W1; Stop II: .13. 1/9." “ring: to 5-17-56 1:16 Julio Plant Start a: t}; «is 53 P014. , 1324 A3730 3.} 5‘16“er 0:155 S 4 9:55 1‘14. 10:05 13 .11 1/2" brine to w?- 4 10:11 3 103115 Lg’lwzt {H.039 11:19 a 11:31 W4: 11" of brine 11:41 B to #3:: :1 we :3 an :9. Q Q but (I! uni-'18": 3‘. § Tim 1 :94 1:3 :0: 1:3 :30 ];3::' 13:4; 113 a"? 53:13 2:33 :zzisz. {3:1357 R:I§5 13:4JS :isffi7 fix'KS I—‘HH HHHHHNEH «'1 mar-m (twink-11100. ) £1. a m V1 37! . 1:. 1,, Mb: 4mm Junk .unl: Sun... um I ' _ J q. if": 2 ' 1: 11' 3‘53: 4 i1... 5 fl" 1. 5'; Plant fi,o;» 1r: 16' 14 25/4" of brine to 2 54: :3}; \hus 25 Brine dose set at 14" B start With 171 :5 film 115 Stop "V 5 a WA: . D 11" to # & R Plant Stop Tug B 11“ of brine Flaunt f'k‘Eart to 5'}: 5 S \‘m 11" of? brine to :3?! 4 as fun. Plant 911.01). of f‘wlt-B—SG w: B 10 1/; z" 0121‘ brine 3{ to #EEE Flair; 511013 {3 5 6 '7 1' $13 '3‘th 111;; value of recovery I} at 6 '1 if“) r; v: 14313 C ;'= 1 5-19—36 4:30 I’.::. 3 ézfifi 6:313: W “:50 9:1"; 5-30—86 13:50 1531. r ' r y 'i P‘ . ~-..,,:_ --. JG 1250 (‘s :10 T! "35 ) {3 3517} ll ) l 1:} U!) Noon 1:3 Hf} 9.on EEK)?» 1 :70 J. ('flJ E3 55 {2 fi:; ('3 a"- .c '7 or: f3 ."51 1‘ 53 11 5" 5 5% A.x. W H n “P a“ flit. 9:013 10: .13 11 :‘M: r- (at) r' I "-1 .ll 1 "ns 1:32“: A0:;' ‘5! i3 1!. ’f 03 W «‘3 )4: DAmA brine "milk ”as 7: ”(u/31’; Tom: Ste. 0 Raw 53:3 fi5 fi 4 =é31 3 3 3 ’5 :35 7-an brine WIS 01113" p 13' Recovery brine on '6! 27 W 1‘! '3! Shard. ‘9.’ I" ‘3! Fm! brine only start with get 1 we}: 15 1/4" brirzo W "'35 "13 14 1/4.." brine set to start ‘" with 51': 1 W 1'! :24; ?fi m :3 1/3" brine , start 2 3?? .g '9' U V!- I? U W W gr V! w ".7? U , Y! Recovery brine star #- 1': 0' . fi-frp 7' .) I... I) " ‘1'? .1.) 8 IS IS 3 mxte r3” ”:4: '7‘: 3!" l‘ 1 9" V fi‘og' :f":)r7 7113-10 110‘ --—-. 09' 113:1} 3.“) 15:18 A in: ‘¢:o~J-' 5w; (1,:v;,J l ":t)0 ()0 3:3 10:19 11:10 vagif} of“ IJ:I. 4:~L’i {33'}? {13:35 7:: If': (It? 2 92538 1:)uu 1 11:5 {-5 :3 J“ 41:53 {3:58 (HIV; 9:51: 10:50 J, :50 luzfifi 1:14 ‘I' ‘ f5'“' .ee 3) .00... E H .‘-. IN V *3 J-O‘ 1’". DI. l?! '."A (oos'xtia'rued) '1.- h ‘ I ”i 7' a l. '1' 7 .8. '"J ‘ a: L! 1.33;. 30.: 1 ‘ am: my: S Ue. Law I I ' l o , n F r. 71’ l 5 u , “3 «.5 ‘1 ’ A: ’ 0 J :' 103‘. m no 1'4 1/23". M 3 :3 :5 1.790 mm brine only ’ 3 5 n- {s Y'lfi etm’t ii" ".5: 1795 5 3 3 V95 80 W U 12' '1! W U! W (A ‘f! «”3031. 1 0‘5. 1,1 m l O {5 F5 {5 '. ’3 ‘5! 5 I ."5 {3 3 {35 W U :36}: W 3 5 I5 3 £34- 111?. W ‘5! ‘5? x .' Q i a W ” fl :3 Wu" 0 a.) W 7‘? VI 0 W DAWJ. (cont iamod) Date “inc 'II; .313: “an: 13: Hank ”3.313; ”3.111: [Sta . 13m? -' 1' I g.‘ :3 l :‘3 :3 in :5 {:12 4 .2“: 5 ll:'i)5 W Fv-zlfw-Iit': " .136 Adi. 3:7 . é . 5 :i’. '3 K7 ('2 :2: t. “7 9 z '11.”? 3 9 : 153 8 9 3130 I? 13 173153 I} S 53”: ll: ; l; J :38 Y 1 :3": TI 3 1‘? ,' ‘Imfi .7.- .4. - u“ . 2". . '-:‘ . ‘I‘ f“.' l I ->.1w07W‘3E‘!Mv£fiJ#~ IFflffl' _ . CJU:Z331¢"."TI'73T 0F EKL'UL’ SOLWIOII ”(We of Water“ Drops of Soap t0 in ppm. Produce a. laminar 2:) 1:3 2&- 14. {-30 16 {'55 53 £20 :3) 4:5 3’13 .. M) :34 j 5!; 36 s‘ 6') 28 ail {:5 :51 a} 070 5‘3: 33 {3(J :52; j 90 “3:8 i 12) J {La-3': ‘ 110 50 2 11.5 54- 120 5:3 11:5 RE (“No diitrorem (11131191411; bottles were used during; this experimntal Work on 11162.net Imming; Water ’hmt. . The abava oalimticm Was made with the first bottle (1). Bottle (1) 130‘} drops n 709 ml {*161‘0118 =3 1.0331. Battle (:3) 5% drops I: 10.0 mt .5195) drops I! 1.0 ml. 4.0 0.3. of Water Were used. in the calibration- CONCLUSIOHS From the results of the work done in performance of this thesis, it has been concluded that the claims made by the Permutite Company for the value of the recovery brine equipment are based on the chemical analysis of the recovery brine and not on actual tests of its regenerating power, for it has been found to have a detrimental effect instead of a practical value. The flow of water, as calculated, has compared quite favorably with the amounts of salt brine found necessary to use in the various softening tanks, except for the indicated difference in flow of tank number four over tank number five. This difference was probably caused by some unseen obstruc- ticn causing excess friction in number five. The smaller flow of water going through tanks number four and five could be remedied by installing equipment to cause less head loss in the flow of water through those tanks. It is suggested that the effluent pipe from those tanks, marked KG' in the flow diagram, be made a 6 inch pipe instead of the 4 inch which is in place at present. If 31 were made a 6 inch pipe, and the first all and two seen tions of pipe of lines IJ and IL were made 5 inch, the flow should be evenly divided among the softening tanks. A further refinement could be made by a slight adjust- "nent of the tine sequence switch. ..| .3: kt” I -_ sI .m’? ‘3' (2‘ 5...;13“ ‘ ,. 'i.- , :‘9‘N‘ “I." P 3. ' l-.. . (Ajax.,f...\'.‘$xc.:cng-. . ' 4.. war a. wan . 9 ‘2, _ t. . I", -In _ v-f “ _.. ‘ 91:...1"‘< .. )Ifll‘iin‘l .JI ,- 1,.I . ‘ I f)... f':'§( fir-$3; ‘2‘.“ ?’#}IT{3¥V\. F? 'i-Nfise‘fcé‘: 7t" "J! $f‘fefl" 9%: iv :5" W ' - ' > w: - . - . v . I ‘ " I‘ ‘. 5 ' . . :‘IQ-(. . .' 1. . ., . ' I» :1 v 1‘ '3 "‘ ‘I IV )“ O: ‘n'l‘l’ ‘1' ’ - In ‘ r ’ "‘L e ‘. '. . ‘ i, k:‘ I‘Ly’fif’: . .n . I e I . ._r . , ‘- a v r , ' . ". ' 9 ' "thwflfi‘g‘iy'. “:1" . “5;.“ (S f w. "1' ‘7'le 36'" 3’ ‘ , \' ' W ‘4 ' ' “Hi" I Jinn-LA arha>'l£:a"% \ ' ,‘ ‘ . .1 "'1 '4 «Vol N :' "a" ‘f"¢-‘ "‘\"—'5"‘ -' u:- d— ‘ ..'e3:'I 'I'v..v'-\z'.~p‘vh ‘.J ‘ .’,' iv. ‘.v‘:.' ~ mew]. .. a s :u ,3 .. , )y I . “,4 ‘ ... n . . . -. ‘.\'- . “' * ..o ' "V0" Ru. 5' ""d‘ ' . 4 ‘-'- "II p ”P: 03y}- '- a, .-‘ - - ‘ ' . .I‘ IIJ,~,I '. . . v. . ‘ ‘. ‘|n'. I 4 . u"/~ _ “I, do: 3;. _F. ‘ I ‘— '5’ “if, .7 ' §~ ‘ ‘fi . .-' J”_»4 I ‘ I Q . \ Q N r v 4.‘ . . . ‘ P 4 ct. - x .V n s‘ ‘ 0' — r n ‘I ‘ . iv. .'~ H" - .‘ f "'j ;.,I r 3.425;; v - ’ ' . "J. ‘ ‘5 Q <. I 'c' F- D 3:3 t Ff , I V . ' L ,4. ' I I ‘3 s e 7‘ \ \ o .«q' p a l , - \t‘; 'v ‘ 3 .. "’1 ,' II 4 o I'. '.' .4 '3’. DY) I ‘0‘ ,. . . ." '1 le" I) v I ».- r .Lr ‘4, ~' ,3. 'r: s; "u I; , '3.“ \ :." , .-‘ I W ' a ~ P . . n4 I . i.'; " ‘C ..y .‘ \I.I Jr. 4 \ ..~" " 1.. I" -\ .~ . . I A. l 1‘ A: 3‘ .“I a. ‘ , '4 "fite '\ I IA.‘ V e ‘- .. a ~ f3 3‘ Re'. - I - . . .. , L h A I 13‘2“. . ' .1 ‘ ‘ .r r I .‘.‘./ -r|.I 1'. '\ ,I II. .II... R ’1’ I .‘f‘ .*,“r,: .. .- ,\ 5‘ o u, . ~' -. 'If‘ ' r - '_". . . -'I ' o . .p O I.- \'. ' -. . .. ' -. ‘ . 't" ' é . n “:"F I. ."f- ' , I'ac ‘ V )1; “ - \a ’ v '; ' x n .I ".1" ’I.‘ Fr. [07: .J' 3’ 4" ' N '1 . “I‘VC ' '.'3~,:. -','r'( 3 ‘1"1‘. run ‘a.' . '3 f a. - -“ ’ 1'» ‘3“: ': . ‘."-.‘.."". '3 .; '."‘~ "-‘ -; v, c L‘ e“ ‘ . I "I i ,, .. .. 51 .v1,, r . t. v I . ..' _|( J ”I A.U‘e‘ .I.a l‘I'fI _‘ . _ , .a ‘ . up _ I.v ..’ It . 4'. ' . . ,\ . , .!v v‘ t 3, . r" '.‘.. ,. .. .. «, b . (,' I' x. ‘54 . l 1\ \‘Q’dk “H .r .. .c . ¢"I~ - z . . , ~..~ 0 ‘ ' - k L‘.‘ ' “ ‘.- w““"" 33-“ -" 1 h‘slf- \. .fI Iv v __‘.‘ v" w:’ 'II 3" ,:\. III-u \MI, I .‘r 1“ l, ' ~‘u . ‘I ,,»'l.\ .v 'I' P, L‘EIIJ.‘ ‘ “ ‘Kn'p. ‘ ,".,‘P. . r ', II! . LOII‘C, A I. .‘V, 3' 7'.“ ‘I. '. ’ . ‘ _ O , J . 1.. 'J‘ . 'I 'I I I | ;'I 'lfl‘ I 4‘ \Ir ‘O'I . - w v a I. . . l, - r r: . t . l . i “I . u . Kl , . Y A . I p‘ . . .b.,n 1 A.,_ . e. ‘ ‘ ,, v‘ . .I. r u .p e .4 , .I,\ s I A 'hfu. .‘...'.,A.“..\‘..'..,. U, .~‘-\...-.'r'w ns"* . « ’ A‘ ‘ 3‘ ' > J“ “"3 ‘9‘”? i .l‘ "‘ V - ‘1' “ yin-i I 'V““ “""-\‘.o‘\ la ‘ - o ‘ .I‘ ' " fl . u ’ l . . ..- ' .K. ‘ “bl-H: ""!e"”“, 5 '79}!. e.’ e. .. I n"' I . I'd . C "l ’9 ", ' .' . ., f L."* " ‘u ,.'l..n. . ' M " ' 'J ’ - “ ‘ 1 " \ l '\ ‘9 ) ’. II . '.‘~ rd; I . ' ’ Q. r I u u ‘ I. f." I , I ‘ ‘5 v C -" . .. . v' '* “A ‘” w'-3"r\" ‘ " - ,. ‘t‘d ‘ o. ~- . ' . ‘ ‘ I 3 ‘ ‘ . '. . . l n'.,‘ ' ‘ -' “NW“ ‘4.” ‘54. ‘ ’I':~‘.“" “ h; b‘r‘fi’i"”( “' . ' 1 ' l r' 1“ p g u ‘ b , ‘ 1": .' ~.OI. V. ‘0'“. \‘e I .I .‘. . J I i 3* We - -> .. .. l -- ., e‘x 1.. 7t "11?"; elf-1424"" .4, .. ,5 .; .- . H (3.“"t4'. D ‘ f. a. u #24 . . ER TY "'Wl’iifiu“\3\ftujlmg’miu [Mi 1“ MI“ wiflmfif“ 'i. I DAf‘A numbers remasen't. drops of? soup to lather o’w mo. Date "is 10 We 11: " 11%.? 121: ".‘m :1: ' he ‘1: ’ few: 2 a. . Item ‘79 l 5-,": £3 =,,-'= {-5 5": 4 3.": 5 . 1—21-38 1:) :2 355 i" .3 I. 3 W :34: fl : {I} J’oL {e (5 3 6:13 Pofiiefi} 5 3 «3 :80 L3 5 :3: ”130 1'7 :5 {2.01 o'- :-:,~) 3% :3 23 23") e :5 «J :3 :3 :5 U 2 ‘15 I ‘ ’9 3 9:15 7? i 3 23'? 9 3:30 :5 :32: 9 :r‘EO {‘3 2% {73:5 0 :50 IS 13:} ~‘E-13r11-I'3n l :05 7.31. 1 57' ‘1' 13:30 in; ‘5 12:50 :14) 15 «gnaw-:51: '7313 33.31. W " :5 a) S :31; '7 p1,? I3 3). 3:3 ’I :53 4“ 7:56 8 3 g {)1 1;: 13d: 8 x 0'7 1-3": *3 8 :10 ‘f.’ 2 n :19 :1 :5 13" 9 :51 15 9 :51) 6 10:10 10 10:13 1115 1034.0 ya ’1‘ (v No ’78 10:43:; ‘« f5 5'3 10:50 3' . W 11:00 11. : i113 4-m—m 25:12:: A .21. 8 :50 15 . {1:48 5 - 03M t .‘ e I 1.115 (II C‘ 9 3:54: - ’ " 1-):~4.". I a. e ' I P L1,:‘fg?g? ta) I.) 10:58 B I") ll :37 l-‘L 3 11:46 3 ll :49 {1 ‘. '9 :5 113:! 13.5 11:57 9 B 1 III WQ‘IEG 11:54: Aefle .. .__ Date 4n?5’)—-.’$fl ss-l—tmazx I ‘1316 11:59 Re. i. 3:05 11.31. 13:14 18:25:: 3:37 113:4;3 1:04 lzflfi 1:10 1:12 1:14 1:23 1:30 3.941 3:51 5:13 5:15; 3:921: wk:fu3 ., G ,1 p .1 I. ,. U "fi v" I! \. " 7‘ c ‘10 "gm-0‘ ww we d. .1. CM ell ‘flar-e CR In - A M :3 O ‘W ‘fd A IA . 3:? {a " w W \5 e e. 0.0. ee e. I. nee e. 00 ee .0 .0 L; "5'? I I a S ..o!§o Pefie C t '4 3x W “:19 0:138 ({3ng £350 921'? S) :50 S? :55 ,9 :40 l‘Jgtfl) 10-00 la 1.“. 8:16? 8:17 9:33 9 :48 Aefle DATA ( continued) 11 0' {5 '7 W12 If e) 15 Tank 1 --1 5) 0‘ ‘0‘ ‘7: 07 M W 4:5 7? ”301 ) H 0'. .L‘w Tank 7' ' v”! S e'IIe ‘ oh"' ‘r' 1!.) B 17 1t! 1:3 17-: 1}} Turn: Tani: Sta. . Raw 935 4: $33 5 5 P183 1t. Stop Plzmt Start 1212 Hunt Stop Plant Start ,5 130 3 :5 ‘35 e} 3 3 Plead; {stop Plant start I: S '7 55 3’1 £3311} Stop 3 ‘ -' l’Jmit 33 1’. 3 Plan 11: Start fl OJ Blant Stop W3 3.31.: mt Y , "‘3”- Placlt :iztart ;) Date ""1273 lOglfi 10:39 10:15:" 12:09 1.53: :3 ”rd li’:13€; 1.39171 113250 12:0 lzi‘d) 1:54: 8:54: {1:517 2')le 9:113 9:17 9 :12!) 9 Fr) 11.):02 10:13 23:10 {5:15; 9:315 0:15 9:11-20 0 :11”: :ISJ lflzhij 11:01 11:11 1121": 11:10 11:53” 1;: . )9 2.37.. 13-3—36 row-1 13.31. «ADEIO 130:1. 7. l WES '. x) 3m! 31A (continued) Flam}: "Rank '33.: 11:“.‘znrflzc Etta.- ital! ‘2." 53 :1" 5 i',‘ 4 ‘3’ n 13 3 3 1 as 30 S 5 5 25 Plant 511307;) 3 P5 5 5 1'5 3 9 P193112 Start 5 Plant Stop re 0 2; of brine to '7? 2 5 9 1e fl) ! "J 3 3 I5 1' 5 3 '1' :5 I") J’lzmt ‘; {I 3 0‘ v. 3 ‘ "r I‘ I5 {:5 2a: of brine 330 Plant Stop 3 Plant Start YB 33 8 Plant Still) W Phi-ll u 3 3 '5 . Start Date ' 7 5-13-15 6 '75: ‘28 11:39 1124-2 11:: a)”, 1.13 31.13 12:18 492135 423451 (1:15.14. N :55 '7 :Ufi V919 7:01; '7 1-1-1 '1’ :49 8:1)? 8:135 £5 Mat) 13 :-';.¢‘3 9 : 015 d : 135 9 :1515 1:48 1:147 ‘93“ “12:56 ..,35() “2255 533.53 '. . ‘N o" #0 4' ‘nJ An In ’3 V' V‘ ‘ "I 9‘ ; ‘3 “: t. \v ‘4‘ On. BJ V‘ 5v U- 0. o. .0 bl 00 0. 5. \'1 0H 1' .. JP. ‘1. y l .J D’“. Q I '0- ‘- g. - s. . 4“ s. J‘ . 1 ’ V r .. 0' 0- .0 .u o. .. R 3 ‘— ... '6 V. p U A 1. I M' DATA (omrbizmml) 2103!. 33.31. 130315 '7)" m . an}: ‘.' ‘ -L R 3'15 "’ i) 0s .- vhi v! r1, - 112.311; a” 2 03 “fr? H l) 33 it V. 0 1:3 Q..a (- ’5 Us Tank 5‘? 1:5 Ta.) 1‘- : 9% 4 4»! ‘ f.“ 5) Plant Stop .L’liu‘lt Start 28 5 3 Plain Start Brine dose out 131/2-181/4: 223 15 '5 15 1:13 3 Plant Stop {5 1 :3 {31:02) Plan-1t Plea: 1?. ‘= '13 Brine (Start 5 VS 1 h.) 1 '~. )1) 10 ) V qv L} yo I.) i) .. t) 3 Start. dose out to 3 i3; ; '1 ‘-‘ c7) '2': ‘2'?! $3.a|’%.)l~l J :1?) '.’ ‘CD ‘1 r‘tJ I? a) "2:3 1'. I“ - Yaw 1m. 110 6" Liz-:tra- brine tofia DN'A (oontimled. ) , 1 r n- .. Date ulno "wfl: "am: 'T‘unk Twit-c ”1:311: Sta. 15:93.: :.: 1 y : .) .. - l‘. .I’ ‘ . . " t ‘1 ‘ L) 3;", J}; 2"! 5 Yaw soap and droppiz‘m bottle 11:11-91 -:. 1-. I r \ r' on - ,V A ' f ,' ’\ ' " nah-0.16 . tb‘c no. to b 3. I) ,, 5 hf; 11,3, :3: l m 11f: tn U0 “:1-‘1 '33:: “:19 I}; T‘tr‘ino (10-30 «3111; to lb/‘L/H" . t -' I ’ '. o . " 8 .0- ‘ .- 1 start Wl'th 9’: A: 1 21‘s.? 1’ o' 1. JJlEL'JTt» :n‘mvt. l :55 1:3 3 :3 : Us.) 5 ,b, 1-: : -‘ l's' "£13 5 5 ’5 «L 1 .S 1: :14 7‘! 1'5 :3 :1 .9 It: 3 :1 2: 51 t l! "'t.‘ :2 x 1'7 ("s .- ’Lau 1t 3‘» .013 :/:() ) ‘; "4' 3 2-1)": 1-1 3 5 :1 ) :3": .‘1 :31} {3 5 :a :1517 :s 1115 R :51 Blunt Start a 3: "5 “1 3‘. :5 '.-’:1.1’. 5 5 5 '1’ :11.“ 3 ii": '1 :35 V15 'f 311:1 i 1 3 5 B 3 54-156 U :54, A .j‘ {. :5 1 1/15 15 15 :56 53 : '18 l’ o." I. 3 I '2’1’3 13.1.: mt Strap s; g u". S s» :20 "'3 v 9 z 1?? 3 '3 {3.4; 9 :1 11’ “S 5 0 :3: .1 5 1'3 _ 9 . 1;“ 5 W15 £111.? It 5130,) .- S—tH-Sfl ’2' :15 A .. i. 1": 3 3 '1 1-1.“ W 0: 3U :1 n :35 ”I i ‘ '7 ~34, 5 33 ‘3“! {1:113 3 r ' '3' {1; 0M» :3 I": 3 L) A ’ 7‘ 1 rr' 8 :533 «’1 9 1:35 {5 9111.311; 3‘00}? 3 l) 135 11:54.. 3 ' =5 11:40 1’» _ 11:58 15 Plant Stop Date :1-9-: 36 5-10—75: : 5-11-33"? r1 1: .10 3:53 5:02: 5:15 5:17 5’» :20 5::15 5:40 5:60 6:53 6:47 6:55 (.3359 7:07 7:20 7:63 8:023 7:56 8:04, 8:27 8:39 8:59 4:02 4:1!“ 7:13. 9:10 9:11 9:3 9:133 53 :37 :2 J 2* :0? m1?» 1‘» :55 7:00 7:07 7:17 7:18 7:57 7:55 was 8:13. 8:56 8:59 1320-1: 12:09 lm’l‘f: ( 0031155.? 11 led. ) '3th ijthk '."fl‘nJC "0.311: ' ‘guflc ,ta . :. {aw 5’ 1 :3 3 32": 3 y": 4, :4: 5 i941: it: :5 3 'f ; «.- 8 4 U13 {3 f‘» 5 R {S Pltmt Stag: :; 3 913.2% Start a '5 3 3 9'5 5 I: R 15 :4 '5 ‘.2‘25 AoEio Elm-1t Start 13 3 it 3 :‘3 3 $71.5 P010 3 1'). :‘3 3 3 311‘in (3.088 P. 1.51/4" to as;- :5 "1’3 P182113 Stop Adi. K5 3 55 1‘5 5 1325 113 V5 33 3: 3 .1." .2 (o 3 5 I3 ' S 2 5; Z'h'ino done out. to :6 a 1419/16" starting With an; ’ $3.1 :; 3 3 I‘: 5 f5 {'5 1335 {i ‘15 :53 Plant Stop .3. .3 1 ol’. 1 3 1'5 {‘5 1335 S I Brine m1]: filled. up 1 L" too ‘2"? 1&111 after a”! 1. 1'3 R :5 a, W? Po: it Plflfil‘t htart 3 3 I5 5 3 13.“ 11/1 DATA (oaé'l‘timed ) Date "71:19 "jun: 'jmfl: '.kuflc ’Ifaau: ""mfl: Etta. 21:21.: ‘1‘" 1 ‘3‘“ 2 W 5 "‘1' ‘5‘: 5 3' 3': in 1451/3" 01’ 19913:; 31 w '0 .ge‘: l: )1: ; grins to, 4- 1306 :_ ' I; 13.1.?) ‘15 5 3:11 J’lmxt Bum 5:153 ES 3 5 {'3 Sum 51 :5 13:35 5 :3 ffixfiri U3 5:50 Plant tit-art. 5:535 25 'f 13 {6 3 5:51: :35 " °-' ” 13:5 7:33 1’me Start 'rz-«L-ss f5 11g;.~’zs“ brine to .52 4 7:50 3 R 8:31 i”) 3 8 24:0 53 133/; 1..“ M1310 9:01 Plant Gtop to .71': 5 i ~113-'3-" “:30 Adi. 1’lm1+{3tt,zu't 63:32. :5 S 5 may 7 5;; 8:45 Wt: , 138353 :3 is 14:" or? hams to i” :5 VB ..':.:5 :3 :3 '13:» '7' 15 "#32 lflzmt Etc? 15 {5/4" of brine to u’: 4 9:33? '5 IS .5 :5 9:‘ 13.. V3 9:37 13 151,2” of 103419 1’1:me Start brine 13:05 V3 11212.: B 1 “ of brine 11:5 11:7“ :3 film .3109 1:435 11.3.. :- 3 3 r; 2.; Brig. 301'. at 14 1/-”to start With '~,-= 2w 3: y, :3 Pump $30}? {2:30 15 Plant Stop 13131211; hurt. :: :5 DIVA (oocn'tirmad) Date Time 'i‘mfi: Wm]: Wm}: Tam}: T2373: Sta. Raw 531. 3'3 54:5 :54: 3'5 634.553 '7 6:53 5 7:00 3 ".11 W? 07:1)1 B U :40 13 9:00 It 930'? Plant :‘top r—13—31 7:147AJI- 3 :5 7:25 3573 3.50391 :8 1.3" of brine to 599 S {A Brine tank 6 1/8” too '7::5:'. 7:41 8:02 8 : OH 0:34 8:33 10 :34: 10:43 10:53 12:41:.) 1:331": 13:80 12:30 lxzéfi 3:03 3:10 3:15 5:15 5:84 5:1' 33:40 6:67 7:05 7:18 7:13!) 6 7::513 7:38 11 2'17 1:00 1:15 :51 N 0031 Po”. 8 3;: 1/2" A 03 '1 o 3.2!. after 55 3 R 13" of brine ta 5% S I; 3 .‘i '5 ‘."3 mflt utOP 3 Urine dose act at 13 1/3“ starts With 5" l 3 Plant Start 0,) 1..) 6 {is : it.) 4: Y V15 Plant Start :73 n 12 1/2" of brine to I: 3'4 l’hmt Start '7 :5 m W13 23 of brine to 9% :5 B 7:5 2 1/2" too nuch.br1ne in tank after 5!: 4, B 153 1/2" of highs to 7,“! 5 P1513113 51:09 I: :5 g: r0 :3 Date 5‘15“; J ' “inc 1:31; l:é8 2:43 13:55.5 417:!)1 «ErX) '"1 :15 é:35 434:0 5:J3 3:07 5"» :1'7' r- I)?" .1 {on} F5 :85 (1:36 {‘5 :(3'3 (1:63;: 8 :04, 9:54 10:15 10:3 10 :13: '. 10:51 10:57 11:13 11:13:; 11:3 11:51.3 12:01: 1:13:35) ru— 2 :-J.’? 313:131 12:52 10 3 14: 10:33 10 :33; 10:40 11:3fl 11:55:12 11:36 13:36 15-3 15"} 11.3% '1‘: m}: ~:: [.4 Ca": {.1 1‘ "..~ i 3 5 Plant liunfi; Plant 1 ’18.: Th "1'3 P. (Q 5‘) I { . r? 77, I) T?“ Stop fitm‘t Sta? Star-t til :4 FR yd 2:1 in? "A (continued) Sta. Raw Tan}: “Paul: I ‘1'” 4! 7” 5 ‘Hfl; .‘7 15313 I: 3" of brine to -,= 4 S 8 {’5 '5 ‘53 B 12' of brine 11 to :f'f: 5 1/11" of brine to --.,*= :5 {‘5 3 ‘33 B 113' of brine to J. 4- 3 n) 3 1". W6 3 2" of brine R to 5&5 ."1 I 4: 7:73 4 534: 108' 13 13" of brine to 5?}: 4 Stop Start Plant Plant. 8 12' of brine tosfi's DA'M (continued) Date 7‘in Wm}: Tan}: Tank Tank mek Esta. Paw ‘5 '3 l 5")"; :3 5&5 5 9'5 4: it?" 5 ’- lgt‘fi‘fl: 13-“. R Plant Stop u :09 D Brine dose moanumdnlfi 5/8' :1st]. R 3 3 5 5 2/2: 1113 381?} S S 3:":3 1'13 5:50 B 4:20]. H mm :5 Plant Stop {3:58 W?) 5:46 B 5::28 :1 1:3" of brine to 4 :54 5 fi-lG—{SG 7:08 Ac“. 3: 3.3.1:. of 5-15-36 . 7:27 3 4, ‘ 7:34 3 4: 734,5 Wt": 73595 B 113" of? brine to vi. (3300 R 8:05 l’lmt Stop 9:01 3 S 5 S 3 9:31 174. 9:41 p B 11 1/2" of In 9,4,3 0 R brine to 5’53 5 10:13 5 i3 10:21 vs {Built (1033 sot at 13* start with a}: 1 10:38 Plant Stop 11 1/2" of brine to 7:3 4: 22:31; P.3I- I: 532117 Plant Stop 3:4" 8 3 43:18 1'95 4’33 B 11 1/8" of mm It brim to 5 6:427 Plant Stop 8:3?» 8 08:45 Plant Stop 4, 1‘1 1/9,» “wine-2 to 5-17-38 1:16 Julio l’lmt Start a»: 4, d: 5+ PM. . 1353 A3: I. 13 5.16-3.1 9:35 53 4: 9:335 UL}: 10:05 13 11 1/2” brine to 9% 4 10:11 22 103115 Lg’lunt Stay 11:19 4, 11:31 W4: 11" of brine 11:41 E to a»? 5‘» beta 5~18~I 3. ‘u Tine ll :94; 1:3 : ()5; 1:: :53 11-3 :35 111% :63 113 VA- :3 :15} 2:23 13:82:? £3 :37 H :I‘e'c; :3:“‘::':) 13:59 (3:3K5 5:19 5 :‘ 36) f3 :34: 5:13“ 7:10 '7 3‘3!) 33:5,: 1,230 1 1:11. 11:02) 1:: :131, 13'317)..' 19.)) :31. 1242.1 :3“? lg-ttfi “:50 0 2:3.) E‘fii‘fi {33%) ‘tH‘h'J DJ": .‘A ( 003141111100.) ’1 1sz I ma! qflszll: -)i)t1.. an" 5 '1'3I' :5 H flaunt Stop in 3.6 14' 54: :3}: W? ”:2 5 5/1" of brine to =33 2 [)K' m) Brine dose set at 14:" B etuz't With in”: 15 Plant 5130;) :5 3 W4, 13 11" R Plant Stop 1'34, B 11" of brine to 5}": 5 .f ' to ‘,_r‘ ‘1: Plant :A't'art S 4 We 11" of brine ta '55 4 a: :3 Am. Plant ‘i-toz) of 5—18-66 1103(- B 10 1/: 2" 0:2? brine R to 5 Plan‘s 1' 113029 f‘ B 6 I7 :9 JF‘ DAfi‘A 'i‘em‘. 121;; value of re covery brine Date ”inc ’.‘zml: "am; ”£312: '.i'cum Tim}: Sta. mm D '- O.‘ “ fr!“ 'L' ~10 ’0 0‘ I. l t 3 ‘J 0‘!“ ‘) l, o 4 if,“ 5 5—19—38 :"0 2%.?2. :5 3 3 as 5 :35 mm brine :15 Hz; only-.13" :34 ‘7 Recover-y brine on 1 J 55:35:13 5-5.30-3 36 W bHfiGv Z: ‘3 .O 3‘ :f‘lf) ‘7! :"10 '5! ":5 ) '3! Eli‘uz‘d P» {if} " 1; H 33' 1:: ()4) Noon ‘3' 7‘01! brine 0:71;; 1:3 53:: 330:!{0 3793 81383.1.- Witgl $73 ‘1 1 {.2 V3101: 1:3 1 -I.-” brizo 3 £53 '«3' . .. ‘4: fi‘ ":3:‘I “.1513 ‘3' 14 1/4" brine set to start with {:9 1 a W 43') «.5 o. .0 0. no 5. no .0 on ”on I. O. CO 0. o. to 00 .0 a... no 00“.. 00 M w J‘. :15 H a O CO . f." "I" 1‘) {3:3 L. . DJ :2 l 53" I! ."---:.Jl-{SG {i {34: AQZ. W 4' n .2. 0.) W5 15 1/8" brine, mart ~ 9 9:5 US 7" 1‘-) :37 u " ll :55.) 'w' 1131253 -"I. V l 55:; I“! 4, 15 '.‘f . 331'. {)6 ‘2! 6 4-1 I! l" K ) " 0 1):; " lO:* "3 W ‘1 ll 2 7M: . . i. :7 5-23—56 1.13202 A-.u .. 1:1’7 ‘53 13:18 v , '7 : 03' Y! 31000?on brine start i7 4: :3 : '14. :3 :3 {-3 “=15 T3 :- Q:()(‘ If I” My?) 142:}. ‘395 8 a .> 3 LN.“ ( cos-Itizmed) Eiwate "inc 'T'azfl: "11.333: '.‘faa'flz Tank ”wit: Sta. . Elam ‘3” l 5:": 2 9.3 3 55' 4: =25 5 Brine 14, 1M: . atcmt 5.2!: 1 ll :37 ‘ ’95”: 11:12 13:31" PM. '3' :35 :5 :3 :5 £90 Trev: brine only : :5: 3 {'3 3 IS ""18 atm‘t 1i? 3 6: :2'5' ‘39:”: 18 I5 3 3 .3 s. 24:: 1-795 (:0 (3:13: W '7 :59 W 9 : .1 3'! 10:10 ‘53 ll :10 1;! r:-:1:5-—: m 2 : Us.) A . . Y! 1 2:35 W 3 :v‘i-O 3 3 I5 {3 '5'3 '7 :53 ‘5? L5 : {30 ‘3! 9 :48 5 \1'3 :3 3 :35 l" l : :15 W 11 :5 «‘3 U 13“}! l 3 0".) P 01:. ‘7 : {39 I? :3 :49 S {3 :56 4 : <15; 11' .‘3 3 (M W 1‘. 3:3: '1' x. '7 :i it; ‘3 Q U! {’5 3 234» 13.23 63c: s9 13 a I! (I: T! ‘7 “R: w ‘\ K“! ‘5' 1‘30?!“ ‘7 A rat-JP ir‘ u‘ld (.393 -".~ ‘0! A! ‘ lounoauaauoa” :1 [Hg 5)} w J n l' : h' t 5“..’:’1.‘";)f7 H . CL 6 3: J‘. Pq F x: it‘d ,4- ._m 1 c: L: 1mm 13.22. ‘7 1:563 3:02. W 4:18 ‘7 {5 :15 ‘ mm (0021111311106. ) 1 "4- w v - ‘ . » . Date Vino 3.31:: ”m "n ”9311: "3311: ”33111: I 3133.. Raw ' 'u 4' ' '3' 5' 1 at 33 5*.“ c 5"" 4 5 ~91 {3 :4”: W 7 24:6 '17 {s :58 W 10 g ’. )H W 11 1 ’35 W 5-. :rI-‘IST": "1: :36 A .310 3‘7 5 :i :6 tr; (3 :38 ‘.‘I 9 z '11.“; :35 9 : 15 B 9 :23 13 {3 ‘.Z'fill'i I} 3 5}".- ll: ; 1 ’J :2: i ‘v '13 11 :zm ‘23 mast. 4: l}; :36 ‘ Y! 1:34: Y! :3 : 15:3 1‘? GILT TB; J'TI'YY OF (‘0. L3 S(')LU"31033 Hanknoas of It’atez‘ Drops of $03.1: 1533 in p .1) 0331 , lfi‘OdUOG 8. 149415116? :3,“ 1‘1 I i I 2 0 18 .1 {'55 8 “ {:0 13 ‘3 s (if) ; 31:33 : NO 24 3 fig; 23 \ (:4) 1-38 65 5 l '70 54‘ 80 {‘58 fl 9 O ‘”:33 1".) ) 4.5:; 110 50 115 54: 1:30 5,3 1;;5 ‘ (:2 (mo diffm dropping bottles were used. (twins: this experimental work on The East. ersin? Water ”111.311: . me abate oalimtim was made with the first bottle (1)- Battle (1) rum drops a: 7.9 ml 58 drops =3 1.0 ml. Battle (:3) 5%.- ch‘opa n 10.0 ml» 33.55 drops :- 1.0 ml. 4.21) 0.0,. of Water Wore used. in tho calibration. CONCLUSIONS From the results of the work done in performance of this thesis, it has been concluded that the claims made by the Permutito Company for the value of the recovery brine equipment are based on the chemical analysis of the recovery brine end not on actual tests of its regenerating power, for it he! been found to have a detrimental effect instead of a practical value. The flow of water, as calculated, has compared quite favorably with the amounts of salt brine found necessary to use in the Various softening tanks, except for the indicated difference in flow of tank number four over tank number five. This difference was probably caused by some unseen obstruc— tion causing excess friction in number five. The smaller flow of water going through tanks number four and five could be remedied by installing equipment to cause less head loss in the flow of water through those tanks. It is suggested that the effluent pipe from those tanks, marked K0' in the flow diagram, be made a 6 inch pipe instead of the 4 inch which is in place at present. If HI were made a 6 inch oipe, and the first ell and two sec— tions of pipe of lines IJ and IL were made 5 inch, the flow should be evenly divided among the softening tanks. A further refinement could be made by a slight adjust- "nent of the time sequence switch. W_ 0%. , " "i b' ' -- ' " ,"g'g » ..' >. I, -' J". . v _. K“ ”i, ‘6": 1 ‘ rife-2': . ‘3. ,’ J fie... (:1 ‘ \ V . 7* .I' \- tJ‘a .s . -- ‘5 I . 1 ‘Yt‘J‘. ‘ I u . \ . T ’ 5“ 7. '. u v~ ' ‘ " ”r ‘c v . _. \1‘ 'l' I . ‘. . -"'i" I .1 1.... .' ‘-I ‘ ".L 'I “V” ‘5 ' ' ‘ . .o.‘.w-’.,'.'_» at . . 'J r\‘ I"\.' -v . I . -' w . \‘J' ‘0.-‘ r‘.'1_-V ““259. “.g' , ‘ ’ -. a; itffivf .. ' s‘ r m;- ‘z ,I .I _.'_<~ .Q‘il‘1’);.- :3 . 34:, 3"}. ' af‘.k?>§a.’ . I ‘z A »,~' h "1‘: Umfi‘ ‘5‘ "' z -- ‘- "t ‘.‘ ‘ ./.'~' 19.3391". 33-6.? .‘ A ‘ . I. -,) -\ . .. . k) “I! ”3;,“ i | v. .v‘ . I, ‘0. 3“ . . . _ ' '.,\. f). {ft'r‘f'l ”If . 3'.: ‘~_., (._‘J: ‘ - I . l . ‘1 '_"s, A "I \. .‘y y 1.3.: . > A "Q fidu, " ' .le' , ‘ .i “I ._ - 3‘."). _; . - . v. '.w‘.‘..‘%- e .. I..." ”w” l. \ 4. 1+ ~.-‘ m 5-,. .. ‘.xnf}. .",“ 3..) V. ' .4» a» » I ' .‘é."l..é.' '. . "'1 _ ' 1 ,‘ , .I t g '. ” o .R.» J - Him -. gnu... I‘ ' _-'-. jrrfiflo 9,: £1"... . ' E". $ 1 , ‘. ., ‘ "3. u , . '_‘ q“'.1 1 w ‘ ‘ ‘ "J “ . . ' '.'"‘-Jix".u q ‘Lu‘r )‘g ‘ . J'. -" v. ‘ - -.- - ‘." -. * . 'J . ‘ ‘ . v . ’-»,‘.'|_’_‘ . ‘, l '. .1 I . ‘ . ~ « ' ,. . , ~ v H a b .l .1“ v J ' I ' \'. v) '.' n '. ._ ' . « ‘V‘ ' '1 - t‘ t v ) ' K I “ 6 2 0 7 7 7 1 3 o 3 9 2 1 3 Illl I'll I‘ll || || I'll. I'll. IIIII l|||| I.Ill'l |I||| Il'l II III | l l Ill Ill III |||I I|||| III‘ ‘I'. II' Illl || I. ll I'll ||| ll II‘II |||||| || || I'll Ill I'll | ‘I