A .. , It... , .r .. rwnyflffim _.‘?§ :14}? ”9.4%“ . Fbwfi . 1N .. ha: drain .. .. ll“ ifimrgfiwa 253., .5... hasvduéfla .. u¢ . .W r. . Ptiflih 1!... {2.3.2. ifiww an." .7. u.‘ v5.3.3.1... I... .: 11...... p 5.0....Hurfl . gm LIBRARY” 2007 MIChIQsfl State University This is to certify that the dissertation entitled EVALUATION OF PORTLAND CEMENT CONCRETE COEFFICIENT OF THERMAL EXPANSION TEST PROTOCOL AND THE IMPACT OF CTE ON PERFORMANCE OF JOINTED CONCRETE PAVEMENTS presented by SHERVIN JAHANGIRNEJAD has been accepted towards fulfillment of the requirements for the PhD. degree in Civil Engineering ”Major Professor’s Signature 6 I 14 I 197 I l I Date MSU is an Affirmative Action/Equal Opportunity Employer PLACE IN RETURN BOX to remove this checkout from your record. TO AVOID FINES return on or before date due. MAY BE RECALLED with earlier due date if requested. DATE DUE DATE DUE DATE DUE 5/08 KglProleccsPresIClRC/Daleoue.indd EVALUATION OF PORTLAND CEMENT CONCRETE COEFFICIENT OF THERMAL EXPANSION TEST PROTOCOL AND THE IMPACT OF CTE ON PERFORMANCE OF JOINTED CONCRETE PAVEMENTS By Shervin J ahangirnej ad A DISSERTATION Submitted to Michigan State University in partial fulfillment of the requirements for the degree of DOCTOR OF PHILOSOPHY Civil Engineering 2009 ABSTRACT EVALUATION OF PORTLAND CEMENT CONCRETE COEFFICIENT OF THERMAL EXPANSION TEST PROTOCOL AND THE IMPACT OF CTE ON PERFORMANCE OF J OINTED CONCRETE PAVEMENTS By Shervin J ahangirnej ad A number of factors affect the magnitude of Portland Cement Concrete (PCC) coefficient of thermal expansion (CTE). The selected factors in this study were aggregate geology, age of the specimens, and the number of heating-cooling cycles applied to the test specimens. The effects of these variables on the measurement of CTE and the practical implications of the variables on the performance of jointed concrete pavements were investigated in this study. A laboratory investigation was conducted to determine the CTE of typical concrete paving mixtures made with coarse aggregate from eight different sources in Michigan. The primary aggregate class included limestone, dolomite, slag, gravel, and trap rock. Three replicate test specimens were fabricated for each mixture-age combination. Over 700 specimens were fabricated to characterize the mechanical properties and CTE of the concrete specimens. The test specimens were moist-cured for 3,7, 14, 28, 90, 180, and 365 days prior to testing. Mechanical properties tests including compressive strength, flexural strength, splitting tensile strength, and elastic modulus tests were conducted to check the quality and specification conformance of the concrete mixtures. The CTE was determined using two test methods; the provisional AASHTO TP60 protocol and a revised method based on the TP60 protocol. The measured average 28-day CTE values ranged from 4.51 to 5.92 us/°F (8.11 to 10.65 us/°C). Statistical analyses were employed to evaluate the significance of the factors affecting CTE magnitude. These analyses included analysis of variance (ANOVA), which was performed using factorial treatment design and mixed effects models. The results of these analyses indicated that aggregate geology, specimen age at the time of testing, and the number of heating-cooling cycles that the Specimen is subjected to, have a statistically significant impact on the magnitude of measured CTE. Sensitivity analyses were conducted to investigate the practical impact of CTE and other variables on short-term (first 72-hours) and long-term performance of jointed concrete pavements using HIPERPAV II and M-E PDG software, respectively. The impact of FCC CTE among other pavement design variables (slab thickness, joint spacing, etc.) on pavement design and performance was investigated. The long-term impacts of the factors that were analyzed statistically are also discussed in this dissertation. Recommendations are made to improve testing of the CTE based on the results of all analyses and suggested CTE values for agency use in Michigan were presented. Com/right by SHERVIN JAHANGIRNEJAD 2009 Dedicated to my family specially to my wzfe ACKNOWLEDGEMENTS I would like to express my deepest gratitude to my advisor Dr. Neeraj Buch, for the Opportunity to work on this project and for his guidance and advice during the course of my Ph.D. studies. I wish to thank Dr. Parviz Soroushian and Dr. Karim Chatti for their advice and comments during this study. Special thanks to Dr. Alexandra Kravchenko for helping me and advising me every step of the way on statistical analyses. I would like to thank Mr. Siavosh Ravanbakhsh for his unconditional support, cooperation, and kindness. I owe my laboratory testing experience to his instructions. I would like to acknowledge the financial support provided by the Michigan Department of Transportation for this project. Finally, I would like to express my gratitude to my family and specially to my wife who understood me, supported me, and made sacrifices during the term of my studies. vi. TABLE OF CONTENTS LIST OF TABLES ix LIST OF FIGURES xii CHAPTER 1 INTRODUCTION 1 1.1 Introduction 1 1.2 Problem Statement 5 1.3 Research Objectives and Plan 6 1.3.1 Research Objectives 6 1.3.2 Research Plan 6 1.4 Dissertation Organization 7 CHAPTER 2 Literature Review 8 2.1 Introduction 8 2.2 Literature on Micro-scale CTE Mechanisms in PCC 9 2.3 Literature on Variables Affecting CTE Value 15 2.4 Literature on CTE Impact on Pavement Performance 28 2.5 Application of the Reviewed Literature to the Research Plan 44 CHAPTER 3 EXPERIMENTAL PROGRAM 46 3.1 Introduction 46 3.2 Materials 47 3.2.1. Aggregates 47 3.2.2. Concrete 51 3.3 Concrete Properties Tests 53 3.4 Thermal Property Test (CTE Test) 55 3.4.1 Controlled Temperature Water Bath 55 3.4.2 Data Acquisition System 57 3.4.3 Linear Variable Differential Transformer (LVDT) 57 3.4.4 Rigid Support Frame 59 3.4.4.1 Frame Apparatus 59 3.4.4.2 Frame Calibration 60 3.4.5 Test Procedures, Data Collection, and CTE Calculations 61 3.4.5.1 Specimen Conditioning 61 3.4.5.2 AASHTO TP60 Test Procedure, Data Collection, and CTE Calculation 61 3.4.5.3 Revised TP60 Test Procedure, Data Collection, and CTE Calculation 63 3.4.5.4 Executed Test Procedure 64 vii ’; CHAPTER 4 RESULTS AND DISCUSSION 67 4.1 Introduction 67 4.2 Physical Properties of Coarse Aggregates 68 4.3 Fresh Concrete Properties 69 4.4 Hardened Concrete Properties 70 4.5 Thermal Property 73 4.6 CTE Test Variability 80 4.7 Statistical Analyses 81 4.7.1 Statistical Analysis of Factors Affecting CTE of PCC 81 4.7.1.1 Aggregate Type Effect 87 4.7.1.2 Sample Age Effect 88 4.7.1.3 Number of Heating-Cooling Cycles Effect 90 4.7.2 Comparison of AASHTO TP60 and Revised TP60 Methods 92 4.8 Impact of CTE on Performance of Jointed Concrete Pavements 96 4.8.1 Short-Term Effects Analysis 97 4.8.2 Long-Term Effects Analysis 101 4.8.2.1 Effect of CTE Variability on JPCP Performance 101 4.8.2.2 Effect of Coarse Aggregate Type on JPCP Performance ------------- 104 4.8.2.3 Effect of CTE at Different Ages on JPCP Performance ------------- 106 4.8.2.4 Effect of Number of Cycles on JPCP Performance 109 4.8.2.5 Effect of CTE among Other Design Features on JPCP Performance113 CHAPTER 5 SUMMARY, CONCLUSIONS, RECOMMENDATIONS, AND FUTURE RESEARCH NEEDS 115 5.1 Introduction 115 5.2 Summary of the Performed Work 116 5.3 Factors Affecting Measurement of CTE and Impact of CTE on Pavement Performance 1 17 5.3.1 Factors Affecting Measurement of CTE 117 5.3.2 Impact of the CTE on Pavement Performance 118 5.4 Recommendations 119 5.4.1 CTE Testing Recommendations 119 5.4.2 Recommended CTE Values for Agency Use in Michigan 119 5.5 Future Research Needs 121 APPENDICES APPENDIX A. HARDENED CONCRETE PROPERTIES DATA 123 APPENDIX B. COEFFICIENT OF THERMAL EXPANSION DATA 132 REFERENCES 142 viii LIST OF TABLES Table 1-1. Influence of CTE on Pavement Performance Table 2-1. Mean, Maximum, and Minimum CTE at Different Sites Table 2-2. Predicted Distresses for Computed and Measured PCC CTE Values for Typical Aggregates in Kansas Table 3-1. Coarse Aggregate Types and Source Names Table 3-2. Mineralogical and Physical Properties of the Coarse Aggregate ............. Table 3-3. Petrographic Composition of Slag and Gravel Aggregates Table 3-4. Chemical Composition of Gabbro Aggregate Table 3-5. Concrete Mixture Designs Table 3-6. Summary of Material Characterization Tests Table 4-1. Physical Properties of Coarse Aggregates Table 4-2. Fresh Concrete Properties Table 4.3 Average 28-day CTE Results Table 44. Typical CTE Ranges for Common Components and Concrete Table 4-5. Physical Properties of the FHWA Coarse Aggregates Table 4-6. CTE Test Results for F HWA Specimens Table 4-7. Factorial Design Table Table 4-8. Description of Terms in the Mixed Effects Model Table 4-9. Tests of Fixed Effects Table 4-10. Factorial Design Table Table 4-11. Description of Terms in the Model for Method Comparison Table 4-12. Tests of Fixed Effects for Method Comparison ix 23 43 47 49 50 50 51 54 68 69 74 74 79 79 82 83 87 93 94 95 Table 4-13. Input Variables for HIPERPAV II Sensitivity Analysis 98 Table 4—14. Examples of HIPERPAV II Sensitivity Analysis Inputs 99 Table 4-15. Examples of HIPERPAV II Sensitivity Analysis Results 99 Table 4—16. Input Variables for M-E PDG Sensitivity Analyses 102 Table 4-17. Percent Slabs Cracked for Mixtures with Different Aggregates ------------- 105 Table 4-18. Percent Slabs Cracked Based on CTE Values for Different Ages ----------- 107 Table 4-19. Performance Criteria for Rigid Pavements 109 Table 4-20. Percent Slabs Cracked Based on CTE Values for Different Cycles --------- 110 Table 4-21. Variables for Designs with Maximum Percent Slabs Cracked 113 Table 5-1. Recommended CTE Values for Concrete Made With Different Coarse Aggregate Used In Michigan 120 Table A-1. Hardened Concrete Properties Table for CTE 1 Mixture 124 Table A-2. Hardened Concrete Properties Table for CTE 2 Mixture 125 Table A-3. Hardened Concrete Properties Table for CTE 3 Mixture 126 Table A-4. Hardened Concrete Properties Table for CTE 4 Mixture 127 Table A-5. Hardened Concrete Properties Table for CTE 5 Mixture 128 Table A-6. Hardened Concrete Properties Table for CTE 6 Mixture 129 Table A-7. Hardened Concrete Properties Table for CTE 7 Mixture 130 Table A-8. Hardened Concrete Properties Table for CTE 8 Mixture 131 Table B-1. CTE Values for CTE 1 Mixture 133 Table B-2. CTE Values for CTE 2 Mixture 134 Table B-3. CTE Values for CTE 3 Mixture 135 Table B-4. CTE Values for CTE 4 Mixture 136 Table B-5. CTE Values for CTE 5 Mixture 137 Table B-6. CTE Values for CTE 6 Mixture 138 Table B-7. CTE Values for CTE 7 Mixture 139 Table B-8. CTE Values for CTE 8 Mixture 140 xi LIST OF FIGURES Figure 2-1. Estimated Typical Response to a Step Input of Temperature for the Three Different Components of Thermal Dilatation, at Various Humidities h 12 Figure 2-2. Dilatation of Solid Microstructure Induced by Relaxation with Increasing Temperature 12 Figure 2-3. Family of Thermal Dilatation Curves for Various Humidities 13 Figure 24. Variation of CTE over Time 17 Figure 2-5. Effect of Coarse Aggregate Volume in Concrete on CTE 18 Figure 2-6. Variation of CTE From 32 Aggregate Sources in Texas 19 Figure 2-7. Effect of Repeated Thermal Cycles on CTE, (a) Increase in R2, (b) Decrease in CTE 20 Figure 2-8. Effect of Saturation on CTE on Two Oven-Dried Cores 22 Figure 2-9. CTE Variability at High Saturation Levels 23 Figure 2-10. CTE of Concrete Made with Gravel, Quartzite, Granite, Diabase, or Basalt 25 Figure 2-11. CTE of Concrete Made with Dolomite and Different Cementitious Materials 25 Figure 2-12. Histogram of the Mean CTE of the Specimens 27 Figure 2-13. Histogram of the OCTE 27 Figure 2-14. Effect of PCC CTE and its Variability on the M-E PDG Predicted --------- 30 Percent Slabs 30 Figure 2-15. Effect of CTE and its Variability on the M-E PDG Predicted Mean Joint Faulting 30 Figure 2-16. Effect of CTE and its variability on the M-E PDG predicted IRI ----------- 31 xii Figure 2-17. Difference in the Predicted Percent Slabs Cracked as a Result of the dCTE 32 Figure 2-18. Difference in the Predicted Faulting as a Result of the dCTE ---------------- 33 Figure 2-19. Difference in the Predicted IRI as a Result of the dCTE 34 Figure 2-20. Effect of Constituent Properties on Pavement Performance Predictions --- 35 Figure 2-21. Examples of FSC, TSC, and CC 37 Figure 2-22. Comparison of Ratio of Cracked Slabs for Pavements with High and Low CTE (F SC and TSC) 38 Figure 2-23. Comparison of Ratio of Cracked Slabs for Pavements with High and Low CTE (FSC+TSC and CC) 39 Figure 2—24. Calculated and Measured PCC CTE Values (x 10'6/°F) for Kansas -------- 41 Figure 2-25. Calculated and Measured PCC CTE Values (x 10'6/°F) for Iowa ----------- 41 Figure 2-26. Calculated and Measured PCC CTE Values (x 10'6/°F) for Missouri ------ 42 Figure 3-1. Locations of the Aggregate Sources 48 Figure 3—2. Schematic of the Test Setup 55 Figure 3-3. Complete Test Setup 56 Figure 3-4. Controlled Temperature Water Bath 56 Figure 3-5. Data Acquisition System 57 Figure 3-6. DaqViewTM Software Channel Setup Screen 58 Figure 3-7. Spring-Loaded LVDTS 58 Figure 3-8. Rigid Support Frame 59 Figure 3-9. Side View (Left) and Plan View (Right) of the Rigid Support Frame -------- 60 Figure 3-10. A Typical Revised TP60 Method Graph 64 Figure 3-11. Three Typical Heating-Cooling Cycles 65 Figure 3-12. A Typical Concrete and Water Temperature Graph 66 xiii Figure 4-1. Average 28-day Compressive Strength Values 71 Figure 4-2. Average 28-day F lexural Strength Values 71 Figure 4-3. Average 28-day Elastic Modulus Values 72 Figure 4-4. Average 28-day Split Tensile Values 72 Figure 4.5 Average 28-day CTE Results 73 Figure 4-6. CTE 1 (Limestone Concrete) Coefficient of Thermal Expansion ------------- 75 Figure 4-7. CTE 2 (Gravel Concrete) Coefficient of Thermal Expansion 75 Figure 4-8. CTE 3 (Dolomitic Limestone Concrete) Coefficient of Thermal Expansion 76 Figure 4-9. CTE 4 (Slag Concrete) Coefficient of Thermal Expansion 76 Figure 4-10. CTE 5 (Dolomite Concrete) Coefficient of Thermal Expansion ------------- 77 Figure 4-11. CTE 6 (Gabbro or Trap Rock Concrete) Coefficient of Thermal Expansion 77 Figure 4-12. CTE 7 (Dolomite Concrete) Coefficient of Thermal Expansion ------------- 78 Figure 4-13. CTE 8 (Dolomite Concrete) Coefficient of Thermal Expansion ------------- 78 Figure 4-14. Variability Histogram 80 Figure 4-15. Histogram of the Residuals 85 Figure 4-16. Normal Probability Plot of the Residuals 85 Figure 4-17. Side-By—Side Box Plots of the Residuals for Age Factor 86 Figure 4-18. Average CTE for Various Aggregates as a Function of Test Specimen Age Based on 3 Replicates 89 Figure 4-19. Average CTE for Various Aggregates as a Function of Number of Cycles Based on 3 Replicates 91 Figure 4-20. HIPERPAV 11 Performance for CTE 1 Designs 100 Figure 4-21. HIPERPAV II Performance for CTE 8 Designs 100 Figure 4-22. Percent Slabs Cracked for CTE Test Variability 104 xiv Figure 4-23. Percent Slabs Cracked for Mixtures with Different Aggregates ------------ 105 Figure 4-24. CTE] Cracking Performance with CTE Values at Different Ages --------- 108 Figure 4-25. CTE2 Cracking Performance with CTE Values at Different Ages --------- 108 Figure 4-26. CTES Cracking Performance with CTE Values at Different Ages --------- 109 Figure 4-27. CTEl Cracking Performance with CTE Based on Different Cycles ------- 111 Figure 4-28. CTE2 Cracking Performance with CTE Based on Different Cycles ------- 112 Figure 4-29. CTES Cracking Performance with CTE Based on Different Cycles ------- 112 XV CHAPTER 1 INTRODUCTION 1.1 Introduction The coefficient of linear thermal expansion is defined as the change in unit length per unit change in temperature. It is referred to as the coefficient of thermal expansion (CTE) or “or” in this dissertation. The general form of the CTE equation is expressed as CTE = [£]/ AT L0 in which AL is the length change, L0 is the original length, and AT is the temperature change. CTE is usually expressed in microstrain (106) per degree Celsius (ue/°C) or microstrain per degree Fahrenheit (us/0F). The CTE of Portland Cement Concrete (PCC) is an important parameter — among other factors — in the development of thermally-induced stresses and deformations in concrete pavements during the first 72 hours after paving and over the design life. For example, CTE affects mean crack spacing in continuously reinforced concrete pavements (CRCPS). Another example is curling stress in the x direction of a finite slab expressed as EaAT - ———(Cx + va) csx — 2 2(1—v ) in which ox is curling stress in the x direction, or is the CTE of concrete, E is the elastic modulus of concrete, AT is the temperature differential between top and bottom of the slab, v is the Poisson’s ratio of concrete, and CK and Cy are correction factors for a finite slab. CTE also influences thermal deformations in slabs which in turn impact crack width in CRCPS, joint spacing (slab length), joint sealant reservoir design, and joint movement in jointed plain concrete pavements (J PCPs). Joint opening for example is affected by CTE. It is expressed as AL = CL(0IAT + s) in which AL is the joint opening, or is the CTE of concrete, C is the adjustment factor due to slab-subbase fi'iction, L is the joint spacing, AT is the temperature range, and 8 is the drying shrinkage coefficient of concrete. The above-mentioned stresses and deformations cause different types of distresses in pavements which consequently affect pavement performance. Mallela et al.1 have listed pavement distresses that are affected by CTE (Table 1.1). Another distress which is related to CTE is the blow-up in concrete slabs at a joint or crack. This type of distress is due to insufficient space for slab expansion. All the mentioned distresses can potentially affect another aspect of pavement performance which is the quality of ride measured by the International Roughness Index (IRI). ”2, CTE is an important factor in According to the “Guide to Concrete Overlays design and construction of bonded concrete overlays of concrete pavements. The PCC overlay and existing pavement should move as one structure in order to achieve desired performance. The unified movement of the two layers will reduce the shear stress at the interface and is achieved if the CTE of the overlay is similar to the CTE of the existing pavement. Table 1-1. Influence of CTE on Pavement Performance (After Mallela et 111.1) Pavement Distress Role of CTE Early-age or premature random cracking due to excessive longitudinal Slab movement High CTE causes excessive longitudinal movement that, if restrained by restraint forces, leads to cracking. Higher curling (temperature-induced) Mid-panel fatrgu e cracking stresses lead to higher mid-panel cracking. Higher corner deflections due to negative Faulting curling, which is a function of temperature gradients and CTE. . . Excessive joint opening and closing causes Jornt spallmg joint sealant failure and joint spalling. Crack load transfer efficiency is affected Punchouts in CRCP by spacing and width of cracks which are impacted by CTE. Based on the above discussion, quantification of the concrete CTE is a necessary step in concrete pavement design. The “Mechanistic-Empirical Pavement Design Guide”3 (M-E PDG) allows for the input of CTE at three levels (quality of data). Level 1 for CTE determination employs direct measurement in accordance with a provisional test protocol developed by the American Association of State Highway and Transportation Officials (AASHTO) designated as AASHTO TP60, "Standard Test Method for the Coefficient of Thermal Expansion of Hydraulic Cement Concrete . Level 2 for CTE calculation uses a weighted average of the constituent CTE values based on the relative volumes of the constituents and is expressed as aconcrete = (aaggregate XV aggregate) + (a paste x Vpaste) in which a is the CTE of the constituent and V is the volumetric proportion of the constituent in the PCC mixture. Level 3 for CTE estimation is based on historical averages. The greatest potential for error is associated with Level 3 data quality, because PCC materials vary considerably. Realistic data for the types of materials being used in concrete mixtures are rarely available and, if they are available, they are likely to be based on specific PCC mixtures. The importance of CTE in pavement design and performance warrants the choice of an appropriate method for CTE determination for concrete pavement projects. Quantification of concrete CTE based on Level 1 is the most reliable method especially for concrete pavement mixtures that are composed of locally supplied aggregates. 1.2 Problem Statement The recently completed M-E PDG uses CTE as one of the parameters to characterize the thermal properties of PCC paving mixture. CTE of the concrete pavement is one of the key inputs for computing response parameters such as curling stresses and joint movement for JPCP as well as crack spacing and width for CRCP. These response parameters in turn influence performance prediction (cracking, faulting, punch-outs, and Currently, the Michigan Department of Transportation (MDOT) does not call for the determination of CTE for the design of concrete pavements. However, CTE has a significant bearing on the computation of concrete pavement response and performance prediction in the new M-E PDG. For the successful implementation of the new design procedure the determination of CTE is necessary. Details about CTE testing and reporting the values should also be described. Finally, the effect of CTE on pavement performance Should be investigated. 1.3 Research Objectives and Plan 1.3.1 Research Objectives The objectives of this research were: Quantification of the concrete CTE composed of different aggregate types used by MDOT Evaluation of the AASHTO TP-60 test protocol Studying variables that affect the direct measurement of concrete CTE Investigation of effects of CTE on pavement performance 1.3.2 Research Plan The research Objectives were achieved by executing the following plan: Development of a test matrix representing the various mixtures for the state of Michigan and different test conditions Execution of the test matrix by casting the required concrete samples for CTE and concrete quality control tests Reporting the results obtained from the testing phase Statistical and practical significance analyses of the test results Conducting sensitivity analyses by using mechanistic-empirical prediction models (HIPERPAV II and M-E PDG software) Presenting the findings of the conducted analyses Recommendation of input ranges for the execution of the new design guide 1.4 Dissertation Organization A review of the literature regarding CTE of concrete, variables affecting the CTE, and the effect of CTE on pavement performance is presented in Chapter 2 of this dissertation. In Chapter 3, the experimental program is presented in detail which includes information about testing equipment and various tests carried out on concrete samples. The results are presented and discussed in Chapter 4. This chapter includes testing results and the results of statistical, practical significance, and sensitivity analyses and discussions. Chapter 5 includes the summary, conclusions, recommendations (test method and CTE values), and future research needs. Appendices and references are presented at the end respectively. CHAPTER 2 LITERATURE REVIEW 2.1 Introduction Several research investigations have been conducted to study the concrete CTE at micro- scale levels. A limited number of studies have been conducted to identify variables that have an influence on the magnitude of CTE, to evaluate CTE variability, and to investigate the effects of PCC CTE on concrete pavement performance. A number of these limited studies only investigate the variables that affect CTE and/or CTE variability. Some other papers only study the effect of CTE on pavement performance, and there are some studies that examine both aspects. The literature review presented in this chapter is divided into three sections. The first section summarizes the studies regarding micro-scale mechanisms of concrete CTE. The second section summarizes information from literature investigating the impact of test variables on the magnitude of CTE and/or the CTE variability. The third section summarizes the impact of CTE on pavement performance of j ointed concrete pavements. At the end of this chapter, the findings from literature review and their application to this research plan are presented. 2.2 Literature on Micro-scale CTE Mechanisms in PCC The CTE of concrete depends on thermal deformations in hardened cement paste (HCP) and in aggregate. The thermal deformations in concrete are tied with its moisture conditions. The CTE of aggregates is not influenced by changes in relative humidity (RH) as it is in the case of HCP according to Meyerss. The thermal expansion (dilatation or dilation) mechanism in HCP has been the subject of several studies some of which are presented in this section. Since the micro-scale CTE mechanisms take place in HCP pore system, this pore system and the water held in it are reviewed before discussing the moisture conditions. Pores in HCP can be classified as capillary pores and gel pores based on their size. The diameter of the capillary pores range between 10 and 10000 nanometers while the diameter of the gel pores range between less than 0.5 and 10 nanometers. Larger capillary pores can hold free (bulk) water while smaller capillary pores can hold water with surface tension forces acting on the water. Larger gel pores can also hold water with large surface tension forces acting on it while smaller gel pores contain adsorbed or interlayer water with no surface tension acting on the water (Mindess et al.6). There are three moisture states in HCP; dry, saturated, and partially saturated. In . dry (bone—dry) state, HCP does not contain any evaporable water. The term “evaporable water” is applied to all classes of water except chemically-bound water. In fully saturated state, all types of pores are filled with water. In partially saturated state, capillary pores are partially filled with water (partially-bound or surface adsorbed water) and gel pores are partially or completely filled with water depending on the RH of HCP. Different mechanisms that cause thermal deformations in HCP and the relations between these mechanisms and various moisture states are discussed below. Bazant7 differentiated three components in thermal dilation of HCP. These components are pure thermal dilation, thermal shrinkage or swelling, and hygrotherrnic dilation. Pure thermal dilation is due to the CTE of HCP constituents (solid particles and different classes of water e.g. free water, adsorbed water, etc.). Dry pastes experience an immediate deformation. For saturated and partially saturated pastes, the immediate deformation is followed by a delayed deformation opposite to the direction of the immediate deformation. For example, rising temperature causes immediate expansion of layers containing adsorbed water. It is then followed by gradual flow of the adsorbed water out of the layer — causing contraction of the layer — until the pressure equilibrium is achieved. This behavior is illustrated in part (a) of Figure 2-1. Letter “h” in this figure refers to RH of HCP, and “a” is volumetric strain. Thermal shrinkage or swelling is caused by redistribution of water between gel pores and capillary pores. Dry pastes do not undergo this type of deformation. For saturated and partially saturated pastes, this type of deformation occurs in opposite direction to the pure thermal dilation. For instance, an increase in temperature results in higher chemical potential in gel water than that of capillary water. In order for the system to be in equilibrium, water from gel pores move into capillary pores and the result is the shrinkage of the gel pores 10 (Helmuthg). This mechanism is classified as a delayed deformation. This mechanism is shown in part (b) of Figure 2-1. Hygrothermic dilation is associated with change in the RH of the pores at constant water content. Dry pastes and saturated pastes do not experience this type of deformation. This phenomenon takes place in specimens that are partially saturated where air-water menisci exist'in capillary pores. A change in RH results in a change in capillary tension which leads to deformation of HCP. For example, an increase in temperature causes expansion of the capillary water which increases the radius of the meniscus and subsequently increases the RH. The increase in temperature also causes reduction of the tension at the air-water interface which again leads to an increase in RH. These two mechanisms are illustrated in Figure 2-2 (Grasley and Lange9). Another possible reason for a raise in RH is the thermal shrinkage or swelling mechanism explained before. An increase in capillary water content (supplied by gel pore upon temperature increase) increases the meniscus radius and RH. This mechanism is recognized as an immediate deformation by Sellevold and Bjrzmtegaard10 while Baiant7 identifies a delayed deformation component in addition to an immediate deformation component in this mechanism. This type of dilation is presented in part (c) of Figure 2-1. 11 STEP INPUT OF I TEMPERATURE To IL I \ h =10 (a) PURE THERMAL uu'n \ h = 0.7 DI A ON h = 9'9 0 a1. 5 h = 0.0 t ’(b) THERMAL h = 0.7 SHRINKAGE h = 1.0 E A h = 0.7 _‘ (c) chRoTHERMIc muuAnou h=0.4ORh=O.85J_ h=0.00Rh=1.0 t .- Figure 2—1. Estimated Typical Response to a Step Input of Temperature for the Three Different Components of Thermal Dilatation, at Various Humidities h (Baiant7) RH=80% RH= 75% Increasing temperature ==9 Figure 2-2. Dilatation of Solid Microstructure Induced by Relaxation with Increasing Temperature (Grasley and Lange9) 12 Combination of the three dilation mechanisms explained above may demonstrate the total thermal deformation behavior of HCP. Figure 2-3 shows an estimation of the combined behavior of HCP with different RH values. Letter “h” in this figure refers to the RH, and “a” is volumetric strain. T h=0.7 h=0.4 11:1.0 h 0.0 Figure 2-3. Family of Thermal Dilatation Curves for Various Humidities (Baiant7) It can be seen form the above figure that dry paste has the lowest thermal dilation, saturated paste has slightly higher delayed dilation (but close to that of the dry paste), and partially saturated paste at RH of 70% has the highest dilation. l3 Other researchers have also compared the thermal deformations of pastes with these three different moisture conditions. Powers and Brownyard11 stated that the thermal coefficients for dry and saturated pastes are about equal and are less than the coefficient of a partially saturated paste. The same observation was reported by Bonnell and Harper12 . Helmuth8 also reported higher CTE values for partially saturated pastes compared with fully saturated pastes. Meyers5 stated that the thermal coefficient is at a minimum in dry and saturated states and that the coefficient is at maximum when the RH of paste is near 70%. Sabri and Illston13 reported a maximum deformation at 75% RH, and similar minimum deformations for dry and saturated states. Yeon et a1.14 stated that the maximum CTE of cement paste — and also concrete — occurs at RH values about 70% to 80%. 14 2.3 Literature on Variables Affecting CTE Value In this section studies (or part of studies) that investigate the variables affecting CTE are presented. Brief descriptions of experimental plans are presented where available. Results and discussions of each study are also presented. In a laboratory study conducted by Alungbe et al.15 in 1992, effects of aggregate type, water to cement ratio, curing, and specimen condition on the magnitude of CTE were investigated. Three types of aggregate were investigated as part of this study. Porous limestone, dense limestone, and river gravel. Three combinations of water to cement ratio and cement content were studied as well as two curing durations (28 and 90 days). Another variable was the specimen condition with two levels, water-saturated, and oven-dried. A length comparator was used to measure the length changes of specimens. Specimens were square prisms with these dimensions: 3 in.><3 in.><11.25 in. In this study, the concrete samples with porous limestone as coarse aggregate, had a CTE that ranged from 5.42 to 5.80 ps/°F (9.76 us/°C to 10.44 us/°C); concrete samples produced from dense limestone had a range of 5.82 to 6.14 ua/° F (10.48 ue/°C to 11.05 Its/0C), and concrete samples made of gravel coarse aggregate had a CTE range of 6.49 to 7.63 Ire/(T (11.68 Its/0C to 13.73 us/OC). A statistical analysis (factorial design) was used to study the effect of different variables on CTE magnitude. Based on statistical analysis results, the authors concluded that aggregate type affects the CTE value, but water to cement ratio and cement content have “no effect” on the CTE. The water-saturated specimen had lower CTE values compared to oven—dried samples. There was no significant difference between samples with different curing durations in water-saturated IS specimens. However, the CTE values of the 28-day cured specimens were higher than the value of 90-day cured samples in oven-dried specimens. Won16 at the University of Texas, Austin evaluated the effect of coarse aggregate content and 32 different aggregate types on the CTE and the effect of sample age, rate of heating-cooling cycle, and size of specimen on measured CTE values. As part of this study, he suggested improvements to the AASHTO TP60 method. The paper stated that the accuracy and repeatability of this test procedure greatly depends on the stability and accuracy of the displacement readings at 50 and 122 °F (10 and 50 °C). As an alternative, it was suggested that the correlation between temperature and displacement changes he used for determination of CTE which results in a repeatable and more accurate CTE test procedure. The testing apparatus and specimen conditioning is the same as in TP60, but the temperature and linear variable differential transformer (LVDT) displacement readings are recorded every minute. The CTE calculation method is also different from the TP60 method and is based on a regression analysis between temperature and displacement readings. It was stated that with the revised procedure, the difference between heating and cooling CTE values is smaller than the difference based on TP60 method resulting in a more accurate and repeatable method in comparison with AASHTO TP60 method. The effect of concrete age was also investigated. Concrete cylinders were tested over a period of 3 weeks and it was found that the age of concrete had little effect on CTE for up to three weeks. This is illustrated in Figure 2-4. 16 CTE (mlcrostralnIC) o 2 4 6 8 10 12 14 16 18 20 22 Time (days) Figure 24. Variation of CTE over Time16 The effect of the rate of heating and cooling was studied. Two difi‘erent rates were applied on a specific test specimen. The CTE value of the slow rate (0.93 °F/hr or 1.67 °C/hr) was found to be 5.82 ua/°F (10.48 WC), and for the fast rate (14.83 °F/hr or 26.7 °C/hr) it was found to be 5.87 ua/‘T (10.57 118/°C). It was concluded that the rate of heating and cooling has little effect on the CTE value. For the effect of the coarse aggregate content on the CT'E value, the experimental results indicated an almost linear relationship between the %volume of coarse aggregate in the PCC mixture and the resulting CTE. It was concluded that there is a 0.025 ue/°F (0.045 pe/°C) change in the measured CTE per percent change in the coarse aggregate volume as shown in Figure 2-5. For the effect of aggregate type on the CTE value, the CTE of concrete Specimens made from coarse aggregate obtained from 32 producers in the state of Texas were measured. The results indicated that concrete specimens fabricated using the limestone aggregate sources had CTE values of about 4.44 us/°F (8.0 us/°C) with a variability of 0.4 ua/°F (0.72 us/° C) whereas, concrete specimens fabricated with gravel as coarse aggregate had a CTE range of 4.50 rte/°F to 7.20 us/‘T (8.10 us/°C to 12.96 rte/°C). It was concluded that this variability is attributed to the different geological make up of the gravel sources. It was stated that this difference in variability between limestone and gravel might explain the better performance and less variability in the performance of PCC pavements made with limestone coarse aggregate versus more variability in performance of the pavements made with gravel aggregates as illustrated in Figure 2-6. CTE (microstrain/C) on ~ . . , _ i. y = -0.0456x + 10.76 ""~-...._R2=0.9963 l 0 25 50 Coarse Aggregate Volume (%) Figure 2-5. Effect of Coarse Aggregate Volume in Concrete on CTE16 18 14 12 Gravel Limestone .L O CTE (microstrain/C) Figure 2-6. Variation of CTE From 32 Aggregate Sources in Texas16 Kohler et al.17 at the University of California, Davis qualitatively investigated the effects of aggregate geology, number of thermal cycles and soaking time on the magnitude of CTE. The CTE test was conducted on 74 core samples obtained from four regions within the state of California. The testing was done in accordance with the revised AASHTO TP60 protocol proposed by Won“. The overall range of CTE was between 4.5 and 6.7 rte/°F (8.10 and 12.06 rte/°C). In order to study the effect of the number of heating-cooling cycles, 74 cores were analyzed. Samples were subjected to three heating-cooling cycles. It was found that the third cycle produced better coefficient of determination (R2) values for the regression analysis used to calculate CTE values and that the difference between heating and cooling cycles was reduced in the third cycle. Also, in 76% of the cases, the third cycle resulted in lower CTE values than the first cycle values. The CTE of the third cycle was found to be on average 0.15 ue/°F (0.27 us/°C) lower than the first cycle CTE value. Figure 2-7 shows the effect of repeated thermal cycles on R2 and CTE values. It was stated that this improvement in R2 value and the difference between heating-cooling cycles improved the confidence in the results and it was an indication that the concrete had reached a stable condition regarding pore water. To quantify the effect of concrete saturation on CTE value, three cores were oven- dried overnight. Two of the cores were tested for CTE immediately after air cooling, and the third one was soaked for 96 hours. The dry cores showed a reduction of the difference between heating and cooling cycles during the first 10 to 15 hours (Figure 2—8). The saturated core showed a constant CTE value for heating and cooling cycles during the 9 cycles to which the core was subjected (Figure 2-9). a) 0.99950 b) 6.0 L L ,, uRising 0.99900 , 5.9 , (heating) E: IFalllng E 5.8 7 - 0.99850 1; CLOOI'UQ 7r 3 5.7 0.99800 E E 5.6 0.99750 . o 5 5 0.99700 5.4 1 2 3 1 2 3 Thermal Cycle Thermal Cycle Figure 2-7. Effect of Repeated Thermal Cycles on CTE, (a) Increase in R2, (b) Decrease in CTEl7 The geographical variability was assessed by testing cores from four California Department of Transportation districts. Northern area (District 2) aggregates were 20 probably sourced from alluvial or glacial deposits. A mix of sandstone and basalt rocks was evident. Southern area (District 11) aggregates were predominantly granitic. Coastal area (District 4) and valley area (District 10) aggregates were predominantly sandstone. The average CTE of District 2 was 6.3 ua/°F (11.34 Its/0C), for District 11 the average was 5 .5 us/°F (9.90 Its/°C), District 4 had an average CTE value of 5.2 ue/‘T (9.36 ua/°C), and the average CTE value of the District 10 was 6.4 ua/°F (11.52 Its/°C). Table 2-1 shows the CTE values at different sites. It was concluded that the geographical l variability is probably associated with variability in aggregates of different mineralogical L composition. Tran et a1.18 evaluated the effects of mixture properties on concrete CTE as part of a study that also evaluated pavement performance sensitivity to CTE values. Twelve standard PCC mixtures were prepared using four major aggregate types including limestone, sandstone, syenite, and gravel. Three types of cementitious materials (cement only, cement and 20% fly ash, and cement and 25% GGBFS) were used with each aggregate type. Twelve additional cement paste samples were prepared by wet-sieving the standard PCC mixtures. For each mixture, three replicates were fabricated and the samples were tested at 7 and 28 days. Range of the CTE values was approximately 5 to 7 us/° F (9 to 12.6 pe/° C). PCC mixtures made with limestone and syenite had the lowest average CTE of about 5.2 ua/°F (9.36 118/0C). PCC mixtures made with gravels had the highest average CTE value of approximately 6.9 us/°F (12.42 ps/° C). The wet-sieved cement paste samples from all mixtures had similar CTE values with an approximate average of 6.6 usf’ F (11.88 Its/°C). 21 After conducting a multi-factor analysis of variance (AN OVA) on mixture properties, it was reported that the aggregate type had a pronounced effect on the CTE. It was also reported that the type of cementitious materials did not influence the CTE of concrete. The fully saturated PCC and cement paste samples showed no significant difference in their respective CTE values at 7 and 28 days. 9 o Rising :1 Falling by G) ? .——D—#— 4:, * U'I CTE(microstraln/°F) O) A (JO q CTE (microstrain/°F) O) I . . 0 10 20 30 4o 50 Time (hours) Figure 2-8. Effect of Saturation on CTE on Two Oven-Dried Cores” 22 CTE (microstrain/°F) 0: 3 I I I 97% 98% 99% 100% 101% Saturation (%) Figure 2-9. CTE Variability at High Saturation Levers" Table 2-1. Mean, Maximum, and Minimum CTE at Different Sites].7 District Site Postmiles Nr.of Mean CTE Min/Max CTE Range cores (arr-10‘) (arr-10'“) 4 SCL-85-N 13.90-15.17 6 5.22 4.73 / 5.68 0.95 4 SCL-85-S 13.52-15.52 12 5.08 4.46 / 6.07 1.61 4 SOL-80-E 18.46-34.34 12 5.38 4.63 / 6.24 1.61 4 SON-lOl-N 50.52-51.79 5 5.14 4.50 / 5.60 1.10 4 SON-lOl-S 50.84-53.02 7 5.18 4.80 / 5.62 0.82 10 SJ-580-E 5.02-8.88 10 6.35 6.12 / 6.57 0.45 10 SJ-580-W 5.35-8.70 9 6.48 6.21 / 6.69 0.48 2 SHA-S-N 37.85-39.91 6 6.29 6.23 / 6.39 0.16 2 SHA-S-S 29.53-31.71 3 6.28 5.96 / 6.69 0.73 I l lMP-86-S 23.50-29.56 4 5.48 5.43 / 5.53 0.10 An investigation was conducted by Naik et al.19 to quantify values for CTE of concrete in order to support the implementation of the M—E PDG program in Wisconsin. Coarse aggregate from 15 sources were used in the fabrication of concrete specimens. Glacial gravel from six sources and dolomite from 5 sources were used. Quartzite, granite, diabase, and basalt each from one source were also used. CTE values were obtained according to the AASHTO TP60 test protocol. Three replicate specimens 23 at the age of 28 days were tested. The cementitious materials proportion of the mixture design included 70% type I cement and 30% class C fly ash. In another part of the study, the effect of cementitious materials on CTE of concrete was evaluated. Four mixture designs were considered. Each mixture design included a different source of dolomitic aggregate. Cementitious materials used were cement, cement plus fly ash (two different mixtures), and cement plus ground granulated blast furnace slag (GGBFS). As shown in Figure 2-10, the concrete made with quartzite showed the highest ‘ CTE value of 6.8 118/OF (12.2 118/0C). The lowest CTE values were those of concrete made with diabase, basalt, and granite ranging from 5.2 to 5.3 Its/°F (9.3 to 9.5 118/°C). Concrete made with glacial gravels from six different sources had CTE values between 5.4 and 5.9 us/°F (9.7 and 10.7 us/°C) and the CTE range for concrete made with dolomite from five different sources (Figure 2-11) was relatively uniform, between 5.8 to 6.0 118/0F (10.4 to 10.8 118/0C). According to this study, the types and sources of cementitious materials had a negligible influence on the concrete made with dolomite. The CTE was influenced very little (0.0 to 0.1 us/°F or 0.0 to 0.2 tie/0C) by the source of cement and class C fly ash, the use of fly ash versus GGBFS, and the use of cement versus cement plus class C fly ash. 24 -r 6.8 '6 E + 6.6 ° 8 If L »—-—-~ 6.4 '5 E -. 6.2 E v .3 5 __dr 6.0 50 g —r 5.8 o 3. 0 x E DJ D 65 N le1- leZ- G\I3- le4- GMS— GVIG- Qtz- Gnt- Dbs- Bst- c1-f1 01-f1 c1-f1 c1-f1 c1-f1 c1-f1 c1-f1 c1-f1 c1-f1 c1-f1 Figure 2-10. CTE of Concrete Made with Gravel, Quartzite, Granite, Diabase, or Basaltl9 -r 6.8 Expansion (10"I°C) 28-Day Coefficient of Thermal Umf Um} mm} UmS UmS Wm¢ Wm¢ UmS Mm5 c1-f1 c1-f1 c2-f1 c1-f1 c1-s c1-f1 c1 c1-f1 c1-f2 Figure 2-11. CTE of Concrete Made with Dolomite and Different Cementitious Materialsl9 Mallela et al.1 presented the effect of aggregate type on CTE value in a paper that discussed the practical significance of CTE variability on the performance of concrete pavements. The CTE results were based on hundreds of cores obtained from LTPP study sections throughout the United States. 25 AASHTO TP60 test protocol was used to measure and calculate CTE values of the specimens. A total of 673 cores representing hundreds of pavement sections throughout the United States were tested and analyzed. The predominant aggregate type in each specimen was identified using different methods including optical microscopy. The general range of CTE values for the tested specimens in this study was between 5 and 7 ue/°F (9 and 12.6 116/°C). It was observed that concrete made with igneous aggregate generally had lower average CTE than concrete made of sedimentary aggregate. It was also observed that with some exceptions, the variability (standard deviation) of the measured CTE was higher for concrete made with sedimentary aggregate than the concrete made with igneous aggregate. In a paper by Tanesi et a1.20 CTE variability was examined in order to be incorporated in the other part of the project in which the effect of CTE variability on concrete pavement performance was investigated. The AASHTO TP60 method was described and possible sources of CTE variability were mentioned. Specimen induced variability (moisture state and temperature gradient within the concrete specimen, specimen inhomogeneities) and equipment induced variability (LVDT sensitivity, power fluctuations, and frame calibration) as well as the intrinsic equipment limitations were mentioned as possible sources of variability among CTE values. Since 1996 the Federal Highway Administration (FHWA) has tested over 1800 core samples from various LTPP sections throughout the country. The CTE values ranged from 4.5 us/°F to 7.5 rte/0F (8.1 11st to 13.5 Its/0C) as shown in Figure 2-12. Approximately 150 specimens were tested multiple times to determine the repeatability of the test procedure. The average variability amongst replicate samples was reported to 26 be 0.4 ua/°F (0.72 ua/°C) as presented in Figure 2-13. SCTE is the maximum difference between CTE test results performed on the same specimen. 35 30 g 25 3 20 5 3 15 S E 10 5 o 4 4.5 5 5.5 6 6.5 7 7.5 Mean CTE (x1o*3 inlinI°F) Figure 2-12. Histogram of the Mean CTE of the Specimens20 20 18 Average acre: 0.4 x 10*5 in/in/°F l 15 __ Standard deviation SCTE = 0.4 x 10‘6 r g 14 - in/in/°F ~ 3 12 ‘ Median 5CTE = 0.3 x 10'6 in/in/°F c 10 T 3 8 ‘ .. 5 - u. 4 _ 0 4 o 0.1 0.2 0.3 0.4 0.5 0.7 0.9 1.2 1.5 2 2.5 8CTE (x1o‘5 inlinloF) Figure 2-13. Histogram of the tier}:20 27 2.4 Literature on CTE Impact on Pavement Performance In this section studies (or part of studies) that investigate the impact of CTE on pavement performance are presented. Results of the analyses and relevant discussions are also presented. As it was mentioned before, the CTE of PCC is a resultant of the HCP CTE and aggregate CTE. It has been suggested that if these two CTE values differ too much (more than 3.0 ue/°F [5.5 Its/°C]), a large temperature change (more than 122 °F [50 0C]) may cause differential movement and breakage of the bond between aggregate and surrounding HCP leading to cracking in concrete (N eville21). Mallela et a1.1 qualitatively investigated the practical significance of CTE variability on the performance of concrete pavements. The authors used the M-E PDG software for this investigation. It was stated that the PCC CTE affects joint spacing, joint load transfer, curling stresses, and comer deflections in JPCP, which in turn affect the transverse cracking, joint faulting, and smoothness. It was also stated that the interaction of CTE with other design features and site conditions plays a Significant role in the extent of effect that CTE has on pavement performance. For example, higher CTE values coupled with a high temperature climate, is more detrimental than a climate with low temperatures. Similarly, the effect of CTE is more pronounced in pavements with larger joint spacing than the ones with shorter joint Spacing. So, two types of sensitivity analyses were carried out on JPCP performance. In one analysis, only the effect of CTE on performance was investigated and in the other analysis, the interaction effects of CTE with other PCC design factors were studied. 28 In the first sensitivity analysis, a representative design with only the CTE being the variable was assumed. Three levels of CTE investigated were mean, mean plus two standard deviations, and mean minus two standard deviations for each aggregate type. The effect of PCC CTE on percent slabs cracked, faulting, and IRI is shown in Figures 2- 14, 2-15, and 2-16 respectively. It was observed that CTE affects cracking, faulting, and IRI, but the CTE effect is more pronounced on predicted cracking than on mean joint faulting. It was also stated that in general, the higher the CTE, the poorer the pavement performance, and that the aggregate type has the largest influence on CTE value. Finally, the higher the variability in the measured CTE (for each aggregate type; aggregate source information is not known from the paper), the more unpredictable the pavement performance. The critical design inputs and site conditions used to investigate the interaction effect of CTE and design factors were PCC flexural strength (500 and 750 psi) and elastic modulus (co-varied with flexural strength), transverse joint spacing (15 and 20 ft), and climatic conditions (wet freeze and dry-no freeze). Three levels of CTE (4.5, 5.5, and 7.0 us/‘T or 8.10, 9.90, and 12.60 us/° C) were also considered in the analysis. It was found that in general, higher CTE values resulted in higher joint faulting, slab cracking, and roughness. Larger joint spacing and concrete strength increased the effect of CTE on joint faulting due to higher curling deflections (higher modulus of rupture relates to higher elastic modulus in the strength relationships used in M-E PDG). In wet freeze climate, higher joint faulting values were observed. Larger joint spacing and lower concrete strength resulted in amplified effect of CTE on transverse cracking. The CTE effect on IRI was more sensitive to concrete flexural strength. 29 80 ..__ - 70~ so. ._ 401 - Ioc ' 10 — f 3 01 J l- Percent Slabs Cracked g6” gt? 96.5” ‘5‘” {\‘é .001{\ «$5 ‘00“ (4;? 1,06% 000 90 {‘00 (9‘0 90 O o\0 0’9 0% 6'9 Y‘ Q Q 06‘ 0 (90° Figure 2-14. Effect of PCC CTE and its Variability on the M-E PDG Predicted Percent Slabs Crackedl 0.20 7% —— ...___.____ _ -.---__ . ___ 0.18 J — A 0.16 i _ 0.14 “l — 0.12 0.101 0.08 ~ 0.06 ~ 0.04 ~ 0.02 In Mean Joint Faulting ( Figure 2-15. Effect of CTE and its Variability on the M-E PDG Predicted Mean Joint Faulting‘ 30 “at... IRI (in/mile) 2 t. :‘3 1‘ 51 fl Figure 2-16. Effect of CTE and its variability on the M-E PDG predicted IRIl In a paper by Tanesi et al.20 the impact of CTE variability on the predicted performance of concrete pavements was documented (as part of a project that also investigated the sources of CTE variability). Based on sensitivity analysis using M-E PDG program the effect of the CTE variability on slab cracking was found to be significant. The higher the CTE, the greater is the effect of variability. As an example, a difference of 2.0 ue/°F (3.6 Its/0C) between minimum and maximum measured CTE values for the same specimen with an average CTE value of 4.0 118/0F (7.2 ua/°C) would result in 8% difference in the predicted percent of slabs cracked, but the difference would be 65% if the average CTE value were 6.5 118/OF (11.7 usl° C). Figure 2-17 shows the effect of CTE variability on predicted percent slabs cracked. dCTE in Figures 2-17, through 2-19 is same as the BCTE. 31 Colorbar: change in Percent Cracking 60 1.75: 1.51 50 of I l , : 125: x=5 . 40 E Y: 0.9 ' , » “to 1 Level= 6.3579 ; : 30 E 0.75 ..... ; g _ 20 0.5 l ‘ 0.251 i 10 0‘ I 0 4 4.5 5 5.5 6 6.5 7 CTE (x10'6 in/in/OF) Figure 2-17. Difference in the Predicted Percent Slabs Cracked as a Result of the dCTE20 The same effect mentioned above can be seen on the predicted faulting of concrete pavements as shown in Figure 2-18. 32 dCTE (x1061n/in/0F) Colorbar: change in Faulting in in. 1.8 1.6 0.1 1.4 0.08 1.2‘ X: 5 , Y: 0.9 . l _ .. . . 1 ‘ Level— 0.028494 . f f. 0.06 0.83 x—6.5 Y: 0.5 0.6 Level: 0.02415 0'04 0.4] 0.02 0.2‘ 0 0 4 4.5 5 5.5 6 6.5 7 CTE (x10‘6 in/in/OF) Figure 2-18. Difference in the Predicted Faulting as a Result of the dCTE20 The impact of 5CTE on the International Roughness Index (IRI) was also documented. The effect is similar to the one of the percent slabs cracked case. For the same example mentioned above, the IRI for the first case (a difference of 2.0 ue/°F or 3.6 lie/°C for a specimen with average CTE value of 4.0 Ila/0F or 7.2 ue/°C) the difference in IRI is 33 inch/mile, while for the second case it is 113 inch/mile. Figure 2-19 illustrates this effect. The authors concluded that the CTE test variability leads to significant discrepancies in the predicted IRI, percent slabs cracked, and faulting. 33 Colorbar: change in IRI (in/mile) X: 5 X. Y: 0.9 ..,, :i' Level: 23.4067 ’effig I X: 6.5 Y: 0.5 Level: 23.9157 dCTE (x1061n/in/0F) 4 4.5 5 5.5 6 6.5 7 CTE (x10'6 in/in/OF) Figure 2-19. Difference in the Predicted IRI as a Result of the dCTE20 Tran et a1.18 evaluated pavement performance sensitivity to CTE values as part of a study that also evaluated effects of mixture properties on concrete CTE. In order to investigate the practical significance to pavement design, a sensitivity analysis using M-E PDG software (version 1.0) was conducted. Three levels of joint spacing and four levels of CTE values corresponding to cement paste, PCC mixtures with sandstone, gravel, and limestone/syenite were considered. The results are showed in Figure 2-20. It was concluded that the type and proportion of coarse aggregate influences the joint spacing design and subsequently, the pavement performance. 34 0.5 g 0.4 I; 0.3 C E 0.2 - 3 \ u_ 0.1 , , 0.0 5.2 6.4 6.6 6.9 (PCC w/ (PCC w/ (Paste) (PCC w/ Limestone or Sandstone) Gravel) Syenite) CTE (1o‘/°l=) (a) Faulting versus CTE for three joint spacings 100 .3 80 E ‘50 in 15 ft E 40 I.“ 20 ft_ 0 20 0 5.2 6.4 6.6 6.9 (PCC w/ (PCC w/ (Paste) (PCC w/ Limestone or Sandstone) Gravel) Syenite) CTE (10‘/°F) (b) Cracking versus CTE for three joint spacings 5.2 6.4 6.6 6.9 (PCC w/ (PCC w/ (Paste) (PCC w/ Limestone or Sandstone) Gravel) Syenite) cTE (io‘PF) (C) IR] versus CTE for three joint spacings Figure 2-20. Effect of Constituent Properties on Pavement Performance Predictions18 35 Kohler and Kannekanti22 studied the influence of PCC CTE on the cracking of the JPCP. One hundred and four in-service highway sections in California were selected for this study and cores obtained from these sections were tested in the University of California Pavement Research Center (UCPRC) laboratory. The CTE testing protocol followed in the University of California study was based on the recommended amendments to the AASHTO TP60 protocol proposed by Won“. The main features of this testing procedure are summarized in Won’s paper. The CTE of each section was generally determined from the CTE results of at least two cores. The total number of tested cores was 185. The CTE values ranged from 4.8 to 6.7 rte/°F (8.6 to 12.0 ire/°C). Three types of cracking levels were incorporated in the data collected by California Department of Transportation. First stage cracks (FSC) are cracks that do not intersect and divide the slab into two or more large pieces; third stage cracks (TSC) are interconnected cracks that divide the slab into three or more large pieces; comer cracks (CC) are diagonal cracks that meet both a longitudinal and transverse joint within 6 feet and over 2 feet at the same slab comer. Figure 2-21 shows examples of these cracking levels. Slab cracking is reported as a percentage based on the number of slabs exhibiting these cracking levels over the surveyed distance (0.1 to 1.5 miles for a given homogeneous section). Ratio of the severely cracked sections to total number of sections was calculated (k). The severity limit used for FSC and TSC was 10% and for CC, 5% limit was used. 36 Figure 2-21. Examples of FSC, TSC, and CC22 The ratio of cracked slabs mentioned above was computed for two groups of sections. One group consisted of sections with CTE values lower than an arbitrary limit and the other group included sections with CTE values higher than the arbitrary limit. Two arbitrary limits were considered. These limits were 5.7 ue/°F (10.26 ue/°C) and 6.0 lie/°F (10.80 lie/°C). This ratio (k) versus pavement age in years was then plotted (Figure 2-22 for FSC and TSC, Figure 2.20 for FCS+TSC and CC). It was stated that the cracking trends for low and high CTE pavements were drastically different when the CTE limit was 5.7 Ila/°F (10.26 Ila/°C). For all types of cracks, pavements with high CTE developed more cracks over time than the pavements with low CTE. It was concluded that if low CTE is specified, it can reduce cracking over the life of JPCP and longer lasting concrete pavements can be expected. 37 Ratio of cracked slabs (k) FSC 0 10 Pavement Age (years) o CTE >5.7 o CI‘E >60 CTE >5.7 ------- CTE >6.0 - CTE <=5.7 .. CTE <=6.0 CTE <=5.7 ------- CTE <=60 Ratio of cracked slabs (k) Pavement Age (years) o CTE >5.7 o CI‘E >6.0 CTE >5.7 ------- CTE >60 I Cl‘E <=5.7 a CTE <=6.0 CTE <=5.7 ------- CTE <=6.0 Figure 2-22. Comparison of Ratio of Cracked Slabs for Pavements with High and Low CTE (FSC and TSC)22 38 'F—i—n—j 90 v o FSC+TSC 80 --— — 8 U) E (I) g c... o .9 $2 0 10 20 30 40 50 Pavement Age (years) 0 CTE >5.7 l CTE <=5.7 o CTE >60 0 CTE <=6.0 CTE >5.7 CTE <=5.7 ------- CTE>6.0 ------'CTE<=6.0 90 80 ‘—~ CC —---—- --—-- A 70 -«-—— ~ — “—7- -~ LL# - #— if: E 60 _ LH_____ W -———~ -—-—-- —— U) 50 __.__._. EAL... .. _ __ .— 8 5 * E 40 n.-,,__,,,,‘,, ‘ -_-_ .-.. . 9.- _-___ . __ (H 30 ----‘ o .9. 20 52 10 —— O ._ 0 10 20 Pavement Age (years) o CTE >5.7 - CTE <=5.7 o CTE >6.0 o CTE <=6.0 CTE >5.7 CTE <=5.7 ------- CTE>6.0 -------CTE<=6.0 1‘ t Figure 2-23. Comparison of Ratio of Cracked Slabs for Pavements with High and Low CTE (FSC+TSC and CC)22 39 Hossain et a1.23 investigated the effect of the hierarchical input levels of CTE on the performance of jointed concrete pavements using the M-E PDG program. The CTE data was obtained from in-service pavements in Kansas. CTE results from LTPP projects in Iowa, Kansas, and Missouri were also reviewed. After an overview of the AASHTO TP60 test procedure and describing the hierarchical input levels used in M-E PDG, input levels 1 and 2 for CTE were presented. For input level 1, two cores were retrieved from a PCC pavement in Kansas. The CTE values were 5.4 and 5.5 p8/°F (9.8 and 9.9 118/°C). The CTE values from the LTPP database were a result of testing on 51 cores and ranged from 4 to 7.1 ue/°F (7.2 to 12.8 118/0C). The lowest 10% (4.3 us/‘T or 7.8 paf’C) and highest 10% (6.5 its/”F or 11.7 us/°C) mean values were used in the sensitivity analyses in this study. The CTE values for Iowa retrieved from LTPP database ranged from 4.4 to 7.6 ue/°F (8.0 to 13.8 ue/°C) based on 62 cores. Also, the CTE values for Missouri were between 4.1 and 11.0 ua/°F (7.3 and 19.8 pus/°C). Level 2 CTE values were calculated from an equation suggested by M-E PDG. The values needed for the calculation were extracted from the LTPP database. For Kansas aggregates, CTE of dolomite, gravel, limestone, and sandstone were calculated and compared to measured values (Figure 2-24). The calculated CTE values were 11 to 19% higher than the measured values. For Iowa, dolomite and limestone CTE values were calculated. The calculated values were 10 to 14% higher than the measured ones (Figure 2-25). The aggregates available in Missouri were dolomite, limestone, a combination of dolomite and limestone, and sandstone. The calculated values, except for 40 dolomite, were 13 to 30% higher than the measured values (Figure 2-26). For dolomite, the calculated values were 25% lower than the measured values. In the same study, in order to investigate the effect of CTE on PCC pavement performance, six in-service jointed plain concrete pavement projects were selected. Three levels of CTE (average of the highest 10% based on LTPP data, CTE based on a recently built project, and average of the lowest 10% based on LTPP data) were used in the M-E PDG design analysis. 8.000 7.500 7.000 <7 6.500 6.000 < 5.500 - 5.000 - 4.500 4.000 < 1 I Calculated l I Measured a pee Dolomite Gravel Limestone Sandstone Coarse Aggregate Type Figure 2-24. Calculated and Measured PCC CTE Values (x 104%) for Kansas23 6.200 , , - , 7 6.100 ~ , —~~ 6.000 5.900 - , ~ 5.800 . , W, 5.700 . 5.600 TA” 5.500 r ~ 5.400 . , ,. 1 i ’ ' El Calculated , 7— . i gIMeasured 3 a pee Dolomite Limestone Coarse Aggregate Type Figure 2-25. Calculated and Measured PCC CTE Values (x 10'6/°F) for Iowa23 41 8.600 8.000 7.400 r__.__’ 3 6.800 ICalculated a. a 6.200 IMeasured : 5.600 —J 5.000 4.400 Dolomite Limestone Limestone 8. Sandstone Dolomite Coarse Aggregate Type Figure 2-26. Calculated and Measured PCC CTE Values (x 10'6/°F) for Missouri23 The effect of CTE on IRI is that higher CTE would result in higher IRI. For example with an increase in CTE from 4.3 to 6.5 ua/°F (7.8 to 11.7 ue/°C), IRI increased from 114 to 135 inch/mile. By studying other pavements, it appeared that the effect of CTE on IRI is more pronounced in pavements with thinner slabs or lower strength. It was also found that the CTE does not affect the predicted IRI for pavements with widened lanes and tied PCC shoulders. Faulting was found to be sensitive to CTE values. A combination of high cement factor and higher CTE values would result in higher faulting. The effect of CTE on percent slabs cracked was found to be very significant. For example, with a CTE value of 4.3 ue/°F (7.8 lie/°C), the percent slabs cracked was 0.2% while for a CTE value of 6.5 ua/°F (11.7 usf’C), the percentage increased to 2% which is a tenfold increase for a 50% increase in the CTE value. Another part of the study was to investigate the hierarchical input levels on PCC performance. For this purpose, one project was selected. Four types of coarse aggregates (dolomite, limestone, gravel, and sandstone) were studied. Level 1 (measured) and level 2 (calculated) inputs were investigated. Table 2-2 shows the results. The design using 42 calculated CTE values failed (based on design reliability of 90%) for IRI and/or percent slabs cracked for all aggregate types and for gravel with measured CTE value. Faulting was relatively unaffected for all aggregate types and both input levels. Table 2-2. Predicted Distresses for Computed and Measured PCC CTE Values for Typical Aggregates in Kansas23 Calculated a pcc (/°F) Measured a pcc (/°F) Coarse Aggregate IRI Faulting % Slabs IRI Faulting % Slabs Type (in/mi) (in) Cracked (in/mi) (in) Cracked 1343* 9.5* Dolomite Failed 0.035 Failed 120.5 0.021 1.0 147.0 20.4 131.1 7.0 Gravel Failed 0'042 Failed Failed 0'0” Failed Limestone 12:33! 0.03 l 5.4 122.0 0.024 1 .5 1755* 46.7* Sandstone Failed 0'055 Failed ”20 0'024 1'5 * one sample 43 2.5 Application of the Reviewed Literature to the Research Plan According to sections 2-2 and 2-3 of this literature review it was found that several factors affect the magnitude of the CTE of concrete. These factors include test-related as well as specimen-related factors. Test-related factors affecting the CTE could be induced by LVDT sensitivity, power fluctuations, frame calibration, intrinsic equipment limitations, number of heating- cooling cycles, and test method used to determine the CTE. Specimen-related factors that affect the CTE could stem from coarse aggregate type, age of the specimen, moisture state and temperature gradient within the concrete specimen, and specimen inhomogeneities. Based on the literature review, available laboratory resources, funding, time frame, and funding agency’s demands, factors investigated in this research plan included coarse aggregate type, specimen age, number of heating-cooling cycles, and test methods. The reviewed literature did not investigate the effects of aggregate type, age (from 3 to 365 days), and number of heating-cooling cycles together in a factorial design the way it was conducted in this study. The effects of these factors were studied by employing a methodical statistical approach not seen in the reviewed studies. The effects of some of these factors on CTE testing were also subjects that had not been investigated in most studies. One factor that was not investigated in this study was the moisture state of the concrete. There are a couple of reasons for not considering this factor. The first reason is that the current testing procedure for concrete CTE is AASHTO TP60 and in this method, 44 the concrete specimen is in tested in saturated state. The second reason is that moisture conditions affect the HCP more than they affect the concrete. Generally, 60% to 80% of the volume of concrete is consisted of aggregates therefore the CTE of aggregate affects the concrete CTE more than that of the other constituents such as cement. Yeon et al.14 reported that the difference between maximum and minimum CTE values in cement paste (associated with difference in RH) was about 10% to 12% while little difference (3%) was observed between maximum concrete CTE at 70% - 80% RH and CTE of concrete at 100% RH. According to section 2-7 of this literature review it was found that CTE of concrete affects different aspects of pavement performance such as cracking, faulting, roughness, and crack spacing and width. Based on the available sources and limitations, sensitivity analysis factorials were developed in this research plan to investigate the early-age stresses and long-term transverse cracking in JPCPs. 45 CHAPTER 3 EXPERIMENTAL PROGRAM 3.1 Introduction This chapter provides details regarding materials that were used in different concrete mixtures, sample fabrication process, curing, tests used for determining fresh and hardened concrete properties, and CTE test protocols. Coarse aggregate from different sources were used in concrete mixtures. One type of fine aggregate form one source was used in all mixtures. Mixture design was a typical MDOT design and the samples were prepared according to ASTM standards. Two types of tests were conducted in this experimental program; quality control tests and CTE test. The quality control tests were conducted in order to check the quality and conformance of the supplied concrete. These tests included fresh and hardened concrete mechanical properties tests. The CTE test was the most important test in this program and was conducted in a way so that its results could be used in two different methods of CTE calculation. This will be explained later in this chapter. 46 3.2 Materials 3.2.1. Aggregates Fine aggregate used in all mixtures was 2NS sand from Schlegel pits. Coarse aggregates were 6AA class and their sources are presented in Table 3-1. The 2NS and 6AA are MDOT grading classes for fine and coarse aggregate respectively and their sieve analysis requirements can be found in “2003 Standard Specifications for Construction”24. Figure 3-1 shows the locations of the various aggregate sources within the state of Michigan. Mineralogical composition and physical properties of coarse aggregate are summarized in Table 3-2. For aggregates with no mineralogical information available, petrographic or chemical compositions are summarized in Tables 3-3 or Table 3-4, respectively. Table 3-1. Coarse Aggregate Types and Source Names Mixture ID Primary Aggregate Class Aggregate Source, County CTE 1 Limestone Pit # 71-47, Presque Isle CTE 2 Gravel Pit # 19-56, Clinton CTE 3 Limestone Pit # 75-5, Schoolcrafi CTE 4 Slag Pit # 82-19, Wayne CTE 5 Dolomite Pit # 49-65, Mackinac CTE 6 Gabbro Pit # 95-10, Ontario CTE 7 Dolomite Pit # 58-11, Monroe CTE 8 Dolomite Pit # 91-06, Cook 47 - 358-11 a 91-06 Figure 31-]. Locations of the Aggregate Sources (After Sutter et ah“) 48 .m-m 03m... 5 02.808 3 02:89:00 32825 .1. .m-m 28H 5 08.88.. g 00280800 0202803 * $28.80 00388.? n U< H .5380 058% 8-030 u Own—O ._. $2 038200 w 5.0 . . 2828 Been . . . . e as o S m mew N 8388 00 new bum 00 :8 EMS on N mm o em 0 3 no 0. ~ D h Eb 0:88 08 5.800 56 Sad 6:80me 88:0 858 608550: a... 0580 o 2.0 68—02me 88.3 BE: .0580 . . 6:528 858 . . . . a 56 e me o mmn m 8.800 00 8388 >an 8 :5 Ems a O we o we 0 3 mo 0. _ D m Eb 0.5808 8803 383 00 536:0» . . 30% 833.80 88% 2: .0305 wk. N mam N .8 0.8 00 8% 08 833.80 880 * wflm 0 who 05 chew 08 833.80 83063 22. and owed 0:988: 808% 00m 93 8 =8 2&3 v0.0 cod 0500 has 0000885 m who end End 32 a. 6280 N who x52: 0:988: v: wwwm 859% 00m a 5 £7.80 080555 who Ed 303 was 008885 _ who 55 0305 x80 8 .0305 00 cup. 650 awed 608 £00828 “9.. .680 858860 25 86m 9 Ewe? .3 ex. 0652 SEE 235: A340 8 830m 80.3.0 Saweuwwaa 08an 05 me 83800.5 .833.— 000 Somme—0852 .Nrm 03:. 49 Table 3—3. Petrographic Composition of Slag and Gravel Aggregates* M‘I’Bm RISES—F3... AggregateTwe M8221?” Igneous/Metamorphic 54 Dense Carbonates 35.4 Absorbent Carbonates 4.7 Non-Friable Sandstone 1.0 CTE 2 Gravel Friable Sandstone 1.7 Siltstone 0.6 Shale + Coal 0.1 Clay Ironstone 0.5 Chert 2 Vesicular Particles 85.7 CTE 4 Slag Dense Particles 10.8 Glassy Particles 3.3 Magnetic Particles 0.2 * These petrographic testing and analyses were conducted by MDOT. Table 34. Chemical Composition of Gabbro Aggregate (After Sutter et al.25) . Primary . Oxide/Element % by Mixture ID Rock Type Ox1de/Element Weight MgO 8.44 A1203 18.61 SiOz 45.53 CTE 6 Gabbro S 0.02 CaO 11.81 Fe203 13.13 50 3.2.2. Concrete The concrete used in the fabrication of cylindrical and prismatic test specimens was supplied by a local ready mix supplier. This ensured that all specimens needed for a given mixture were produced fiom a single batch, thereby reducing experiment variability. The concrete mixture design used in the fabrication of the test specimens was a typical paving mixture design used by MDOT (designated as P1). Individual mixture designs are summarized in Table 3-5. Table 3-5. Concrete Mixture Designs (lbs/yd3) * This mixture design also included 94 lbs/yd of Fly Ash. TAEA=Air Entraining Agent Ingredients CTE 1 CTE 2 CTE 3 CTE 4 CTE 5 CTE 6 CTE 7 CTE 3* Cement 564 564 560 560 560 573 560 376 Water 259 259 250 252 275 258 242 155 Coarse Agg. 1740 1760 1838 1575 1908 1774 1715 1942 Fine Agg. 1360 1360 1338 1348 1260 1230 1330 1444 ABAT, (fl, 01) 10.0 10.0 7.5 7.5 7.5 7.5 7.5 28.0 3 Concrete specimens (except for CTE 8) were prepared at the Michigan State University (MSU) Civil Infrastructure Laboratory (CIL) according to the ASTM C 192 “Standard Practice for Making and Curing Concrete Test Specimens in the Laboratory”. CTE 8 specimens were field-prepared specimens from an actual paving project in Michigan. Concrete specimens fabricated for elastic modulus, compressive strength, and tensile strength tests were cylindrical specimens 4 inches in diameter and 8 inches in 51 length (height). The dimensions of the concrete beams (square prisms) fabricated for flexural strength test were 4 x 4 x 14 inches. The samples made for CTE test were cylinders 4 inches in diameter and 7 inches in length (height). At least three replicate samples were fabricated for each test. Over 700 specimens were fabricated to characterize the mechanical properties and CTE of the concrete paving mixtures. Thermocouples were embedded in the center of designated specimens to monitor concrete temperature for the CTE tests. All specimens were de-molded 24 hours after fabrication and were cured at 100% relative humidity and 23 °C temperature in an environment chamber until the time of testing. CTE specimens were placed in a limewater bath as required by the test protocols. Once the specimens were de-molded and cured for an appropriate time, various tests were conducted to assess the properties of interest. 52 3.3 Concrete Properties Tests Fresh and hardened concrete mechanical properties tests and thermal property test were conducted on concrete specimens. The fresh and hardened concrete mechanical properties tests were conducted in order to check the quality of the supplied concrete and its conformance to specifications. CTE test was conducted in a way so that its results could be used in two different methods of CTE calculation. This will be explained in the next section. The fresh concrete tests included slump, air content, unit weight, and temperature tests conducted according to American Society for Testing and Materials (ASTM) standards. The hardened concrete mechanical properties tests included compressive, tensile, and flexural strength tests in addition to elastic modulus test. These tests were also conducted according to ASTM standards. The CTE test was conducted according to AASHTO TP60 and is described in the next section. The material characterization tests performed on the concrete samples and their frequency are summarized in Table 3-6. 53 Table 3-6. Summary of Material Characterization Tests Test ASTM Measured No. of Frequency Test Name Attribute Designation Property Specimens of Testing Concrete Slump C 143 workability P . Total air ro ertres ofrlzresh Air content C 231 cortirtenltl Of One per Once C es batch oncrete concrete Unit weight C 138 Unit weight Temperature C 1064 Temperature Compressive strength* C 39 Mechanical Flexural Concrete 1, 3, 7, 14, Properties strength C 78 strength 28,90,365 of days after Hardened Split tensile specimen Concrete strength C 496 Three fabrication replicates Elastic Concrete for each modulus C 469 stiffness test/batch AASHTO Linear unit 3a 79 143 28: Coefficient of TP60 length 90’ 180’ Thermal . 365 days thermal change/unit Property . . afier expansron change in . Revised temperature SPCF‘mF’“ TP60 fabrrcatron * Compressive strength was determined by the same apparatus and specimen used to determine the modulus of elasticity. 54 3.4 Thermal Property Test (CTE Test) CTE test was conducted according to the AASHTO TP60 “Standard Test Method for the Coefficient of Thermal Expansion of Hydraulic Cement Concrete”4. The CTE test apparatus consists of a temperature controlled water bath, a rigid frame to support the test specimen, an LVDT to record the change in specimen length, and a data acquisition system for continuous data collection. Figures 3-2 and 3-3 illustrate the CTE test setup. Thermocouple \. ~ > ,__;|3-- r__ LVDT . . . Data Acquisition Power S stem Slipply y _ ; LVDT , g H— ’ 3:; h I. Fixture r 1 and {3.2-.191 Invar J, =- 6 SpCCian E 1 ‘7}?- -: 4"? ROd {,’=3.‘ Controlled Temperature Water Bath Computer Figure 3-2. Schematic of the Test Setup 3.4.1 Controlled Temperature Water Bath Three “Programmable Refrigerating/Heating Circulators” by PolyScience were used in this experiment. The temperature range for these circulators is -25 to +150 °C with temperature stability of i001 °C. Figure 3-4 shows a Model 9612 circulator. 55 Computer Data Acquisition LVDT Power Supply Water Bath LVDT Fixture Figure 3-3. Complete Test Setup <— Temperatnre Controller Water Reservoir Lid Figure 3-4. Controlled Temperature Water Bath (PolyScience26) 56 3.4.2 Data Acquisition System A Personal Daq/3000 data acquisition system by IOtech was used to read and record the length changes of the specimens measured by LVDTS and also read and record water bath temperatures measured by thermocouples. This system is shown in Figure 3-5. Figure 3-5. Data Acquisition System (IOtech27) The software used with this system was DaqViewTM which allows the user to save the data in text format among other file formats. A screen shot of the channel setup is illustrated in Figure 3-6. 3.4.3 Linear Variable Differential Transformer (LVDT) Three “GHSD 750-050 Spring-Loaded DC-LVDT Position Sensors” by Macro Sensors were used to measure the length changes of concrete specimens subjected to temperature cycles. These LVDTS have a nominal range of i0.050 in. from null position and full scale output of O to $10 V DC. Figure 3-7 shows the LVDTS. 57 [Priq‘r’iew - ['AOVIEWZDAQ [Peisonnlliaq3("100[261‘l'l 66}] file Edit Qata window Qevice Llelp . 10 14 ‘ng i 2 El .11 £1 P §_ :- Analog & Scanned Digital inputs E g. l ChannelUrt Yes v F% Pg 3% . ‘1 1 SEE] HEB q) ‘ CH Un ] Type I Polarity ] Label | Units 1 Reading 5;; P1 0 Yes T 2 . Bipolar” _ TEMP-W3 ‘13 P1 1 Yes _T Bipolar TEMP-W1 'C 1 P1 2 Yes xi .. ,_ jBlpOlar LVDT-225 _Mili|n_ P1 4 Yes . (xi Bipolar“ LVDT-128 7min. P1 6 Yes“ 111 ‘ Bipolar LVDT-3-COMmln. P1 7 Yes _T . Bipolar TEMP-W2 'C CJCIUU-Elm Yes CJC Bipolar .CJCUU-EIO ‘C 013101-02] Yes, 7 CJCW Bipolar . E‘JCUi-UZ ‘C _ 011107-071 Yes CJC Bipolar [311307-07 ‘C v Figure 3-6. DaqViewTM Software Channel Setup Screen Figure 3-7. Spring-Loaded LVDTs (Macro Sensors”) 58 3.4.4 Rigid Support Frame 3.4.4.1 Frame Apparatus Rigid support flames were fabricated based on AASHTO TP604 appendix X.1 “Specimen Measuring Apparatus”. Figure 3-8 shows the rigid support flame. The circular base plate is made of stainless steel and has a diameter of 10 inches. Three semi-spherical support buttons equally spaced around a 2 inch diameter circle are placed on the base plate. The flame height is 10 inches and the vertical rods are made of Invar (a nickel-iron alloy with very low CTE) in order to minimize the effect of flame length changes on the measurements. The side view and plan view of the rigid support flame are shown in Figure 3-9. Invar Vertical Rods Semi-Spherical Supports Base Plate Figure 3-8. Rigid Support Frame 59 Invar Vertical Rods Base Plate @ O Semi-Spherical Supports O O A Figure 3-9. Side View (Left) and Plan View (Right) of the Rigid Support Frame (After AASHTO TP604) l'—'l n A 1' 3.4.4.2 Frame Calibration Expansion of the frame during the test must be accounted for in the CTE calculation. A method for determining a correction factor (CF) based on AASHTO TP604 appendix X.2 “Reference Test for Determination of Correction Factor” was employed. In this method, a calibration specimen with known CTE, having the same measurements as the concrete specimens (cylinders with 4 in. x 7 in. dimensions) is subjected to CTE test. A stainless steel specimen (grade 304) was used in this process. The C1: is defined as CF = ALF / LCS / AT in which AL]: is the length change of the frame, LCS is the length of calibration specimen in room temperature and AT is the temperature change. AL}: is expressed as ALF = ALA - ALM 60 and is the difference between the actual calibration specimen length chance (AL A) and the measured calibration specimen length change (ALM). AL A is defined as ALA=LCS >< ac x AT in which the ac is the known CTE of the calibration specimen. 3.4.5 Test Procedures, Data Collection, and CTE Calculations Two test procedures were followed; AASHTO TP604 procedure and a revised procedure based on TP60 suggested by Won16 which is going to be called “Revised TP60” hereafter. Specimen conditioning and heating-cooling cycle are the same in both procedures. Data collection and CTE calculation however, are different. The CTE test was performed in a way that it satisfied data collection requirements for both procedures. The relevant parts of data were then used to calculate the CTE based on each method. 3.4.5.1 Specimen Conditioning In order to condition the specimens, they were submerged in a saturated limewater bath for at least 48 hours at 73 °F (23 °C). Conditioning was verified by weighing surface- dried specimens at 24-hour intervals. The conditioning criterion was a weight increase of less than 0.5 % between two successive weighings. 3.4.5.2 AASHTO TP60 Test Procedure, Data Collection, and CTE Calculation In this procedure, after the concrete specimen is conditioned, it is subjected to heating, cooling, and temperature equilibrium segments during which the temperature of the 61 surrounding water and displacement of the specimen are monitored. A summary of the procedure is followed. The first step is to place the flame in the water bath and the specimen in the flame. LVDT is then mounted on the flame. Silicon grease is applied to the support buttons and the tip of the LVDT to prevent any sticking to the concrete specimen. The water bath is cooled down to 50 °F (10 °C) and is kept at this temperature until thermal equilibrium of the specimen has been achieved. The thermal equilibrium is denoted by “consistent readings of the LVDT to the nearest 0.00001 in. taken every ten minutes over a one-half hour time period” (AASHTO TP604). The temperature and displacement readings are recorded as initial readings. The water bath is then heated to 122 °F (50 °C) and the same process is followed to record the second readings. The system is cooled again to 50 °F (10 °C) and the final readings are recorded. Recorded readings mentioned above are used in the following computational sequence in order to calculate the CTE value. The CTE of the specimen is calculated by averaging the heating and cooling cycle CTE values providing that the difference between these values does not exceed 0.3 ue/°F (0.5 118/°C). If the CTE values differ more than the specified value, the test has to be repeated until this criterion is satisfied. The CTE equation is expressed as the following. CTE = (CTEHEATING + CTECOOLING) / 2 CTE of the heating or cooling cycle is defined as the actual length change of the specimen (AL ACTU AL) divided by the initial length of the specimen (LINITIAL) over the temperature range (AT) as denoted by the following equation. CTE HEATING or COOLING = (ALACTUAL / LINITIAL) / AT 62 AL ACTU AL is defined as the summation of the measured length change of the specimen (ALSPECIMEN) and the length change of the measuring apparatus (ALAPPARATUS)- ALACTUAL = ALSPECIMEN + ALAPPARATUS The length change of the measuring apparatus is defined as ALAPPARATUS = CF X LINITIAL X AT in which C1: is correction factor of the flame (explained in section 3.4.4.2). 3.4.5.3 Revised TP60 Test Procedure, Data Collection, and CTE Calculation The Revised TP60 procedure is similar to AASHTO TP60 method with regards to specimen conditioning, heating and cooling segments. In this method however, the temperature, specimen displacement, and time are recorded every minute during heating and cooling segments. A summary of the procedure follows. After conditioning and placement of the specimen in the flame inside the water bath, the temperature of the bath is set to 50 °F (10 °C) and temperature, specimen displacement, and time are recorded every minute. The bath temperature is kept at 50 °F (10 °C) for an hour. The same procedure takes place when the temperature is raised to 122 °F (50 °C) and back to 50 °F (10 °C). Recorded readings are then used to plot a temperature versus displacement graph in which heating and cooling data are plotted separately. A typical graph such as the one explained is shown in Figure 3-10. A linear regression analysis is applied between temperature and displacement for the range of 59 °F (15 °C) to 113 °F (45 °C). Won16 stated that temperature gradients inside the specimen are not consistent below and above 63 this range and therefore are not considered in the regression analysis. The R2 of the regression analysis for heating and cooling should be greater than 0.999. CTE of each segment is then calculated using the regression equation. The difference between CTE of each segment must be less than or equal to 0.15 p8/°F (0.3 tie/°C). If the CTE values differ more than this specified value, the test has to be repeated until this criterion is satisfied. Temperature (°F) 41 50 59 68 77 86 95 104 113 122 0.0025 1 I 1 ‘ 1 I ‘ L l A Cooling I Heating —Linear (Cooling) —Linear (Heatingfl 0.0020 4 0.0015 - 0.0010 ~ 0.0005 ~ Displacement (in.) 0.0000 ~ -0.0005 ~ '0-0010 I I I I I I I I 5 10 15 20 25 30 35 40 45 50 Temperature (°C) Figure 3-10. A Typical Revised TP60 Method Graph 3.4.5.4 Executed Test Procedure A test procedure was designed in order to satisfy both AASHTO TP60 and Revised TP60 requirements. Specimens were subjected to heating and cooling cycles between 50 °F and 122 °F (10 °C and 50 °C) and the thermal equilibrium time was one hour between the segments. Several tests with different thermal equilibrium time periods were conducted to 64 establish an optimal time period. Temperature, specimen displacement, and time were recorded continuously throughout the testing period. Relevant parts of the recorded data were used for CTE calculation based on each method. Specimens were subjected to at least three heating-cooling cycles (Figure 3-11). This way, if one cycle was not suitable for CTE calculations due to problems with test conditions (specimen and LVDT misalignment, lack of proper seating of the specimen, etc.), the replicate cycles could be used for CTE calculations. 0.0035 0.0030 - 0.0025 - 0.0020 — 0.0015 a 0.0010 - Displacement (In.) 0.0005 ~ 0.0000 1 -0.0005 -0.0010 . . . . . . . 0 200 400 600 800 1000 1200 1400 Time (Min.) Figure 3—1 1. Three Typical Heating-Cooling Cycles Thermocouples were inserted in water bath to record the water temperature. Thermocouples were also embedded in a number of concrete samples to monitor the specimen temperature during the CTE test. It was found that both the specimen and water follow similar temperature signature, however, the concrete specimen lags the water 65 temperature by approximately 10 minutes. Figure 3-12 shows a typical time-temperature graph. 60 122 501 § I 00 0\ Temperature (°C) L») o l. \1 Temperature (°F) ~68 10 ~50 0 1 1 1 1 1 32 0 50 100 150 200 250 300 Time (Min.) I Concrete Temp. 0 Water Temp. Figure 3-12. A Typical Concrete and Water Temperature Graph 66 CHAPTER 4 RESULTS AND DISCUSSION 4.1 Introduction Results of the laboratory experimental program described in Chapter 3 are documented in this chapter. The summarized results in this chapter include physical properties of aggregate, flesh and hardened properties of concrete, and coefficient of thermal expansion of concrete fabricated using various aggregate types. Furthermore, the statistical and operational (practical) impact of test variables on the magnitude of CTE is presented in this chapter. Two methods of CTE calculation were compared using statistical analysis. The impact of CTE on pavement design and its implications are also discussed. 67 4.2 Physical Properties of Coarse Aggregates The absorption capacity and specific gravity tests (ASTM C127) were conducted on sampled aggregates. For each aggregate type, the aggregate sample was divided into four batches and tests were conducted on each batch. The results were then averaged. The summarized results are presented in Table 4-1. CTE 8 specimens were field-prepared specimens from an actual paving project in Michigan (supplied by the MDOT) and therefore no laboratory test information was available for this mixture. Table 4-1. Physical Properties of Coarse Aggregates - S ecific Gravi (SD)** Mixture Airgge Pit AC * p ty .1. B 1k ID Class Number (SD) Apparent u 1 Bulk Dry SSD . 1.13 2.655 2.591 2.552 [ CTE] “mm” “'47 (0.04) (0.004) (0.033) (0.052) 2.77 2.762 2.637 2.566 / CTE2 Gravel ”'56 (0.11) (0.011) (0.010) (0.011) Dolomitic 0.69 2.698 2.668 2.649 LCTE 3 Limestone 75'“ (0.04) (0.002) (0.004) (0.005) 3.47 2.490 2.393 2.329 [ CTE4 Slag 82‘” (0.12) 0.0440 (0.008) (0.037) . 0.68 2.787 2.753 2.735 / CTE 5 DOIOm‘te 49"” (0.02) (0.001) (0.001) (0.002) Gabbro 0.21 2.928 2.916 2.91 LCTE 6 (Trap Rock) 95‘") (0.01) (0.005) (0.005) (0.006) . 3.13 2.769 2.628 2.548 K CTE 7 DOIOm‘te 58‘” (0.27) (0.009) (0.006) (0.012) / CTE 8 1 Dolomite 91-06 N/A N/A N/A N/A " AC = Absorption Capacity (%). ** SD = Standard Deviation. T SSD = Saturated Surface-Dry. 68 4.3 Fresh Concrete Properties Fresh concrete properties results conducted according to aforementioned standards (Table 3.6) are shown in Table 4-2. The target slump was 3 :1: 0.5 in. and the target air content was 6.5 i 1.5 %. It should be noted that these tests were conducted to make sure that the concrete tested in laboratory is not significantly different from the concrete used in field for paving. However, strict conformance to field parameters was not the goal of this study. CTE 8 specimens were field-prepared specimens from an actual paving project in Michigan and no flesh concrete properties test information was available for this mixture. Table 4-2. Fresh Concrete Properties Mixture ID Test Parameter Slump, inches Air, % Unit Weight, pcf" Temperature, °F CTE 1 3.0 6.0 147.0 54 CTE 2 4.0 5.2 149.4 70 CTE 3 6.0 6.0 145.0 70 CTE 4 3.0 5.8 145.4 77 CTE 5 3.8 4.2 150.8 75 CTE 6 4.0 5.0 152.0 61 CTE 7 3.0 4.9 148.2 69 CTE 8 N/A N/A N/A N/A * pcf = pounds per cubic foot 69 4.4 Hardened Concrete Properties Hardened concrete properties tests were conducted on laboratory cured specimens at 1, 3, 7, 1 4, 28, 90, and 365 days after casting. Average 28-day test results for all mixtures are summarized in Figures 4-1 through 4-4. Figures 4-1 and 4-2 show the average 28-day compressive and flexural strengths respectively. Dashed lines in these figures represent target strengths suggested by MDOT. Figures 4-3 and 4-4 show 28-day elastic modulus and split tensile strength. The error bars in figures 4-1 through 4-4 represent the standard deviation of test values among three replicates. The data used for developing these summary graphs are presented in Appendix A. All concrete batches conformed to average 28-day compressive strength of 3500 psi. The 28-day flexural strength requirement of 650 psi was met for all mixtures except for mixture 3. Two specimens of this mixture met the 650 psi requirement (658 and 666 psi). The third specimen had flexural strength of 612 psi which brought the average to 645 psi. However, this mixture met the requirement at 90 days of age. The hardened concrete property tests were conducted for two reasons: | To evaluate the quality of the concrete ' To be used as level 1 inputs in M-E PDG and HIPERPAV 11 software In general, the delivered concrete met the required specified strengths. 70 28-day compressive strength, psi CTE] CTE2 CTE3 CTE4 CTE5 CTE6 CTE7 CTE8 Mixtrn'e ID Figure 4-1. Average 28-day Compressive Strength Values 1 000 900 — 800 — 700 — 600 — 500 ~ 400 — 300 — 200 - 100 — p 0 ' . ~ 1 28—day flexural strength, psi I l I CTE] CTE2 CTE3 CTE4 CTE5 CTE6 CTE7 Mixture ID Figure 4-2. Average 28—day Flexural Strength Values* * There was no flexural specimen for CT E 8. o. 9 O O I :5 O l 28—day elastic modulus x 10‘, psi N t.» 'o o p—i O l .0 O l CTE] CTE2 CTE3 CTE4 CTE5 CTE6 CTE7 CTE8 MixtureID Figure 4-3. Average 28-day Ela stic Modulus Values 700 8 O 1 28-day split tensile strength, psi CTEl CTE2 CTE3 CTE4 CTE5 CTE6 CTE7 CTE8* Mixtm'e ID Figure 4-4. Average 28-day Split Tensile Values * There was only one split tensile specimen for CTE 8. 72 4.5 Thermal Property The CTE test was conducted on laboratory cured specimens at 3, 7, 14, 28, 90, 180, and 365 days after casting. CTE was calculated based on both the AASHTO TP60 and the Revised TP60 methods. Figure 4.5 shows average 28-day CTE results for each aggregate type based on AASHTO TP60 method. The numbers shown above each aggregate type are typical CTE ranges as reported in the M-E PDG3 . Average 28-day results based on both methods are presented in Table 4.3. 11'5 _ pa/°F 3.4—5.1 6.0-8.7 51-59 445.3 5.1-6.4 6'4 11.0 — (pa/°C (6.1-9.2) 10.8—15.7 (9.2-10.6) (7.9-9.5) (92-115) 2 6.1 10.5 — _ __ 58 10.0 — _ 55 5,9 3(5) 5 . 5.2 a 3 ' — 4.9 1 III 8.5 — III F n — 4.6 p. U 8.0 1' U .0 2 4.3 7.5 — g. 7.0 — .8 ‘ 4-0 "m — 3 7 6.0 ..... 53“ — 3.4 5.5 1 ’4 . 3.1 CTE 1 CTE 3 CTE 2 CTE 4 CTE 6 CTE 8 CTE 7 CTE 5 Mixture ID Figure 4.5 Average 28—day CTE Results The CTE results for each mixture at all ages are presented in Figures 4-6 to 4-13. The data used for computing the summary information are presented in Appendix B. The error bars in these figures show the standard deviation of the test specimens based on three replicates. The dashed lines show the typical CTE ranges for concretes made with that particular aggregate according to M-E PDG3. These ranges are shown in Table 4.4. 73 Table 4.3 Average 28-day CTE Results 28-da CTE, e/°F a/°C Mixture ID y 11 (p. ) AASHTO TP60 Revised TP60 CTE 1 4.54 (8.18) 4.51 (8.12) CTE 2 5.84 (10.52) 5.82 (10.47) CTE 3 4.51 (8.11) 4.53 (8.16) CTE 4 5.71 (10.27) 5.72 (10.29) CTE 5 5.92 (10.65) 5.99 (10.79) CTE 6 5.41 (9.73) 5.44 (9.79) CTE 7 5.90 (10.62) 5.94 (10.69) CTE 8 5.87 (10.57) 6.00 (10.80) Table 44. Typical CTE Ranges for Common Components and Concrete3 Material Coefficient of Concrete Coefficient of T Thermal Thermal Expansion (made ype Expansion, 10'6/°F from this material), 10‘6/°F Aggregates Marbles 2.2-3.9 2.3 Limestones 2.0-3.6 3.4-5.1 ] Granites & Gneisses 3.2-5.3 3.8-5.3 Syenites, Diorites, Andesite, Basalt, Gabbros, 3.0-4.5 4.4-5.3 Diabase [Dolomites 3.9-5.5 5.1-6.4 Blast Furnace Slag 5.1-5.9 Sandstones 5.6-6.7 5.6-6.5 Quartz Sands & Gravels 5.5-7.1 6.0-8.7 [ Quartzite, Cherts 6.1-7.0 6.6-7.1 Cement Paste (saturated) w/c = 0.4 to 0.6 1 10-11 -- Concrete Cores Cores from LTPP pavement -6 -6 -6 sections, many ofwhich N/A 40*10 - 55*10 — 72*10 were used in calibration (Min - Mean - Max) 74 7.5 14 28 180 Time, days 90 —AASHTOTP60 [:1RevisedTP6O — - -Minimum - - - -Maximum Figure 4-6. CTE l (Limestone Concrete) Coefficient of Thermal Expansion 17.5 ~ _ 9.5 16.5 — 15.5 -' """""""""""""""" '1 8.5 14.5 — U 13.5 — — 7.5 m g, 12.5 - a =': 11.5 - - 6.5 .. E 10.5 — ' E. U 9.5 - ’ 5'5 U 8.5 ~ 7.5 _ 4.5 6.5 — — 3.5 5.5 ~ 4.5 4 2.5 14 28 90 180 365 Time, days _ AASHTO TP60 [:3 Revised TP60 — - - Minimum - - - - Maximum Figure 4—7. CTE 2 (Gravel Concrete) Coefficient of Thermal Expansion 75 13.5 7.5 p—n p—s (I! l l O\ U! 1 U: U! CTE, uePC CTE, u£I°F Time, days F-AASHTOTP6OZIRevisedTP6O — ' -Minimum‘ ' ' 'Maximum Figure 4-8. CTE 3 (Dolomitic Limestone Concrete) Coefficient of Thermal Expansion 13.5 v e v—vv e vv—ve vvv‘ 7.5 1 12.5 1 ‘ 11.5 ; i 6.5 10.5 5 7 - - -‘ g L 5.5 g 1 9.5 " _ _ _ _ 1 m“ ‘ m“ 8.5 1 . 8 r 4.5 S 7.5 7‘1 6.5 ~ 1 3.5 5.5 ‘ 4.5 1 e e L 2.5 3 7 14 28 90 180 365 Time, days L— AASHTO TP60 1:1 Revised TP60 — - - Minimum - - - - MaximumJ Figure 4-9. CTE 4 (Slag Concrete) Coefficient of Thermal Expansion 76 13.5 12.5 - 11.5 ~ 10.5 - 9.5 ~ 8.5 7 CTE, paPC 7.5 A 6.5 - 5.5 7 4.5 - 3 7 14 28 Time, days 90 180 365 7.5 —— 2.5 —AASHTOTP60E:RevischP60— ' 'Minimum- - - -Maximum Figure 4-10. CTE 5 (Dolomite Concrete) Coefficient of Thermal Expansion 13.5 12.5 e 11.5 - 10.5 ‘ CTE, u£/°C 28 Time, days 90 180 365 7.5 !— AASHTO TP-60 III Revised TP60 — - - Minimum - - - - Maximumj Figure 4-11. CTE 6 (Gabbro or Trap Rock Concrete) Coefficient of Thermal Expansion 77 13.5 , v 7.5 12.5 e 11.5 e ------------------------------- ” 6-5 10.5 e g — 5.5 9‘; =- 9.5 fl __ - I _ - _ _ - _ _ . 1 “'5 8.5 _ ‘5 5 — 4.5 S 7.5 e 6.5 . - 3.5 5.5 - 4.5 e _. — er . v 2.5 3 7 14 28 90 180 365 Time, days _AASHTOTP60i:IRevisedTP60— - -Minimum- - - Mammy] Figure 4-12. CTE 7 (Dolomite Concrete) Coefficient of Thermal Expansion 13.5 17 'v‘" 77 7 7.5 12.5 7 11.5 i 6.5 10.5 7 g 5.5 g 1 9.5 7 1 H“ - m“ 5 8.5 4.5 5 7.5 7 ‘ 6.5 7 ‘ 35 5.5 7 4.5 7 2.5 7 14 28 90 180 365 Time, days _ AASHFO TP60 :1 Revised TP60 — - - Minimum - - - - Maximum Figure 4-13. CTE 8 (Dolomite Concrete) Coefficient of Thermal Expansion 78 F HWA is conducting a study to determine the variability in CTE test results as well as variability in different CTE devices. As part of this research, a number of specimens were tested at MSU CIL according to AASHTO TP60 protocol. A Grey Cast Iron (grade 410), a concrete specimen made with gravel coarse aggregate, and a concrete specimen made with limestone coarse aggregate were shipped to the laboratory. Physical properties of the coarse aggregates including specific gravity (SG), absorption capacity (AC), and moisture content (MC) are presented in Table 4-5. Table 4—5. Physical Properties of the FHWA Coarse Aggregates Coarse Aggregate SG AC, % MC, % Gravel 2.655 0.83 0.1 Limestone 2.710 0.38 0.1 The test plan required each specimen to be tested twice on two consecutive days. The CTE test results are reported in Table 4-6. Table 4-6. CTE Test Results for F HWA Specimens Material CTE, 118/°F CTE, 118/°C 6.33 1 1.39 Steel 401 6.34 1 1.41 Gravel 6.83 12.29 concrete 6.84 12.32 Limestone 4.06 7.31 Concrete 4.05 7.29 At the time of writing this dissertation, no information about the results from other laboratories is available, and therefore no additional analysis can be conducted at this point. 79 4.6 CTE Test Variability The test variability (5CTE) was determined by subtracting the measured CTE within a batch (i.e. for a given mixture ID and sample age) from the batch mean (deviation). Figure 4-14 illustrates the frequency histogram of 5CTE- Approximately 97% of the data have a SCTE which is between $0.3 118/0F (i0.5 1.13/°C). The coefficient of variation ranges between 2.5% and 6% among different mixtures. These results are based on AASHTO TP60 test method. 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