PLACE IN RETURN BOX to remove this checkout from your record. TO AVOID FINES return on or before date due. MAY BE RECALLED with earlier due date if requested. DATE DUE DATE DUE DATE DUE J9§1°§290§ 11/00 animus-914 ._.,.__ a _ ._____._ _ MODEL FOR PREDICTING APPLICATION TORQUE AND REMOVAL TORQUE OF A CONTINUOUS THREAD CLOSURE By Supachai Pisuchpen A THESIS Submitted to Michigan State University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE 2000 ABSTRACT MODEL FOR PREDICTING APPLICATION TORQUE AND REMOVAL TORQUE OF A CONTINUOUS THREAD CLOSURE By Supachai Pisuchpen Classical engineering mechanics is applied in the analysis of the closure- container system. The basic assumption that the system can be modeled as a rigid-body leads to the TLRD method for determining the static coefficient of friction of a closure-container system (p3, p4) and the predictive models for the application torque and the removal torque. The static coefficients of friction were measured for six closures and seven liners. The discrepancy found between theoretical predictions of torque and experimental results is attributed to the inability of the models to account for the viscoelastic properties of the liner materials as a result of the damping effect. The “f factor” or the sealing force ratio derived from the spring & dashpot model of the liner materials is a good indicator for determining the capability of the liner materials to hold the sealing force. Modifications to the predictive models by incorporating the viscoelastic behavior are suggested. Copyright by SUPACHAI PISUCHPEN 2000 ACKNOWLEDGMENTS As ever, this research wouldn’t be accomplished without encouragement and guidance. I gratefully acknowledge the expertise, valuable advice and tolerance of Dr. Hugh Lockhart, Dr. Gary Burgess, and Dr. Gary Cloud. I also wish to thank Bob Hurwitz who inspired me and gave valuable suggestions in developing the testing device. I heartily thank my parents for their interest, support and encouragement to my judgement in goal of life. Last but not least, I would like to acknowledge this latest of many debts to my beloved wife, Wariya, who temporarily lost a husband to a research. I can not thank her enough for her patience and understanding. TABLE OF CONTENTS LIST OF TABLES ............................................................................... vi LIST OF FIGURES ............................................................................. vii LIST OF ABBREVIATIONS ................................................................... ix 1. INTRODUCTION ........................................................................... 1 2. LITERATURE REVIEW .................................................................. 4 3. MATERIALS AND METHODS .......................................................... 19 4. RESULTS .................................................................................... 42 5. CONCLUSIONS ............................................................................ 57 APPENDIX-RAW DATA TABLES ........................................................... 60 BIBLIOGRAPHY ................................................................................ 124 sew 10. 11. 12. 13. 14. 15. 16. LIST OF TABLES . The Static Coefficient of Friction from Robert V. McCarthy’s Experiment ..... 18 Details of Bottles Used in the Research ........................................................ 19 Details of Closures Used in the Research .................................................... 20 Summary of the Dimension Parameters of Various Treatments Tested ....... 42 Static Coefficient of Friction at the Thread Interface, m, n = 5 ...................... 44 Static Coefficient of Friction at the Liner Interface, Its. n = 5 ......................... 45 Comparison of the Predicted Removal torque, T' and the Measured Removal Torque, ISRT, and lRT ................................................................... 49 Comparison of T‘IT and ISRT/AT, and the “f Factor” or sealing force ratio .. 53 Comparison of T’IT and lRT/AT, and the “f Factor" or sealing force ratio ..... 53 Raw Data of the Static Coefficient of Friction at the Thread Interface ........... 60 Raw Data of the Static Coefficient of Friction at the Liner Interface .............. 90 Raw Data of the Measured Application Torque and Instantaneous Removal Torque ......................................................................................... 1 17 Raw Data of the Measured Application Torque and Immediate Removal Torque ......................................................................................... 1 19 The Predicted Removal Torque, T’ Calculated Using AT from Table 12 ..... 121 The Predicted Removal Torque, T’ Calculated Using AT from Table 13 ..... 121 ka ad kr for Equations (18) and (19) ............................................................ 122 vi LIST OF FIGURES 1. The Most Popular Finish Designs of CT Closure ........................................... 5 2. Standard Code Letters for Continuous Thread Plastic .................................... 6 3. Plastic Container Thread Profiles .................................................................... 8 4. The Structure of F-217 Liner ......................................................................... 13 5. Force Field of Screw Thread ......................................................................... 14 6. Torque-Friction Tester and the Concept ....................................................... 18 7. The Conceptual Design for Measuring the Static Coefficient of Friction of Closure-Container System ............................................................................ 24 8. Free-Body Diagram of the Liner and Finish in Contact ................................. 25 9. Free-Body Diagram of the Closure Thread and Container Thread in Contact ...................................................................................................... 27 10. The Treatments Tested for the Static Coefficient of Friction at the Thread Interface ........................................................................................................ 29 11. The Treatments Tested for the Static Coefficient of Friction at the Liner Interface ........................................................................................................ 3O 12. Free-Body Diagram of the Closure-Container System .................................. 34 13. Relative Magnitude of Torque Contributed by Thread and Liner Factor ....... 35 14. The Spring-Dashpot Model for Liner Materials under Compression ............. 38 15. The “L” and “M” Thread Profiles Obtained from the Unscrewing and Stripping Mold ........................................................................................ 43 16. Comparison of ISRT and T’ ......................................................................... 50 ‘17. Comparison of lRT and T’ ............................................................................ 50 vii 18. Comparison of the “f factor" 10 sec and 15 min after Application ................ 55 viii C.T. TIP TLRD AT RT ISRT lRT Avg Sd LIST OF ABBREVIATIONS Continuous Thread Torque Inch Pounds Top Load/Rotation/Deadweight Loading Application Torque Removal Torque Instantaneous Removal Torque Immediate Removal Torque Average Standard deviation 1. INTRODUCTION A closure system is a mechanical device that seals the contents within a container and can be removed to allow the contents to be dispensed. A closure is applied to the “finish” of a glass, metal, or plastic container. It is an important part of the container in maintaining integrity of the packaging system throughout the entire process of storage, picking and packing. The security of the closure depends upon a number of variables such as resiliency of liner, flatness of seal surface on the container, and the most important; tightness or torque that it is applied. Torque is a moment or twisting resistance that occurs during the application or removal of a closure on a container. Application torque is a measure of closure tightness created by the contact between a closure and a container, whereas removal torque is a measure of the amount of moment or twisting effort necessary to loosen while attempting to open it. The literature review on the prediction of closure torque indicates that there are not many works published in this area. In addition, most of the published research on removal torque has been done on varieties of closure and environment systems rather than development of a predictive model. As a matter of fact, the latter area is as important and challenging as the former for the investigators to unveil the phenomena hidden in the closure during exposure to the environment. This study was initiated to develop a model for predicting torque of a continuous thread closure. The model will deal with forces and moments, and the effects of forces and moments acting on rigid bodies at rest. This study is the first step in developing a more complicated model reflecting the actual conditions to which a closure system is susceptible in the environment. The closure system engaged with a container can be viewed as a mechanical system to clearly understand how it functions to provide a seal protection for the product. The continuous threaded closure-container system is a torque dependent system. The seal is usually accomplished through the use of a liner in a cap which is applied with the proper amount of torque. The liner performs like a gasket to seal around the finish. When the closure is properly applied, the liner is under compression and reacts like a spring to keep the closure thread in contact with the bottle threads and to secure the closure of the container. The closure- container system thus functions through the interaction of many factors which include sealing force, torque and other characteristics of threaded closures. There are two main goals of this study. The first one is to establish the method of determination of two static coefficients of friction; one between thread of closure and thread of container and another between liner and finish of container. This goal is important for developing a predictive model since currently there is no means yet to determine the parameters, and a static coefficient of friction mainly depends on types of material in contact, and types of surface. The second goal is to develop a static model for predicting torque of a continuous thread closure. This development of a predictive model is based on a static equilibrium, which has no movement and deformation; it does not associate with time and environment factors eg. temperature, humidity. In fact, temperature and humidity fluctuations and their extremes in storage and transportation can affect removal torque. In addition, shock and vibration from handling or shipping and compression or top loading from storage also exist and influence closure tightness as well. Understanding this model is very useful for explanation of the translation of torque into sealing force, the effect of friction, and the closure performance. It is expected that the information from this study will be extended to develop a model associated with time and environment factors, which describe the closure-container systems when exposed to actual conditions. 2. LITERATURE REVIEW 1. Continuous thread closure The advent of continuous thread closures arose from a Philadelphian named Espy who conceived the idea of affixing a disc of cork inside the cap so when screwed down on the neck of the jar, the cap brought the cork in compressing contact around the mouth. The Espy patent issued in 1856 could have been a landmark in closure history. However, there were deficiencies in sealing effectiveness of the first design of thread. This brought inventors to consider development in this area. In 1858, John L. Mason was granted patents for his improved thread and improved mold for blowing bottles with threads. His idea was to start a diagonal thread slightly below the top and let it fade away before reaching the shoulder. After this improvement, many materials were used in the closure and bottle industry, accompanied by the continuous improvement of closure design. In 1927, plastic closures were introduced with a promise of freedom of design e.g. colors, textures. As the new technology in resin improvement became available, and more suitable for specific purposes, the variety of products packed with plastic closures drastically increased. In basic principle, the threads of the screw closure engage with corresponding threads molded on the neck of the container; this style offers a mechanical means of generating force for effective sealing. Acceptable mechanical properties and protection can be accomplished by the use of plastic continuous thread closure. Therefore, it has become a principal type of closure. To standardize the dimensions and terms used in the closure industry, the Closure Manufacturers Association has prepared a guide and standard for both metal and plastic closures. By definition, a continuous thread (C.T.) closure has a spiral thread, the design of which is tailored to the container finish and its thread. Hence, a closure is retained on a container by threads that engage corresponding threads of the container. Single lead threads having one thread with a single start are the most common. The size and type of thread are usually designated by the diameter in millimeters coupled with a number which signifies the finish style, such as shallow, deep. Thus 28—400, or sometimes written, 400- 28 means 28 mm in major diameter and a shallow continuous thread. Series designations for the most popular C.T. closures are 400 and 425 for shallow continuous thread designs, 410 for medium CTs, and 415 for tall CTs (Figure 1). Typleal 400 Series MIMI 410 3.11.; typical 415 Series c.r. Closure (:3; Closure III: esure Figure 1. The Most Popular Finish Designs of CT Closure Source: The Closure Manufacturers Association, 1993, Closure Guides A cross section of the continuous thread closure shows the basics of closure construction in Figure 2. ' LINER WELL o—E PITCH HELIX ANGLE I” DRAFT ANGLE THREAD START BOTTOM VI EW Figure 2. Standard Code Letters for Continuous Thread Plastic closures Source: The Closure Manufacturers Association, 1993, Closure Guides where E = Minor diameter of thread E’ MAX = Similar to E, allows for molding draft angle. T = Major diameter of thread T’ MAX = Similar to T, allows for molding draft angle. H = Vertical distance from bottom of closure to the inside top surface [3 = Helix angle PITCH = Vertical distance between corresponding points on adjacent threads. The important closure dimension terms to recognize and understand are defined by the Closure Manufacturers Association in the Closure Guides and described as follows: 1. T dimension, and E dimension. T is the major diameter of the thread on a CT. closure, whereas the minor diameter of the thread on a CT. closure is E. The T and E dimensions are measured at the top of the closure at a point near the end of full thread. 2. H dimension. The vertical distance between the inside top of the closure at the sealing area and the bottom of the skirt excluding any liner (if used), or Iinerless, or any other sealing elements. 3. Helix angle (8). The inclination angle made by the spiral of the thread in relation to the horizontal axis is the helix angle. 4. Pitch. Pitch is the distance from any one point on a closure thread to the corresponding point on the next thread. Thus, pitch is also equal to the inverse of threads per inch. 5. Pressure angle. The angle of the tangent line at the point where the closure thread contacts the finish thread. This is also known as the bearing angle. 6. Threads per inch (T.P.l). T.P.I. is the number of threads in a distance of an inch. It is also equal to 1 divided by pitch. The next issue to be considered in this study is plastic container thread profiles. Although voluntary standards for plastic closure thread profiles have not been developed yet, there are 3 standard container thread profiles (Figure 3). Z—F’RESSI.IRE ANGLE “L” Style “M” Style “P” Style Figure 3. Plastic Container Thread Profiles Source: The Closure Manufacturers Association, 1993, Closure Guides Closure manufacturers have modified these standard container threads into their closure designs along with variations of each. The closure sizes are usually designed in accordance with the finish size of the container. For example, if the finish size of the container has diameter of 28 mm., the 28 mm. diameter of the closure is needed to fit this container. However, the closure thread profiles modified from the container thread profiles have often been used without relation to a specific container finish thread. In Figure 3, L style is designated as an all-purpose thread for either plastic or metal closures and has a symmetrical 30° pressure angle. M style is a modified buttress type with 10° pressure angle which is the preferred style for plastic containers and is used exclusively for this purpose, whereas P style is similar to M style, except it has a full nose radius for use on certain pour-out finishes. Thus, plastic closure thread profiles are designed to fit one of these three container thread profiles. Thermoplastic materials are mostly used in manufacturing C.T. closures. Most often polyolefins (e,g. polypropylene, polyethylene) are used but there is some use of polystyrene. Each of these materials has specific properties that influence the choice of thread profile, and the performance of closure. 1. Polyethylene. PE is available in three densities: LDPE, MDPE, and HDPE. As density increases, the material becomes stiffer, glossier, and harder, and also the tensile strength increases. HDPE is used for manufacturing containers more than for closures. Advantages Limitations a. Flexibility allows for undercuts a. Limited heat resistance b. Remains flexible over wide temperature b. Low abrasion resistance range. c. Low barrier to oils, gases, c. Good moisture and chemical barrier flavors and odors. d. Good processabilty d. Stress cracking e. Heatsealable e. Deforrn under loading, creep f. Wide range of available colors f. May be degraded by UV 9. Variety of surface finishes is possible. Source: The Closure Manufacturers Association, 1993, Closure Guides Polypropylene. PP has unusually high resistance to stress cracking. This is an essential characteristic for hinged closures. In thin hinged sections, it has the quite remarkable property of strengthening with use. Thus, plastic closures are widely made from PP. Advantages Limitations a. Higher heat resistance than PE a. Embrittle at low temperature b. Flexible enough for certain undercuts. b. Limited abrasion and creep resistance 0. Excellent moisture barrier c. Poor gas barrier d. Good chemical resistance d. Limited stress cracking resistance e. Good processabilty e. May be degraded by UV f. Stiffer and harder than PE 9. Vlfide range of available colors h. Low weight per unit volume Source: The Closure Manufacturers Association, 1993, Closure Guides 2. Liner The closure liner, a material that creates a seal between the closure and container, is critical in maintaining the quality of product and the integrity of the seal on the container. The selection of the closure liner on a product-container system can make the difference between the success and failure of a product. The liner is composed of two major parts: a backing and a facing. Compressibility, resiliency, and resealability are provided by the backing, whereas the facing directly contacting a product provides barrier protection. 10 There are variables that should be considered when selecting the closure liner for a certain product (Source: Crawford, Brian, Choosing the Right Closure Liner). These variables can be categorized as follows: 1. Product compatibility. A liner should be compatible with a closure and a product. Basically, liner should be chemically inert to the product and resistant to container’s content in compliance with the FDA regulations. Macroseal. Physically, the liner must compensate for imperfections on the container’s lip and on the closure in order to prevent the leakage of the product. Microseal. This means a seal against small molecules such as water vapor, gas, flavor and odor. Loss of barrier protection characteristics has direct results in product deterioration. Therefore, the loss of these chemical molecules or the entering of environmental components from outside into the container must be impeded. Application and removal torque. They are partly related to the coefficient of friction between thread of closure and thread of container, and between the liner and container finish. Ideally, the amount of friction should facilitate the capper in application and consumer in removal without backing off during transportation. In addition, the torque is also related to compression and tensile stress behavior in container finish, closure and liner. Other considerations. In some applications, particular properties may be needed, for instance, heat resistance, tamperproofing. 11 Materials used for closure liners can be grouped into two categories: homogeneous and heterogeneous composition. The use of a single material in the liner is defined as homogeneous; heterogeneous refers to the incorporation of two or more different materials. Recently, combinations of materials in liners especially extruded polymers have become widely used because new technology allows customizing properties needed from one material and combining with other materials. Some of the commonly used combinations (backing/facing) are: polyethylene/EVAlpolyethylene polyethylene/foamed poIyethylenelpolyethylene polyethylene/foamed EVA/polyethylene high density polyethylene/foamed low density polyethylene lhigh density polyethylene polypropylene/foamed low density poIyethylene/polypropylene acrylonitritelpolyethylene pulp/Saran film pulp/polyvinyl lubricant film pulp/polyethylene coated paper 12 In 1972, F-217 liner was developed by Tri-Seal. This patented seal is a coextruded structure: a low density polyethylene foam core sandwiched between two layers of low density polyethylene film (Figure 4). Identical top-bottom layers of solid Foamed plastic core, plastic protects against product 4 engineered for optimum penetration and evaporation compression and resiliency Figure 4. The Structure of F-217 Liner F-217 is one of the most popular lining materials used in the market. It is a general-purpose liner and is recommended for sealing household, cosmetic, liquor, drug, food, and other products. Pulpboard, a backing material, waxed, coated with vanish, or laminated to plastic films were the first combination materials used for liners. Vanished pulp liners offer good resistance to heat and chemicals, low water-vapor transmission and a glossy appearance, but they tend to be brittle. Therrnoplastics such as vinyl, Saran, and polyethylene are also good choices for laminating or coating on pulp as facing materials. The selection of type of coating is dependent on what protections are needed. For instance, polyethylene is a good moisture protection but inferior in barrier to most gases. So it is not suitable for oxygen-sensitive products. 13 3. Mechanics of the closure-container system To understand the mechanism of how torque is translated into sealing force and the performance of the closure, one must know how the mechanics of screws is adapted into the closure-container system. Since 1856, the continuous thread closure has been in use; unfortunately, there are not many researches in this area published. It is open for more studies to understand the mechanics of the closure-container system. This, with the understanding of the physical behavior of materials under load and the modeling of this behavior will lead to the development of new theory. Robert V. McCarthy (1956) conducted research in determining performance of plastic screw thread attachments. By applying the concept of the inclined plane to screw threads as shown in Figure 5, the equations which describe the relationship between torque and sealing force can be developed. The expressions can be summarized as follows; . 'n ' I A I U § 4 . F. . ' r. 0030.003. * E V A-A g I " W'OI‘ fl " 3m . ’ ‘ ‘ ‘ , eomeer . " 0 mm: l‘n—F I r o: raceeensmo/. )c ""0 . A HELIX ANGLE] ' I 7v Figure 5. Force Field of Screw Thread 14 cosBsina + .cosa T=RL ” (1) cos l9.cos a - ,u.sin a T’ = Fv J. ,ucosa — cos 6. sin a (2) psm a + cos 6. cos a where T = the necessary torque to develop a particular holding or sealing force T’ = the torque required to remove the threaded attachment Fv = the sealing force (axial force) it = the coefficient of friction at the thread interface or = thread helix angle 9 = contact angle In fact, these expressions were originally developed by similar summations of forces and moments of loaded closures in Boomsliter (1945). One limitation of these expressions in predicting removal torque or sealing force effectively is the assumption that all parameters remain constant during loading. In fact, relaxation of the liner material causes the sealing force to decay and must be included in the design of the closure screw thread. McCarthy reported that the relaxation of plastic material associated with the closure skirt amplifies the sealing force decay. The investigator developed further mechanical models to simulate the major relaxation mechanism affecting the observed sealing force decay. The model compared favorably with actual data. This research, however, did not include the effect of liner behavior in the model. Technically, torque depends mostly on the behavior of the closure liner rather 15 than the threads. Therefore, the model does not quite represent the actual static equilibrium of the closure-container system. There is no other research reported in this area since 1956 while the technology in material and packaging machinery has been developing continually. However, there was some research conducted to investigate various effects on the removal torque of closure. Most was conducted by Dr. Lockhart of -'.u--"i ' the School of Packaging at Michigan State University and Dr. Greenway of University of Missouri-Rolla. McCarthy’s research leaves an important aspect of closure-container systems unanswered. As mentioned above on the effect of the liner, this research continues the analysis of the effect of the liner further by using the static equilibrium approach. 4. Coefficient of friction Frictional behavior is important in many packaging applications involving banding of unitized loads, lifting of packages, abrasion or scuffing. In addition, the coefficient of friction plays a major role in the torque of the closure. Friction is a measure of the force that resists the motion of one surface against another surface. Furthermore, the force required to start the object moving is related to the static coefficient of friction, while the kinetic coefficient of friction is related to the force required to maintain motion. Fundamentally, the kinetic coefficient of friction is always less than the static coefficient of friction because force to keep the object moving is less than force to start the object moving. There are many 16 factors affecting the coefficient of friction. They can be classified into two categories. External factors include those such as temperature, velocity of sliding, and load. Internal factors involve nature of the contact surface (smooth or rough), nature of the materials, presence or absence of lubricants. To apply a predictive model in the design of the continuous thread closure, an appropriate value of the static coefficient of friction is necessary. A great variety of instruments have been developed to measure coefficient of friction from a simple inclined plane to complex apparati. Precise values of static coefficient of friction for the application of closures are not currently available for particular plastics on container materials (eg glass, metal, plastics). McCarthy developed a technique to simulate friction conditions for a closure screw thread. The method employed a spring clamp of known k (spring constant) and a closure of the subject material cut to relieve resistance to deformation in one diameter (d) for a distance of at least 0.06” (Figure 6). The jaws of the clamping unit were faced with neoprene. The torque- friction tester was applied to a loose fitting closure. By applying a clamping force generated by the spring, the spring compression force was a direct reading of the radial force applied to the closure. The rotation of torque-friction tester would unscrew a closure from a contact material (bottle), then the torque reading was recorded. The coefficient of friction could be experimentally determined using a relationship of T = p.Fc.d. 17 SPRING! I047 LB/ IN CLOSURE SAMPLE where k = spring constant, lb/in x = displacement, in T = urea where T = torque, TIP p = static coefficient of friction Fc = spring compression force, lb = closure diameter, in Figure 6. Torque-Friction Tester and the Concept The static coefficients at thread interface obtained from McCarthy’s experiment are summarized in Table 1. Table 1. The Static Coefficient of Friction from Robert V. McCarthy’s Experiment Materials in contact ll Polypropylene on glass 0.08 Polystyrene on glass 0.28 Linear low density polyethylene on 0.08 glass 18 3. MATERIALS AND METHODS 1. Materials and instruments 1. The closure-container systems The systems were categorized into 2 groups; 28 mm and 38 mm diameter. Tables 2 and 3 show the details of the bottles and closures tested. Table 2 Details of Bottles Used in This Research Designation Finish size-style, Material Description mm A* 20-410 HDPE Brick red color, round shape, made by Owen-Brockway Plastics & Closures, received 10/1197 B 28-400 HDPE White color, 60 ml volume, square shape, made by Owen-Brockway Plastics & Closures, received 08/25/99 1. Machine #48 2. Mold #5437 3. Product #25-006-024 C 38-400 HDPE White color, 100 ml vol , square shape made by Owen-Brockway Plastics 8. Closures, received 10l8/96 Note: A’ was eliminated from this research because the static coefficient of friction could not be measured using the TLRD method. 19 Table 3 Details of Closures Used in This Research Designation Finish size- Closure Liner material Description style, mm material A1* 20—410 PP PE foam FRST PP WH 7135 PE FM, (F-217) white color, made by Poly-Seal Corporation, received 10/1l97 B1 28-400 PP PE foam Fine rib closure, prod#lot# (OB-Seal) 992526, white color, glued 1. outer cap-Philips HLN-120: (OIP 32699) 2. the lining mat is 0.040 PL- 4025 08 seall lot # 151 171 3. Colorant: white OIC #60110 made by Owen-Illinois, received 1 1/17/99 B2 28-400 PP PE foam Fine rib closure, white color, (OB-Seal) hand lined, non—glued, made by Owen-Illinois, received 1 1/22/99 83 28-400 PP PE foam Fine rib closure, black color, (OB-Seal) hand lined, non-glued, made by Owen-Illinois , received 1 1/22/99 B4 28-400 PP Pulp/Saran(Pl Fine rib closure, black color, SF) hand lined, non-glued, made by Owen-Illinois , received 12I01I99 B5 28-400 PP Pulp/Saran(Pl Fine rib closure, white color, SF) hand lined, non-glued, made by Owen-Illinois , received 12I01l99 20 Table 3 (cont’d) 86 28-400 PP Pulp/Polyvinyl Fine rib closure, black color, lubricant glued, made by Owen-Illinois, film(P/RVTLF) received 11/26/97 B7 28-400 PP Pulp/Polyvinyl Fine rib closure, white color, lubricant hand lined, non-glued, made film(P/RVTLF) by Owen-Illinois, received 1 1/22/99 B8 28-400 PP Pulp/Polyvinyl Fine rib closure, white color, lubricant hand lined, non-glued, made film(P/RVTLF) by Owen-Illinois, received 1 1/22/99 C1 38-400 PP PE foam Fine rib closure, white color, (F-217) glued, made by Poly-Seal Corp, received 11/12/94 C2 38-400 PP PE foam Fine rib closure, white color, (OB-Seal) hand lined, non-glued, made by Owen-Illinois, received 12lO1/99 Note: A* was eliminated from this research because the static coefficient of friction could not be measured using the TLRD method. 2. Secure Pak torque tester electronic model (digital display) 3. Mitutoyo digimetric caliper 4. Bridgeport comparator 5. Clear casting resin and polyester catalyst for making closure specimens for cross-sectional measurement 21 6. An instrument developed for determining the static coefficient of friction of the closure-container systems. 2. Methods 1. Cross-sectional measurement of the closure-container system Duplicate of treatments in Figure 10 applied on the similar diameter containers were tested. A closure was applied on the container with the prescribed application torque of 14 TIP for 28 mm diameter closure and 19 TIP for 38 mm diameter closure. Then a closure-container system was placed upside down into the prepared box 3x3x1.25 inches (the inside surface of the box was covered with pressure sensitive tape). The clear casting resin and the polyester catalyst were thoroughly mixed and poured into the prepared box. This step was performed in the hood. The box was cured in the hood until the casting was completely dry, after which the casting was removed from the box. Finally, the casting was cross-sectioned using a band saw and polished to make a smooth clear surface. The measurements of T, E, l, and the angles a and 0 were made using the optical comparator. On the bottles, the T dimension is the major diameter of the bottle finish including the threads. The E dimension of the bottle is the minor outside diameter of the bottle finish excluding the threads. The diameter at the smallest opening inside the finish is the l dimension. The angle a is the incline angle made by the spiral of the thread in relation to the horizontal plane measured at the mean diameter of the thread interface. Finally, the angle 9 is the contact angle between the closure threads and the container 22 threads measured along the vertical axis. The illustrations of these parameters are shown in Figures 2 and 9a 2. The static coefficient of friction measurement This research began with the use of McCarthy’s concept for measuring the static coefficient of friction at the thread interface. A clamping unit similar to McCarthy’s was fabricated and used. However, the static coefficient of friction measured this way was very dependent on the speed of rotation, either clockwise or counterclockwise. The data obtained were scattered and unrepeatable. The results dictated the development of a better means which is simple, controllable, and repeatable. The method developed in this research allows for measuring the static coefficient of friction at the thread interface, and at the liner interface regardless of the speed of rotation and the twisting direction. The concept of the experimental setup is shown in Figure 7. The closure is attached to a circular plate. The forces applied on both sides of the circular plate are just sufficient to initiate sliding of the closure on the container at the contact point, while the top load exerts a downward force on the closure. This conceptual design was carried on to develop the testing device in Figure 7 which allows placement of a top load on the closure while applying an increasing torque by means of deadweight loading a string and pulley system. For convenience, this device is named Top Load/RotationlDeadweight Loading Device. The short name for it is TLRD. The results show that the method gives repeatable results 23 under various experimental conditions. In general, friction forces involved when two bodies are in contact can be examined by the static equilibrium approach. Beginning with a simple system, a static coefficient of friction between the liner surface and the finish of the container is considered before stepping up to a more complicated system. F. /— Aluminum rod op :oa . A. Figure 7 The Conceptual Design for Measuring the Static Coefficient of Friction of Closure-Container Systems (TLRD Method) To determine the static coefficient of friction at the liner interface, the threads around the container neck have to be eliminated. Thus, the only contact is between the liner and the finish of the container. A free-body diagram showing the forces acting on the liner and finish in contact is given in Figure 8. It shows that the top load F, in Figure 7 vertically pushes the liner surface against the 24 finish of the container, and the normal force F" is the reaction exerted on the liner at the points of contact to balance the force F, shown in Figure 8. Closure L—X Liner Finish \ Figure 8 Free-Body Diagram of the Liner and Finish in Contact These forces are equal but in opposite directions, and are present whenever the bodies are in contact, whether or not there is any tendency for one to slide relative to the other. Thus, a force balance in the vertical direction produces the equation. Zg=q R=E (& When a torque is applied to the closure, there is a tendency for the liner to slide over the finish. The finish exerts frictional forces, fan the liner all around the rim of the container. Za=m (o From symmetry, the net horizontal force created by this distribution is zero (Equation (4)). but the torque is not. Each friction force f can be written as 25 f = pan and F" is the normal force acting at the same point. The torque around the axis of the container created by this frictional force is f F— , where r— is the mean radius from the axis of the container to the finish (Figure 8). Summing torque from all contact points, the required T to start the liner sliding over the finish is T=m££ (6 Solving for Its yields: T . = _. 6 l1. FM. ( ) Equation (6) shows that u, at the liner interface is the ratio of the torque required to initiate sliding to the product of the top load and the mean radius F: . Clearly, if we apply a known load Fv on the liner, and then increase the torque either clockwise or counterclockwise until sliding begins, the static coefficient of friction between liner and finish then can be determined. For instance, if a liner having a diameter of 28 mm (Z = 0.45425 in i 18%) is loaded with FV = 1.32 lb, and the torque required to start the liner sliding is 0.41 TIP 1: 14% , the static coefficient of friction of the liner in contact with the finish is 0.69 i 32%. The next step is to determine the static coefficient of friction between the threads of the closure and threads of the container, which is handled using a similar approach. The threads are assumed to be in continuous contact. A representative contact point is shown in Figure 9a where the closure thread contacts the container thread at some angle 8. The closure spins freely in Figure 26 9a because there is no contact between the liner and finish yet. The experiment was setup this way so that only thread-to-thread friction was involved. A free— body diagram of this system under clockwise torque looking along a radius is depicted in Figure 9b. F V l T in clockwise direction \\‘ FH ‘— container thread p A Figure 9 Free-Body Diagram of the Closure Thread and Container Thread in Contact Solving the equilibrium equations yields the following: ZFy =0, -Fv +Fn cosQ.cosa+y,.Fn.sina=0 (7) where )1: is the static coefficient of friction at the thread interface, a is thread pitch angle, p is thread pitch, and 9 is contact angle looking along the thread. So F, = Fn.(cos 0.cosa + y, sin a) (8) 27 X F, = O, ,u, .Fn.0osa - Fncosflsina — F H = O (9) where FH is the horizontal twisting force applied to the closure by the torque. Rearranging Equation (9) gives: F H = 141.01, .0030: - cosl9.sina) (10) Then the required torque to start clockwise twisting is T = F H .r, (11) where Z is the mean radius at the point of contact. Since Fn and F... are known from Equations (8) and (10), Equation (11) can be written as T=Fv.r,. —[/1I cosa—cos 6.8ma] (12) cos 6.003 a + ,u, sin a The above equation can be related to the thread geometry by substituting for sin 0t and cos on using the triangle shown in Figure 9b: sina = Tami cosa = 2'7” . where I is the length of a thread in one complete revolution and p is the vertical spacing between threads (thread pitch). Then, T = FM: ,u,.2.7r.r, —_cos 0.p (13) cos 6.2.7rJ, + ,u,p Therefore, the static coefficient of friction between the thread of the closure and the thread of the container under clockwise twisting is = 038051121: + Fwy] F2.Fv.2.fl —T.pJ (14) I”: 28 The equation for determining the static coefficient of friction under counterclockwise twisting can be done in a similar manner except that the friction forces are reversed. The result is = cos 9.21127: — F, .p] F2 .F,.2.7r + T.pJ It. (15) Equations (14) and (15) contain closure-container parameters (Z , 0, p)which are readily measured: only T and F, are left to determine 0:. Then if we apply a known load Fv and measure the torque T for starting a closure thread sliding on container thread either clockwise or counterclockwise, pt can be calculated. In addition, ll: should be constant regardless of the twisting direction and the top load chosen. To determine the static coefficient of friction between the thread of the closure and the thread of the container, the closure-container systems selected from Table 2, and 3 were based on the closure diameter, the types of mold, and color. The combinations are presented in Figure 10. 28 mm diameter 38 mm diameter B C L L I I 1 r , I . Unscrewing Stripping Unscrewing Stnpplng mold mold mold mold B1 B6 B2 B4 C1 C2 Figure 10 The Treatments Tested for the Static Coefficient of Friction at the Thread Interface 29 In this research, closures made from different types of mold will have different thread profiles as a result of different contact angle. The unscrewing mold of Figure 10 provides the “L” style thread profile. The threaded cores are unscrewed out of the closures so that precise thread dimensions can be made. In the stripping mold, the closures are stripped off the thread cores and have the “M” style thread profile. In Figure 10, there are 6 different treatments, with 5 runs for each treatment under clockwise and counterclockwise twisting. The series of the top loads used in each run range from 400 g to 2000 g with increments of 200 9. Equations (14) and (15) were used to calculate the static coefficient of friction. The static coefficient of friction between the liner and the finish of the container was also obtained. The combinations of the treatments are shown in Figure 11, also with 5 runs for each treatment. The selection of the treatments was based on the closure diameter, the types of liner, and the method of attaching the liner to the inside of the closure. 28 mm diameter 38 mm diameter B C I l I I I I l 81 82 84 86 87 C1 C2 Figure 11 The Treatments Tested for the Static Coefficient of Friction at the Liner Interface 30 In order to achieve contact only between the liner and the finish of the container, all of the threads all around the neck of the container were eliminated using the grinding and hand sanding tools. Hence, the container was ready for testing in both twisting directions. The top loads used in this case were dependent on the closure diameter and liner type. The loads of 150 g, 200 g, 300 g, 400 g, 600 g, and 800 g were applied to closures containing the 28 mm diameter PE foam liner. Closures containing the 38 mm diameter PE foam liner were loaded with 200 g or 300 g, 400 g, 600 g, and 800 g. The 28 mm diameter paper pulp backing liners were subjected to a series of 600 g, 800 g, 1000 g, 1200 g and 1400 9. Equation (6) was used to calculate the static coefficient of friction at the liner interface. 3. Predictive model. The application of mechanics to the closure-container system can be used to find the friction coefficients us and M separately when either application or removal torque takes place. In actual conditions, when the closure is applied on the container, both p, and p. are involved at the same time. The application torque imposed during application of a closure on the finish of a container is converted to compression of the liner against the finish-sealing surface. The conversion of torque to compression force at the sealing surface is not completely efficient because friction losses occur in the region of the seal as well as in contact area between closure threads and container threads. There are 31 two predictive models derived from the application of mechanics; an application torque model, and a removal torque model. Both models are developed by using an approach similar to that discussed in the coefficient of friction section. Free- body diagrams of the closure-container system under application and removal torque are shown in Figure 12. When the horizontal twisting force F... is applied to the closure by the torque T, the magnitude of the applied torque T is composed of two parts: one from the liner interface and another from the thread interface. At the liner interface, the contribution to the torque is the same as Equation (5), which is repeated here as Equation (16) for reference in this section. T = F,.,u_,..r_, (16) Figure 12a shows that the closure thread is under the container thread at some contact angle 0 which gives a result similar to Equation (13); the contribution to the application torque from thread-to-thread contact is T = Fr; cos6l.p+2Jr.,u,.r, (17) cos/9.2.7”, — ,u,.p Then Equations (16) and (17) are combined to give the total application torque T=Fvlzl::::::;.§’:‘:;zf:.lmil where T = Application torque, (TIP) F, = Sealing force, (lb) p = Thread pitch, (inches) 32 p4 and HS = Coefficient of friction at thread interface, and sealing surface 7, and r— : Mean radius of the thread contact, and sealing surface, (inches) 0 = Contact angle, (degrees) Equation (18) shows that the sealing force during application can also be calculated if the application torque is known. The removal torque is lower than the application torque for mechanical reasons. The predictive model for the removal torque is derived the same way as described above except that the FH and friction forces are reversed as shown in Figures 12d and e. The result is 7": Fr E 21:44.); :cos6l.p 41’s.; (19) cos 0.2.7”, + ,u, . p Equations (18) and (19) are comparable to the McCarthy’s equations. However, substantial differences occur in predicted torques using Equations (18)and (19) are expected due to the liner factor included. Equation (19) shows that the removal torque is composed of two components. They are as follows: F —[ 2.7r.,u, .2- — cos 0.p ,. , _. ] is the contribution produced by frictional restraint 0080.2Jr.r, + ,u,.p between the closure threads and container threads. This will be called the thread factor. 17.71.; is the contribution created by frictional restraint between the face of. the liner and the container finish. This will be called the liner factor. 33 T', Removal torque T, Application torque Via " slat" \ X\\\\ \X\ I \\I‘< l : F? 5—— T, Application torque . .. Closure container “"9" Fv thread f FH F " Finish b Liner H F 7 Closure container thread Finish Figure 12 Free-Body Diagram of the Closure-Container System 34 closure closure If we use typical information of a 28-400 closure and a F-217 liner, then the magnitude of each factor can be computed separately. It will be found that the thread factor accounts for only 18% of total removal torque and the liner factor accounts for about 82% of total torque as shown in Figure 13. Thread factor 1 8% Liner factor 82% Figure 13. Relative Magnitude of Torque Contributed by Thread and Liner Factor Figure 13 shows that the liner factor contributes much more to the removal torque than the threads do. Hence, the selection of the proper liner in relation to the container finish is very important in order to get the desired removal torque. Thread factor determines whether or not the closure threads are self- locking. When a positive removal torque is obtained from the thread factor, the closure thread is said to be self-locking. Thus, the condition for self-locking is 2741,; > cos I9. p (20) Solving for m and relating the thread geometry to or gives p, >cosfltana (21) 35 This relation states that self-locking is obtained whenever the coefficient of friction between closure threads and container threads is greater than the product of the tangent of the thread angle and the cosine of the contact angle. For example, the 28-400 closure-container system has a thread angle 296° and a contact angle 25.75° :I: 19%, which means that in order to obtain self looking, a minimum static coefficient of friction at the thread interface of 0.047 i 19% is needed to achieve this. 4. Sealing force The sealing force is defined as the compression force at the sealing surface resulting from the translation of torque to the vertical force. This is F, in the previous analysis. Currently, there is no easy way to measure this force directly in closure systems. This task is also interesting and challenging for investigators. The sealing force depends on the mechanical properties of the liner. At present, the specification of the tightness of closure-container systems is partly based on the removal torque. Equation (19) shows that if a certain similar removal torque is required on the different closure-container systems, they will have different sealing forces. The sealing force, F, is what pushes the liner on the finish of the container. The removal torque is what needs to be applied to start the various surfaces sliding against friction forces. Therefore, the sealing force is a better indicator of the mechanical seal of the liner than the 36 removal torque. A low sealing force means that the compression force pushing the liner is low, so the mechanical seal protection is weak. The mechanical characteristics of the liner significantly influence the sealing force. The most important of these properties in relation to the sealing force is viscoelasticity. Familiar examples of this behavior are present in many cases involving packaging materials. When foam cushions are used in a drop test, they do not completely return to their original initial thickness. Corrugated boxes also show similar behavior in a compression test. A box under compression will immediately relax if the test is momentarily stopped and never return to its original height after unloading. The concept to remember is that in viscoelastic materials, the force required to compress it is always more than the force required to restrain it during expansion. A model consisting of a spring and a dashpot is useful in conceptualizing the viscoelastic behavior of the liner materials. The spring is considered an ideal solid element obeying Hooke’s law and the dashpot is considered an ideal fluid element. The spring and dashpot can be connected in various ways to portray viscoelastic behavior. The particular combination of these elements used here is shown in Figure 14. 37 F application moving down at I 1 speedv 4 force l (compression) / / / / / / mefim=kx+cv a F force required to restrain it while it 1 moves back up . (removal force) movmg up atspeedv [ j T k c /////77 =kx-cv removal Figure 14 The Spring-Dashpot Concept for the Liner Materials under Compression The force required to compress the liner and then restrain it during removal are expressed in Equations (22) and (23), F applicau'on F nmval =kx+av = k.x — c.v (22) (23) where k is the spring constant, x is the amount of compression, c is the damping constant, and v is the compression rate. At a particular compression x, the ratio of FM”... to Fappncauon is an _ k.x — c.v F Wm,” k.x + c.v < 1 (24) During compression, both the spring and dashpot push up and resist force Fawumn, but during expansion, the spring still pushes up while the dashpot pulls down. Basically, a dashpot acts to make the material want to stay in the shape 38 that it is in, while the spring acts to return it to its original shape. The magnitude of the damping and spring effect is dependent on c, and k respectively. If there is very little damping (low 0 as in metals), then the ratio of Fremova. to Fappucauon is close to 1. At the opposite extreme, If there is a lot of damping (plastics, foams), the ratio is close to 0. The above analogy says that the sealing force Fv in the predictive equations for the application torque is like the applied compression force F in Figure 14a, and F, in the predictive equation for the removal torque is like the restraining force during removal in Figure 14b, which is smaller by some factorf (000 «>00 Q/K°% co” ‘00 %Q QQQ f»? 'b‘Q 'vQ \~ ‘1, Figure 18 Comparison of the “f factor” 10 sec and 15 min after Application Even though the results from the predictive model of the removal torque are an overestimation, the predictive model is still useful because the sealing 55 force during removal can be calculated by this equation. By determining the ratio of the sealing force during removal to the sealing force during application, the “f factor" or the sealing force ratio is obtained. The “f factor” can assist in the selection of the proper liner for the effective sealing from the interpretation previously described. 56 5. CONCLUSIONS The TLRD method utilizing the static equilibrium approach was developed to determine the static coefficient of friction at the thread interface and at the liner interface. This method was validated under various experimental conditions and gave acceptable results. The concept of this method is simple and works well in directly measuring the static coefficient of friction under the practical conditions where the closure and the container are in contact. The static coefficient of friction is an important piece of information for the development of the predictive model. The present predictive model does not fully describe the closure-container system since it does not account for the viscoelastic properties and the function of time. Much work remains to improve the accuracy of predicted results and to make the model more realistic. However, it is still useful in calculating the sealing force during removal which is proposed in this research. The sealing force is a better indicator than the removal torque in determining how good is the seal. The liner is the most important factor in contribution to the removal torque. The spring-dashpot model well describes the liner material behavior under compression. The “f factor” or sealing force ratio deduced from the damping and spring effect in the liner is an essential indicator for determining how good the liner retains the sealing force. The application of the “f factor” shows that the paper pulp liner provides better retention of the sealing force than the PE foam liner after application for 15 min. These results might contradict current belief 57 and practice, but they seem to be valid. The closure-container system thus functions through the interaction of many material properties including the static coefficient of friction, the liner, and other characteristics of threaded closure. Many interesting issues have been found during this research. Future researches should be conducted to compare the use of the removal torque and the sealing force as the indicator for the mechanical seal of the closure-container system. The effects of different thread profiles and geometry of the closure- container system on the mechanical seal also need to be investigated because they are generally present in practical applications. In addition, there are only a few published studies about the characteristics of the liner materials. This area should be scrutinized; especially the mechanical properties of the liner materials as these affect the mechanical seal of the closure-container system. 58 APPENDIX 59 Table 10 Raw Data of the Static Coefficient of Friction at the Thread Interface 8-81 contact m 25.75 degree n= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb Ilcw 400 0.88 6.16 0.01 0.05 0.16 600 1.32 9.16 0.02 0.08 0.16 800 1.76 13.16 0.03 0.12 0.16 1000 2.21 14.66 0.03 0.13 0.15 1200 2.65 18.66 0.04 0.17 0.16 1400 3.09 21.16 0.05 0.19 0.15 1600 3.53 24.66 0.05 0.22 0.16 1800 3.97 28.56 0.06 0.25 0.16 2000 4.41 30.16 0.07 0.27 0.15 Avg 0.16 Sd(n-1) 0.004 n 9 8-81 contact ang 25.75 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CCW 28 mm White F,, g Fv, lb F, g F, lb T, in-lb pom 400 0.88 12.16 0.03 0.11 0.17 600 1.32 18.16 0.04 0.16 0.17 800 1.76 24.16 0.05 0.22 0.17 1000 2.21 32.16 0.07 0.29 0.18 1200 2.65 39.16 0.09 0.35 0.18 1400 3.09 44.16 0.10 0.39 0.17 1600 3.53 48.16 0.11 0.43 0.16 1800 3.97 50.16 0.11 0.45 0.15 2000 4.41 55.66 0.12 0.50 0.15 Avg 0.17 Sd(n-1) 0.012 n 9 60 Table 10 (cont’d) 8-81 contact ang 25.75 degree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CW 28 mm White F... g F,, lb F, g F, lb T, in-lb pm, 400 0.88 8.16 0.02 0.07 0.19 600 1.32 11.66 0.03 0.10 0.19 800 1.76 15.16 0.03 0.14 0.18 1000 2.21 19.16 0.04 0.17 0.18 1200 2.65 22.66 0.05 0.20 0.18 1400 3.09 25.16 0.06 0.22 0.18 1600 3.53 27.16 0.06 0.24 0.17 1800 3.97 30.66 0.07 0.27 0.17 2000 4.41 34.16 0.08 0.30 0.17 Avg 0.18 Sd(n-1) 0.009 n 9 8-81 contact ang 25.75 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CCW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb pm, 400 0.88 16.16 0.04 0.14 0.24 600 1.32 22.16 0.05 0.20 0.21 800 1.76 30.16 0.07 0.27 0.22 1000 2.21 35.16 0.08 0.31 0.20 1200 2.65 41.66 0.09 0.37 0.20 1400 3.09 49.16 0.11 0.44 0.20 1600 3.53 53.16 0.12 0.47 0.19 1800 3.97 41.16 0.09 0.37 0.11 2000 4.41 68.16 0.15 0.61 0.19 Avg 0.20 Sd(n-1) 0.034 n 9 61 Table 10 (cont’d) 8-81 contact ang 25.75 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb new 400 0.88 8.66 0.02 0.08 0.20 600 1.32 12.16 0.03 0.11 0.19 800 1.76 16.16 0.04 0.14 0.19 1000 2.21 19.16 0.04 0.17 0.18 1200 2.65 23.16 0.05 0.21 0.18 1400 3.09 25.16 0.06 0.22 0.18 1600 3.53 27.66 0.06 0.25 0.17 1800 3.97 30.16 0.07 0.27 0.17 2000 4.41 35.16 0.08 0.31 0.17 Avg 0.18 Sd(n—1) 0.012 n 9 8-81 contact an 25.75 degree r.= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CCW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb no“, 400 0.88 15.16 0.03 0.14 0.22 600 1.32 21.16 0.05 0.19 0.20 800 1.76 26.16 0.06 0.23 0.18 1000 2.21 32.16 0.07 0.29 0.18 1200 2.65 38.16 0.08 0.34 0.18 1400 3.09 43.16 0.10 0.39 0.17 1600 3.53 49.66 0.11 0.44 0.17 1800 3.97 58.16 0.13 0.52 0.18 2000 4.41 64.66 0.14 0.58 0.18 Avg 0.18 Sd(n-1) 0.016 n 9 62 Table 10 (cont’d) 8-81 contact ang 25.75 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb new 400 0.88 8.66 0.02 0.08 0.20 600 1.32 12.16 0.03 0.11 0.19 800 1.76 16.16 0.04 0.14 0.19 1000 2.21 19.16 0.04 0.17 0.18 1200 2.65 23.16 0.05 0.21 0.18 1400 3.09 26.16 0.06 0.23 0.18 1600 3.53 30.66 0.07 0.27 0.18 1800 3.97 34.16 0.08 0.30 0.18 2000 4.41 39.16 0.09 0.35 0.19 Avg 0.19 Sd(n-1) 0.007 n 9 8-81 contact ang 25.75 degree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CCW 28 mm White F... g Fv, lb F, g F, lb T, in-lb p.00” 400 0.88 14.66 0.03 0.13 0.21 600 1.32 20.16 0.04 0.18 0.19 800 1.76 25.16 0.06 0.22 0.17 1000 2.21 31.16 0.07 0.28 0.17 1200 2.65 36.16 0.08 0.32 0.17 1400 3.09 41.66 0.09 0.37 0.16 1600 3.53 48.16 0.11 0.43 0.16 1800 3.97 53.66 0.12 0.48 0.16 2000 4.41 61.16 0.13 0.55 0.17 Avg 0.17 Sd(n-1) 0.016 n 9 63 Table 10 (cont’d) 8-81 contact ang 25.75 deglee rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CW 28 mm White F,,, g F,, lb F, g F, lb T, in-Ib pm 400 0.88 8.66 0.02 0.08 0.20 600 1.32 12.66 0.03 0.11 0.20 800 1.76 16.16 0.04 0.14 0.19 1000 2.21 19.66 0.04 0.18 0.19 1200 2.65 23.16 0.05 0.21 0.18 1400 3.09 26.16 0.06 0.23 0.18 1600 3.53 30.16 0.07 0.27 0.18 1800 3.97 34.16 0.08 0.30 0.18 2000 4.41 37.16 0.08 0.33 0.18 Avg 0.19 Sd(n-1) 0.008 n 9 8-81 contact ang 25.75 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CCW 28 mm White Fv, g Fv, lb F, g F, lb T, in-Ib pom 400 0.88 14.16 0.03 0.13 0.20 600 1.32 20.66 0.05 0.18 0.19 800 1.76 26.16 0.06 0.23 0.18 1000 2.21 32.16 0.07 0.29 0.18 1200 2.65 38.16 0.08 0.34 0.18 1400 3.09 43.66 0.10 0.39 0.17 1600 3.53 49.16 0.11 0.44 0.17 1800 3.97 56.16 0.12 0.50 0.17 2000 4.41 62.16 0.14 0.55 0.17 Avg 0.18 Sd(n-1) 0.011 n 9 64 Table 10 (cont’d) 8-82 contact ang 42.25 dggree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CW 28 mm White F,, g F,, lb F, g F, lb T, in-lb Hm 400 0.88 10.16 0.02 0.09 0.19 600 1.32 12.16 0.03 0.11 0.16 800 1.76 17.16 0.04 0.15 0.16 1000 2.21 24.66 0.05 0.22 0.18 1200 2.65 22.66 0.05 0.20 0.15 1400 3.09 29.16 0.06 0.26 0.16 1600 3.53 33.66 0.07 0.30 0.16 1800 3.97 35.16 0.08 0.31 0.15 2000 4.41 47.66 0.11 0.43 0.18 Avg 0.17 Sd(n-1) 0.014 n 9 8—82 contact ang 42.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CCW 28 mm White F,, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 13.66 0.03 0.12 0.16 600 1.32 19.16 0.04 0.17 0.15 800 1.76 29.66 0.07 0.26 0.18 1000 2.21 35.16 0.08 0.31 0.16 1200 2.65 42.66 0.09 0.38 0.17 1400 3.09 56.17 0.12 0.50 0.19 1600 3.53 60.66 0.13 0.54 0.18 1800 3.97 66.66 0.15 0.59 0.17 2000 4.41 77.16 0.17 0.69 0.18 Avg 0.17 Sd(n-1) 0.014 n 9 65 Table 10 (cont’d) 8-82 contact ang 42.25 degree r,= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CW 28 mm White F,, g Fv, lb F, g F, lb T, in-Ib pm 400 0.88 11.16 0.02 0.10 0.20 600 1.32 13.16 0.03 0.12 0.17 800 1.76 12.66 0.03 0.11 0.13 1000 2.21 21.66 0.05 0.19 0.17 1200 2.65 23.16 0.05 0.21 0.15 1400 3.09 27.16 0.06 0.24 0.15 1600 3.53 35.16 0.08 0.31 0.17 1800 3.97 43.66 0.10 0.39 0.18 2000 4.41 55.16 0.12 0.49 0.20 Avg 0.17 Sd(n-1) 0.023 n 9 8-82 contact ang 42.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CCW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb new, 400 0.88 16.16 0.04 0.14 0.19 600 1.32 21.16 0.05 0.19 0.16 800 1.76 24.66 0.05 0.22 0.14 1000 2.21 41 .66 0.09 0.37 0.20 1200 2.65 38.16 0.08 0.34 0.15 1400 3.09 53.16 0.12 0.47 0.18 1600 3.53 59.66 0.13 0.53 0.18 1800 3.97 63.16 0.14 0.56 0.16 2000 4.41 78.66 0.17 0.70 0.19 Avg 0.17 Sd(n-1) 0.021 n 9 66 Table 10 (cont’d) 8-82 contact ang 42.25 degee rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CW 28 mm White Fv, g Fv, lb F, g F, lb T, in-Ib new 400 0.88 10.66 0.02 0.10 0.20 600 1.32 14.66 0.03 0.13 0.18 800 1.76 19.16 0.04 0.17 0.18 1000 2.21 22.66 0.05 0.20 0.17 1200 2.65 22.16 0.05 0.20 0.15 1400 3.09 32.66 0.07 0.29 0.18 1600 3.53 35.16 0.08 0.31 0.17 1800 3.97 36.66 0.08 0.33 0.16 2000 4.41 46.66 0.10 0.42 0.18 Avg 0.17 Sd(n-1) 0.014 n 9 8-82 contact ang 42.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CCW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb How 400 0.88 16.66 0.04 0.15 0.20 600 1.32 25.16 0.06 0.22 0.20 800 1.76 28.16 0.06 0.25 0.16 1000 2.21 37.66 0.08 0.34 0.18 1200 2.65 41.66 0.09 0.37 0.16 1400 3.09 48.66 0.11 0.43 0.16 1600 3.53 59.66 0.13 0.53 0.18 1800 3.97 62.66 0.14 0.56 0.16 2000 4.41 80.66 0.18 0.72 0.19 Avg 0.18 Sd(n-1) 0.017 n 9 67 Table 10 (cont’d) 8-82 contact ang 42.25 degree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CW 28 mm White F,, g Fv, lb F, g F, lb T, in-lb pcw 400 0.88 11.16 0.02 0.10 0.20 600 1.32 10.66 0.02 0.10 0.14 800 1.76 18.16 0.04 0.16 0.17 1000 2.21 20.16 0.04 0.18 0.16 1200 2.65 25.16 0.06 0.22 0.16 1400 3.09 29.16 0.06 0.26 0.16 1600 3.53 36.16 0.08 0.32 0.17 1800 3.97 38.66 0.09 0.35 0.16 2000 4.41 44.66 0.10 0.40 0.17 Avg 0.17 Sd(n-1) 0.016 n 9 8-82 contact ang 42.25 degLee r.= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CCW 28 mm White Fv, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 16.66 0.04 0.15 0.20 600 1.32 25.16 0.06 0.22 0.20 800 1.76 28.16 0.06 0.25 0.16 1000 2.21 37.66 0.08 0.34 0.18 1200 2.65 41.66 0.09 0.37 0.16 1400 3.09 48.66 0.11 0.43 0.16 1600 3.53 59.66 0.13 0.53 0.18 1800 3.97 62.66 0.14 0.56 0.16 2000 4.41 80.66 0.18 0.72 0.19 Avg 0.18 Sd(n-1) 0.017 n 9 68 Table 10 (cont’d) 8-82 contact ang 42.25 degree r¢= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CW 28 mm White Fv, g F,, lb F, g F, lb T, in-lb new 400 0.88 9.66 0.02 0.09 0.18 600 1.32 11.16 0.02 0.10 0.15 800 1.76 21 .66 0.05 0.19 0.20 1000 2.21 23.16 0.05 0.21 0.17 1200 2.65 26.66 0.06 0.24 0.17 1400 3.09 27.66 0.06 0.25 0.15 1600 3.53 39.66 0.09 0.35 0.18 1800 3.97 39.66 0.09 0.35 0.17 2000 4.41 44.66 0.10 0.40 0.17 Avg 0.17 Sd(n—1) 0.015 n 9 8-82 contact ang 42.25 degree r.= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CCW 28 mm White Fv, g F.,, lb F, g F, lb T, in-lb pm 400 0.88 14.66 0.03 0.13 0.17 600 1.32 20.66 0.05 0.18 0.16 800 1.76 25.16 0.06 0.22 0.14 1000 2.21 34.16 0.08 0.30 0.16 1200 2.65 46.16 0.10 0.41 0.18 1400 3.09 54.66 0.12 0.49 0.19 1600 3.53 65.16 0.14 0.58 0.20 1800 3.97 70.66 0.16 0.63 0.19 2000 4.41 77.66 0.17 0.69 0.19 Avg 0.17 Sd(n-1) 0.017 n 9 69 Table 10 (cont'd) 8-84 contact ang 44.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CW 28 mm Black Fv, g F,, lb F, g F, lb T, in-lb llcw 400 0.88 11.66 0.03 0.10 0.20 600 1.32 18.66 0.04 0.17 0.22 800 1.76 22.16 0.05 0.20 0.20 1000 2.21 20.66 0.05 0.18 0.15 1200 2.65 28.16 0.06 0.25 0.17 1400 3.09 27.66 0.06 0.25 0.15 1600 3.53 33.66 0.07 0.30 0.16 1800 3.97 39.16 0.09 0.35 0.16 2000 4.41 48.16 0.11 0.43 0.17 fig 0.18 Sd(n-1) 0.024 n 9 8-84 contact an 44.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CCW 28 mm Black Fv, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 14.66 0.03 0.13 0.17 600 1.32 21.16 0.05 0.19 0.16 800 1.76 27.66 0.06 0.25 0.16 1000 2.21 36.16 0.08 0.32 0.16 1200 2.65 44.16 0.10 0.39 0.17 1400 3.09 49.66 0.11 0.44 0.16 1600 3.53 62.66 0.14 0.56 0.18 1800 3.97 68.66 0.15 0.61 0.18 2000 4.41 73.16 0.16 0.65 0.17 Avg 0.17 Sd(n-1) 0.008 n 9 70 Table 10 (cont’d) 8-84 contact ang 44.25 de49ree r.= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CW 28 mm Black F,, g Fv, lb F, g F, lb T, in-lb pew 400 0.88 10.16 0.02 0.09 0.18 600 1.32 13.16 0.03 0.12 0.16 800 1.76 17.16 0.04 0.15 0.16 1000 2.21 21.16 0.05 0.19 0.16 1200 2.65 25.16 0.06 0.22 0.16 1400 3.09 29.16 0.06 0.26 0.16 1600 3.53 33.16 0.07 0.30 0.16 1800 3.97 39.16 0.09 0.35 0.16 2000 4.41 47.16 0.10 0.42 0.17 Ang 0.16 Sd(n-1) 0.009 n 9 8-84 contact ang 44.25 degiee rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CCW 28 mm Black F,, g Fv, lb F, g F, lb T, in-Ib pm 400 0.88 12.66 0.03 0.11 0.14 600 1.32 24.16 0.05 0.22 0.19 800 1.76 27.66 0.06 0.25 0.16 1000 2.21 34.66 0.08 0.31 0.16 1200 2.65 45.66 0.10 0.41 0.17 1400 3.09 56.16 0.12 0.50 0.19 1600 3.53 59.16 0.13 0.53 0.17 1800 3.97 66.16 0.15 0.59 0.17 2000 4.41 81.16 0.18 0.72 0.19 Avg 0.17 Sd(n-1) 0.017 n ~ 9 71 Table 10 (cont’d) 8-84 contact fl 44.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CW 28 mm Black Fv, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 13.16 0.03 0.12 0.23 600 1.32 16.16 0.04 0.14 0.19 800 1.76 19.16 0.04 0.17 0.17 1000 2.21 24.16 0.05 0.22 0.18 1200 2.65 30.66 0.07 0.27 0.18 1400 3.09 31.16 0.07 0.28 0.16 1600 3.53 32.66 0.07 0.29 0.15 1800 3.97 39.16 0.09 0.35 0.16 2000 4.41 47.16 0.10 0.42 0.17 Avg 0.18 Sd(n-1) 0.021 n 9 8-84 contact ang 44.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CCW 28 mm Black F,,, g Fv, lb F, g F, lb T, in-lb pom 400 0.88 15.66 0.03 0.14 0.18 600 1.32 24.16 0.05 0.22 0.19 800 1.76 31.16 0.07 0.28 0.18 1000 2.21 36.16 0.08 0.32 0.16 1200 2.65 43.16 0.10 0.39 0.16 1400 3.09 60.16 0.13 0.54 0.20 1600 3.53 59.16 0.13 0.53 0.17 1800 3.97 65.66 0.14 0.59 0.17 2000 4.41 78.16 0.17 0.70 0.18 Avg 0.18 Sd(n-1) 0.013 n 9 72 Table 10 (cont’d) 8-84 contact ang 44.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CW 28 mm Black Fv, g Fv, lb F, g F, lb T, in-lb new 400 0.88 7.66 0.02 0.07 0.15 600 1.32 11.66 0.03 0.10 0.15 800 1.76 19.66 0.04 0.18 0.18 1000 2.21 23.66 0.05 0.21 0.17 1200 2.65 27.66 0.06 0.25 0.17 1400 3.09 30.66 0.07 0.27 0.16 1600 3.53 36.66 0.08 0.33 0.17 1800 3.97 38.16 0.08 0.34 0.16 2000 4.41 47.66 0.11 0.43 0.17 Ag 0.16 Sd(n-1) 0.011 n 9 8-84 contact ang 44.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CCW 28 mm Black H. g Fv, lb F, g F, lb T, in-lb pm 400 0.88 17.66 0.04 0.16 0.21 600 1.32 21.16 0.05 0.19 0.16 800 1.76 26.66 0.06 0.24 0.15 1000 2.21 35.66 0.08 0.32 0.16 1200 2.65 41.66 0.09 0.37 0.16 1400 3.09 56.66 0.12 0.51 0.19 1600 3.53 60.66 0.13 0.54 0.17 1800 3.97 67.66 0.15 0.60 0.17 2000 4.41 78.66 0.17 0.70 0.18 Avg 0.17 Sd(n-1) 0.018 n 9 73 Table 10 (cont’d) 8-84 contact ang 44.25 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CW 28 mm Black F,, g Fv, lb F, g F, lb T, in-lb Ilcw 400 0.88 11.16 0.02 0.10 0.20 600 1.32 12.16 0.03 0.11 0.15 800 1.76 18.66 0.04 0.17 0.17 1000 2.21 25.16 0.06 0.22 0.18 1200 2.65 23.66 0.05 0.21 0.15 1400 3.09 31.66 0.07 0.28 0.17 1600 3.53 33.66 0.07 0.30 0.16 1800 3.97 41.66 0.09 0.37 0.17 2000 4.41 46.16 0.10 0.41 0.17 Avg 0.17 Sd(n-1) 0.015 n 9 8-85 contact ang 44.25 degree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CCW 28 mm Black F,, g F,, lb F, g F, lb T, in-lb pm 400 0.88 17.66 0.04 0.16 0.21 600 1.32 19.16 0.04 0.17 0.14 800 1.76 30.16 0.07 0.27 0.17 1000 2.21 33.16 0.07 0.30 0.15 1200 2.65 45.16 0.10 0.40 0.17 1400 3.09 51.66 0.11 0.46 0.17 1600 3.53 60.66 0.13 0.54 0.17 1800 3.97 66.66 0.15 0.59 0.17 2000 4.41 78.66 0.17 0.70 0.18 Avg 0.17 Sd(n-1) 0.019 n 9 74 Table 10 (cont’d) 8-86 contact ang 20 (Legree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CW 28 mm Black Fv. g Fv. lb F, g F, lb T, in-lb pew 400 0.88 6.66 0.01 0.06 0.17 600 1.32 11.66 0.03 0.10 0.19 800 1.76 15.16 0.03 0.14 0.19 1000 2.21 22.66 0.05 0.20 0.22 1200 2.65 20.16 0.04 0.18 0.17 1400 3.09 27.16 0.06 0.24 0.19 1600 3.53 25.16 0.06 0.22 0.17 1800 3.97 30.16 0.07 0.27 0.17 2000 4.41 34.66 0.08 0.31 0.18 Avg 0.18 Sd(n-1) 0.016 n 9 8-86 contact ang 20 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CCW 28 mm Black Fv, g F,, lb F, g F, lb T, in-lb pm 400 0.88 15.16 0.03 0.14 0.23 600 1.32 20.66 0.05 0.18 0.20 800 1.76 25.16 0.06 0.22 0.18 1000 2.21 31.66 0.07 0.28 0.18 1200 2.65 39.66 0.09 0.35 0.19 1400 3.09 44.16 0.10 0.39 0.18 1600 3.53 48.16 0.11 0.43 0.17 1800 3.97 50.16 0.11 0.45 0.16 2000 4.41 55.66 0.12 0.50 0.16 Avg 0.18 Sd(n-1) 0.023 n 9 75 Table 10 (cont’d) 8-86 contact an 20 degree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CW 28 mm Black Fv, g F,, lb F, g F, lb T, in-lb pm 400 0.88 5.16 0.01 0.05 0.14 600 1.32 10.66 0.02 0.10 0.18 800 1.76 14.16 0.03 0.13 0.18 1000 2.21 18.16 0.04 0.16 0.18 1200 2.65 21.16 0.05 0.19 0.18 1400 3.09 22.66 0.05 0.20 0.17 1600 3.53 30.16 0.07 0.27 0.19 1800 3.97 32.16 0.07 0.29 0.18 2000 4.41 35.16 0.08 0.31 0.18 Avg 0.18 Sd(n-1) 0.013 n 9 8-86 contact ang 20 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CCW 28 mm Black Fv, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 16.16 0.04 0.14 0.25 600 1.32 22.16 0.05 0.20 0.22 800 1.76 30.16 0.07 0.27 0.23 1000 2.21 35.16 0.08 0.31 0.21 1200 2.65 41 .66 0.09 0.37 0.21 1400 3.09 49.16 0.11 0.44 0.21 1600 3.53 53.16 0.12 0.47 0.19 1800 3.97 41.16 0.09 0.37 0.12 2000 4.41 68.16 0.15 0.61 0.20 Avg 0.20 Sd(n-1) 0.035 n 9 76 Table 10 (cont’d) 8-86 contact ang 20 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CW 28 mm Black F,, g Fv, lb F, g F, lb T, in-lb pcw 400 0.88 7.16 0.02 0.06 0.18 600 1.32 10.16 0.02 0.09 0.18 800 1.76 14.66 0.03 0.13 0.19 1000 2.21 20.66 0.05 0.18 0.20 1200 2.65 25.66 0.06 0.23 0.21 1400 3.09 20.66 0.05 0.18 0.16 1600 3.53 26.16 0.06 0.23 0.17 1800 3.97 28.16 0.06 0.25 0.17 2000 4.41 31.66 0.07 0.28 0.17 Avg 0.18 Sd(n-1) 0.017 n 9 8-86 contact ang 20 degree rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CCW 28 mm Black Fv, g F,, lb F, g F, lb T, in-lb pm 400 0.88 15.16 0.03 0.14 0.23 600 1.32 21.16 0.05 0.19 0.21 800 1.76 26.16 0.06 0.23 0.19 1000 2.21 32.16 0.07 0.29 0.19 1200 2.65 38.16 0.08 0.34 0.18 1400 3.09 43.16 0.10 0.39 0.18 1600 3.53 49.66 0.11 0.44 0.18 1800 3.97 58.16 0.13 0.52 0.19 2000 4.41 64.66 0.14 0.58 0.19 Avg 0.19 Sd(n-1) 0.016 n 9 77 Table 10 (cont’d) 8-86 contact ang 20 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CW 28 mm Black Fv, g F... lb F, g F, lb T, in-Ib pm, 400 0.88 9.66 0.02 0.09 0.23 600 1.32 12.66 0.03 0.11 0.21 800 1.76 16.66 0.04 0.15 0.20 1000 2.21 16.66 0.04 0.15 0.17 1200 2.65 23.66 0.05 0.21 0.20 1400 3.09 22.16 0.05 0.20 0.17 1600 3.53 26.16 0.06 0.23 0.17 1800 3.97 27.66 0.06 0.25 0.16 2000 4.41 31.66 0.07 0.28 0.17 Avg 0.19 Sd(n-1) 0.023 n 9 8-86 contact an 20 degge rt: 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CCW 28 mm Black F,, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 14.66 0.03 0.13 0.22 600 1.32 20.16 0.04 0.18 0.20 800 1.76 25.16 0.06 0.22 0.18 1000 2.21 31.16 0.07 0.28 0.18 1200 2.65 36.16 0.08 0.32 0.17 1400 3.09 41.66 0.09 0.37 0.17 1600 3.53 48.16 0.11 0.43 0.17 1800 3.97 53.66 0.12 0.48 0.17 2000 4.41 61.16 0.13 0.55 0.18 Avg 0.18 Sd(n-1) 0.016 n 9 78 Table 10 (cont’d) 8-86 contact an 20 degree rt= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CW 28 mm Black Fv, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 5.16 0.01 0.05 0.14 600 1.32 9.16 0.02 0.08 0.16 800 1.76 10.16 0.02 0.09 0.14 1000 2.21 19.16 0.04 0.17 0.19 1200 2.65 20.66 0.05 0.18 0.18 1400 3.09 23.66 0.05 0.21 0.17 1600 3.53 26.66 0.06 0.24 0.17 1800 3.97 31.16 0.07 0.28 0.18 2000 4.41 37.66 0.08 0.34 0.19 Alg 0.17 Sd(n-1) 0.017 n 9 8-86 contact ang 20 cljgree r.= 0.514 in T=1.0755 E= 0.9790 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CCW 28 mm Black Fv, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 14.16 0.03 0.13 0.21 600 1.32 20.66 0.05 0.18 0.20 800 1.76 26.16 0.06 0.23 0.19 1000 2.21 32.16 0.07 0.29 0.19 1200 2.65 38.16 0.08 0.34 0.18 1400 3.09 43.66 0.10 0.39 0.18 1600 3.53 49.16 0.11 0.44 0.18 1800 3.97 56.16 0.12 0.50 0.18 2000 4.41 62.16 0.14 0.55 0.18 Avg 0.19 Sd(n-1) 0.012 n 9 79 Table 10 (cont'd) C-C1 contact an 41.5 degree I}: 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CW 38 mm White F,, g Fv, lb F, g F, lb T, in-lb new 400 0.88 8.16 0.02 0.07 0.12 600 1.32 12.16 0.03 0.11 0.12 800 1.76 14.66 0.03 0.13 0.11 1000 2.21 17.66 0.04 0.16 0.10 1200 2.65 20.16 0.04 0.18 0.10 1400 3.09 23.16 0.05 0.21 0.10 1600 3.53 26.16 0.06 0.23 0.10 1800 3.97 29.66 0.07 0.26 0.10 2000 4.41 32.66 0.07 0.29 0.10 Avg 0.10 Sd(n-1) 0.007 n 9 C-C1 contact ang 41.5 d ree r.= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CCW 38 mm White F... g F,, lb F, g F, lb T, in-lb pm 400 0.88 14.16 0.03 0.13 0.12 600 1.32 19.16 0.04 0.17 0.11 800 1.76 26.16 0.06 0.23 0.11 1000 2.21 33.16 0.07 0.30 0.11 1200 2.65 35.66 0.08 0.32 0.10 1400 3.09 44.16 0.10 0.39 0.11 1600 3.53 53.66 0.12 0.48 0.12 1800 3.97 60.66 0.13 0.54 0.12 2000 4.41 67.16 0.15 0.60 0.12 Agg 0.11 Sd(n-1) 0.007 n 9 80 Table 10 (cont’d) C-C1 contact ang 41.5 degiee rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CW 38 mm White F,, g F,, lb F, g F, lb T, in-lb new 400 0.88 7.66 0.02 0.07 0.11 600 1.32 13.66 0.03 0.12 0.13 800 1.76 16.16 0.04 0.14 0.12 1000 2.21 16.16 0.04 0.14 0.10 1200 2.65 23.66 0.05 0.21 0.11 1400 3.09 27.66 0.06 0.25 0.11 1600 3.53 29.66 0.07 0.26 0.11 1800 3.97 32.66 0.07 0.29 0.11 2000 4.41 32.66 0.07 0.29 0.10 Avg 0.11 Sd(n-1) 0.009 n 9 C-C1 contact an 41.5 degree rt: 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CCW 38 mm White F,, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 14.66 0.03 0.13 0.13 600 1.32 24.16 0.05 0.22 0.14 800 1.76 23.16 0.05 0.21 0.10 1000 2.21 38.66 0.09 0.35 0.14 1200 2.65 37.66 0.08 0.34 0.11 1400 3.09 42.66 0.09 0.38 0.10 1600 3.53 51.66 0.11 0.46 0.11 1800 3.97 65.66 0.14 0.59 0.13 2000 4.41 69.66 0.15 0.62 0.12 Ai 0.12 Sd(n-1) 0.016 n 9 81 Table 10 (cont’d) C-C1 contact ang 41.5 degree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CW 38 mm White Fv, g Fv, lb F, g F, lb T, in-lb pm 400 0.88 5.66 0.01 0.05 0.09 600 1.32 14.16 0.03 0.13 0.13 800 1.76 14.66 0.03 0.13 0.11 1000 2.21 19.66 0.04 0.18 0.11 1200 2.65 19.66 0.04 0.18 0.10 1400 3.09 31.16 0.07 0.28 0.12 1600 3.53 25.16 0.06 0.22 0.10 1800 3.97 31.66 0.07 0.28 0.10 2000 4.41 33.16 0.07 0.30 0.10 Avg 0.11 Sd(n-1) 0.013 n 9 C-C1 contact ang 41.5 degree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CCW 38 mm White F,, g F,,, lb F, g F, lb T, in-lb pm 400 0.88 18.16 0.04 0.16 0.17 600 1.32 22.16 0.05 0.20 0.13 800 1.76 29.66 0.07 0.26 0.13 1000 2.21 31 .66 0.07 0.28 0.11 1200 2.65 34.66 0.08 0.31 0.10 1400 3.09 43.66 0.10 0.39 0.11 1600 3.53 56.66 0.12 0.51 0.12 1800 3.97 63.66 0.14 0.57 0.12 2000 4.41 65.66 0.14 0.59 0.11 Avg 0.12 Sd(n-1) 0.020 n 9 82 Table 10 (cont’d) C-C1 contact ang 41.5 degree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CW 38 mm White F,, g F,, lb F, g F, lb T, in-lb new 400 0.88 8.16 0.02 0.07 0.12 600 1.32 11.66 0.03 0.10 0.11 800 1.76 16.66 0.04 0.15 0.12 1000 2.21 20.66 0.05 0.18 0.12 1200 2.65 15.66 0.03 0.14 0.08 1400 3.09 25.66 0.06 0.23 0.11 1600 3.53 28.66 0.06 0.26 0.11 1800 3.97 32.66 0.07 0.29 0.11 2000 4.41 34.16 0.08 0.30 0.10 Avg 0.11 Sd(n-1) 0.010 n 9 C-C1 contact ang 41.5 degLee rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CCW 38 mm White F.., g F,, lb F, g F, lb T, in-Ib pm 400 0.88 17.16 0.04 0.15 0.15 600 1.32 19.66 0.04 0.18 0.11 800 1.76 23.66 0.05 0.21 0.10 1000 2.21 32.66 0.07 0.29 0.11 1200 2.65 39.66 0.09 0.35 0.11 1400 3.09 45.66 0.10 0.41 0.11 1600 3.53 50.16 0.11 0.45 0.11 1800 3.97 58.16 0.13 0.52 0.11 2000 4.41 66.66 0.15 0.59 0.11 Avg 0.11 Sd(n-1) 0.016 n 9 83 Table 10 (cont’d) C-C1 contact ang 41.5 degree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CW 38 mm White Fv, g F,, lb F, g F, lb T, in-lb new 400 0.88 10.16 0.02 0.09 0.14 600 1.32 8.66 0.02 0.08 0.09 800 1.76 16.66 0.04 0.15 0.12 1000 2.21 17.66 0.04 0.16 0.10 1200 2.65 20.66 0.05 0.18 0.10 1400 3.09 24.16 0.05 0.22 0.10 1600 3.53 26.66 0.06 0.24 0.10 1800 3.97 32.16 0.07 0.29 0.11 2000 4.41 36.66 0.08 0.33 0.11 Avg 0.11 Sd(n-1) 0.013 n 9 C-C1 contact egg 41.5 dggree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CCW 38 mm White Fv, g F,, lb F, g F, lb T, in-lb pm 400 0.88 16.16 0.04 0.14 0.14 600 1.32 21.66 0.05 0.19 0.13 800 1.76 21.66 0.05 0.19 0.09 1000 2.21 30.66 0.07 0.27 0.10 1200 2.65 37.66 0.08 0.34 0.11 1400 3.09 43.66 0.10 0.39 0.11 1600 3.53 56.66 0.12 0.51 0.12 1800 3.97 62.16 0.14 0.55 0.12 2000 4.41 71.66 0.16 0.64 0.12 AVL 0.12 Sd(n-1) 0.017 n 9 84 Table 10 (cont’d) C-C2 contact ang 39.75 degee rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CW 38 mm White Fv, g F... lb F, g F, lb T, in-lb new 400 0.88 8.66 0.02 0.08 0.12 600 1.32 10.66 0.02 0.10 0.11 800 1.76 14.16 0.03 0.13 0.11 1000 2.21 17.16 0.04 0.15 0.10 1200 2.65 20.16 0.04 0.18 0.10 1400 3.09 23.16 0.05 0.21 0.10 1600 3.53 27.16 0.06 0.24 0.10 1800 3.97 30.16 0.07 0.27 0.10 2000 4.41 32.66 0.07 0.29 0.10 Avg 0.11 Sd(n-1) 0.007 n 9 C-CZ contact ang 39.75 degree n= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 1 CCW 38 mm White Fv, g F,, lb F, g F, lb T, in-lb pm, 400 0.88 13.16 0.03 0.12 0.12 600 1.32 18.16 0.04 0.16 0.10 800 1.76 26.66 0.06 0.24 0.12 1000 2.21 33.66 0.07 0.30 0.12 1200 2.65 39.16 0.09 0.35 0.11 1400 3.09 47.16 0.10 0.42 0.12 1600 3.53 48.16 0.11 0.43 0.10 1800 3.97 55.16 0.12 0.49 0.11 2000 4.41 72.16 0.16 0.64 0.13 Avg 0.11 Sd(n-1) 0.009 n 9 85 Table 10 (cont’d) C-C2 contact ang 39.75 degree rt: 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CW 38 mm White F,, g F,, lb F, g F, lb T, in-lb pm, 400 0.88 9.66 0.02 0.09 0.14 600 1.32 10.16 0.02 0.09 0.10 800 1.76 15.66 0.03 0.14 0.12 1000 2.21 20.16 0.04 0.18 0.12 1200 2.65 17.66 0.04 0.16 0.09 1400 3.09 20.66 0.05 0.18 0.09 1600 3.53 25.66 0.06 0.23 0.10 1800 3.97 30.66 0.07 0.27 0.10 2000 4.41 27.16 0.06 0.24 0.09 Avg 0.11 Sd(n-1) 0.015 n 9 C-CZ contact ang 39.75 degree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 2 CCW 38 mm White Fv, g F,, lb F, g F, lb T, in-Ib pm 400 0.88 13.66 0.03 0.12 0.12 600 1.32 20.66 0.05 0.18 0.12 800 1.76 31.66 0.07 0.28 0.14 1000 2.21 31 .66 0.07 0.28 0.11 1200 2.65 41.16 0.09 0.37 0.12 1400 3.09 48.66 0.11 0.43 0.12 1600 3.53 53.16 0.12 0.47 0.12 1800 3.97 55.66 0.12 0.50 0.11 2000 4.41 74.66 0.16 0.67 0.13 Avg 0.12 Sd(n-1) 0.012 n 9 86 Table 10 (cont’d) C-C2 contact ang 39.75 digree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CW 38 mm White Fv, 9 Fe, lb F, g F, lb T, in-lb pm 400 0.88 10.16 0.02 0.09 0.14 600 1.32 11.66 0.03 0.10 0.12 800 1.76 15.66 0.03 0.14 0.12 1000 2.21 18.16 0.04 0.16 0.11 1200 2.65 18.16 0.04 0.16 0.10 1400 3.09 19.16 0.04 0.17 0.09 1600 3.53 29.66 0.07 0.26 0.11 1800 3.97 30.66 0.07 0.27 0.10 2000 4.41 33.66 0.07 0.30 0.10 Avg 0.11 Sd(n-1) 0.015 n 9 C-CZ contact ang 39.75 degee rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 3 CCW 38 mm White Fv, g F,, lb F, g F, lb T, in-lb It,“ 400 0.88 15.16 0.03 0.14 0.14 600 1.32 16.16 0.04 0.14 0.09 800 1.76 26.16 0.06 0.23 0.11 1000 2.21 32.16 0.07 0.29 0.11 1200 2.65 36.16 0.08 0.32 0.10 1400 3.09 51.66 0.11 0.46 0.13 1600 3.53 50.66 0.11 0.45 0.11 1800 3.97 58.66 0.13 0.52 0.11 2000 4.41 70.66 0.16 0.63 0.13 Avg 0.12 Sd(n-1) 0.015 n 9 87 Table 10 (cont'd) C-C2 contact ang 39.75 degree r.= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CW 38 mm White F,, g F,, lb F, g F, lb T, in-lb pcw 400 0.88 8.66 0.02 0.08 0.12 600 1.32 10.66 0.02 0.10 0.11 800 1.76 18.66 0.04 0.17 0.13 1000 2.21 20.66 0.05 0.18 0.12 1200 2.65 20.16 0.04 0.18 0.10 1400 3.09 26.66 0.06 0.24 0.11 1600 3.53 28.16 0.06 0.25 0.11 1800 3.97 28.66 0.06 0.26 0.10 2000 4.41 32.66 0.07 0.29 0.10 Avg 0.11 Sd(n-I) 0.011 n 9 C-CZ contact ang 39.75 degree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 4 CCW 38 mm White F,, g F.,, lb F, g F, lb T, in-lb pm 400 0.88 14.66 0.03 0.13 0.13 600 1.32 20.16 0.04 0.18 0.12 800 1.76 25.66 0.06 0.23 0.11 1000 2.21 34.66 0.08 0.31 0.12 1200 2.65 44.16 0.10 0.39 0.13 1400 3.09 43.16 0.10 0.39 0.11 1600 3.53 50.16 0.11 0.45 0.11 1800 3.97 50.66 0.11 0.45 0.09 2000 4.41 73.66 0.16 0.66 0.13 Avg 0.12 Sd(n-1) 0.013 n 9 88 Table 10 (cont’d) C-CZ contact ang 39.75 degree rt= 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CW 38 mm White Fv, g F,, lb F, g F, lb T, in-lb pm 400 0.88 10.16 0.02 0.09 0.14 600 1.32 10.66 0.02 0.10 0.11 800 1.76 18.66 0.04 0.17 0.13 1000 2.21 18.66 0.04 0.17 0.11 1200 2.65 22.66 0.05 0.20 0.11 1400 3.09 29.66 0.07 0.26 0.12 1600 3.53 28.16 0.06 0.25 0.11 1800 3.97 33.66 0.07 0.30 0.11 2000 4.41 37.16 0.08 0.33 0.11 Avg 0.12 Sd(n-1) 0.012 n 9 C-CZ contact ang 39.75 degree rt: 0.7059 in T=1.4630 E= 1.3605 p= 0.167 in (1 inl6 thrd) d= 4.048 in Run 5 CCW 38 mm White F,, g F,, lb F, g F, lb T, in-Ib pm 400 0.88 13.16 0.03 0.12 0.12 600 1.32 20.16 0.04 0.18 0.12 800 1.76 30.66 0.07 0.27 0.14 1000 2.21 39.66 0.09 0.35 0.14 1200 2.65 46.66 0.10 0.42 0.14 1400 3.09 45.66 0.10 0.41 0.11 1600 3.53 53.16 0.12 0.47 0.12 1800 3.97 54.16 0.12 0.48 0.10 2000 4.41 72.66 0.16 0.65 0.13 Avg 0.12 Sd(n-1) 0.014 n 9 89 Table 11 Raw Data of the Static Coefficient of Friction at the Liner Interface 8-81 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 1 CW 28 mm White PE foam glued Fv, g F,. lb F,g F, lb T, in-lb How 150 03311.66 0.026 0.10 0.69 200 0.441616 0.036 0.14 0.72 300 0.66 23.16 0.051 0.21 0.69 400 0.88 33.16 0.073 0.30 0.74 600 1.32 46.16 0.102 0.41 0.69 800 1.76 68.16 0.150 0.61 0.76 Alg 0.71 Sd(n-1) 0.03 n 6 8-81 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run1 CCW 28 mm White PE foam glued Fv, g Fv. lb F, g F, lb T, in-lb new, 150 03311.16 0.025 0.10 0.66 200 0.441516 0.033 0.14 0.68 300 0.66 22.16 0.049 0.20 0.66 400 0.88 31.16 0.069 0.28 0.69 600 1.32 43.16 0.095 0.39 0.64 800 1.76 63.16 0.139 0.56 0.70 Avg_ 0.67 Sd(n-1) 0.02 n 6 90 Table 11 (cont’d) 8-81 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 2 CW 28 mm White PE foam glued Fv, g F... lb F, g F, lb T, in-lb new 150 0.33 11.66 0.026 0.10 0.69 200 0.44 16.16 0.036 0.14 0.72 300 0.66 23.16 0.051 0.21 0.69 400 0.88 33.16 0.073 0.30 0.74 600 1.32 46.16 0.102 0.41 0.69 800 1.76 68.16 0.150 0.61 0.76 Avg 0.71 Sd(n-1) 0.03 n 6 8-81 E, in 0.979 I, in 0.838 r_.,, in 0.45425 d, in 4.048 Run 2 CCW 28 mm White PE foam glued Fv, g Fv. lb F, g F, lb T, in-lb pm 150 0.33 15.16 0.033 0.14 0.90 200 0.44 20.16 0.044 0.18 0.90 300 0.66 28.16 0.062 0.25 0.84 400 0.88 40.16 0.089 0.36 0.89 600 1.32 48.16 0.106 0.43 0.72 800 1.76 74.16 0.164 0.66 0.83 Av 0.85 Sd(n-1) 0.07 n 6 91 Table 11 (cont’d) 8-81 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 3 CW 28 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pa... 150 0.33 14.16 0.031 0.13 0.84 200 0.44 15.66 0.035 0.14 0.70 300 0.66 25.16 0.055 0.22 0.75 400 0.88 40.16 0.089 0.36 0.89 600 1.32 44.16 0.097 0.39 0.66 800 1.76 70.16 0.155 0.63 0.78 Avg 0.77 Sd(n-1) 0.09 n 6 8-81 E, in 0.979 I, in 0.838 r... in 0.45425 d, in 4.048 Run 3 CCW 28 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pm... 150 0.33 14.16 0.031 0.13 0.84 200 0.44 17.66 0.039 0.16 0.79 300 0.66 25.66 0.057 0.23 0.76 400 0.88 34.16 0.075 0.30 0.76 600 1.32 46.66 0.103 0.42 0.69 800 1.76 73.66 0.162 0.66 0.82 Avg 0.78 Sd(n-1) 0.05 n 6 92 Table 11 (cont’d) 8-81 E, in 0.979 I, in 0.838 r3, in 0.45425 d, in 4.048 Run 4 CW 28 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb In... 150 0.33 12.66 0.028 0.11 0.75 200 0.44 14.66 0.032 0.13 0.65 300 0.66 25.66 0.057 0.23 0.76 400 0.88 34.66 0.076 0.31 0.77 600 1.32 47.16 0.104 0.42 0.70 800 1.76 65.16 0.144 0.58 0.73 ALS 0.73 Sd(n-1) 0.04 n 6 8-81 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 4 CCW 28 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pm... 150 0.33 12.66 0.028 0.11 0.75 200 0.44 19.16 0.042 0.17 0.85 300 0.66 23.66 0.052 0.21 0.70 400 0.88 38.16 0.084 0.34 0.85 600 1.32 47.16 0.104 0.42 0.70 800 1.76 74.66 0.165 0.67 0.83 Avg 0.78 Sd(n-1) 0.07 n 6 93 Table 11 (cont’d) 8-81 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 5 CW 28 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pg... 150 0.33 11.66 0.026 0.10 0.69 200 0.44 20.16 0.044 0.18 0.90 300 0.66 23.66 0.052 0.21 0.70 400 0.88 37.66 0.083 0.34 0.84 600 1.32 48.66 0.107 0.43 0.72 800 1.76 66.66 0.147 0.59 0.74 Avg 0.77 Sd(n-1) 0.08 n 6 8-81 E, in 0.979 I, in 0.838 rs, in 0.45425 d, in 4.048 Run 5 CCW 28 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pm 150 0.33 12.66 0.028 0.11 0.75 200 0.44 17.16 0.038 0.15 0.76 300 0.66 23.66 0.052 0.21 0.70 400 0.88 28.66 0.063 0.26 0.64 600 1.32 42.66 0.094 0.38 0.63 800 1.76 72.66 0.160 0.65 0.81 A19 0.72 Sd(n-1) 0.07 n 6 94 Table 11 (cont’d) 8-82 E, in 0.979 I, in 0.838 rs, in 0.45425 d, in 4.048 Run1 CW 28 mm White PE foam Non-glued F..,g F.,.lb F,g F, lb T, in-lb p... 150 0.33 7.16 0.016 0.06 0.43 200 04410.16 0.022 0.09 0.45 300 0.661516 0.033 0.14 0.45 400 0.88 22.16 0.049 0.20 0.49 600 1.32 33.16 0.073 0.30 0.49 800 1.76 45.66 0.101 0.41 0.51 Avg 0.47 Sd(n-1) 0.03 n 6 8-82 E, in 0.979 I, in 0.838 rs, in 0.45425 d, in 4.048 Run1 CCW 28 mm White PE foam Nomlued F..,g F...lb F,g F, lb T, in-lb pm... 150 0.33 7.16 0.016 0.06 0.43 200 0.441016 0.022 0.09 0.45 300 0.661616 0.036 0.14 0.48 400 0.88 23.16 0.051 0.21 0.52 600 1.32 33.16 0.073 0.30 0.49 800 1.76 46.66 0.103 0.42 0.52 [EL 0.48 Sd(n-1) 0.04 n 6 95 Table 11 (cont’d) 8-82 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 2 CW 28 mm White PE foam Non-glued F..,g F...lb F,g F, lb T, in-lb pm, 150 0.33 9.16 0.020 0.08 0.54 200 0.441216 0.027 0.11 0.54 300 06617.16 0.038 0.15 0.51 400 0.88 23.16 0.051 0.21 0.52 600 1.32 33.16 0.073 0.30 0.49 800 1.76 46.16 0.102 0.41 0.51 Avg 0.52 Sd(n-1) 0.02 n 6 8-82 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 2 CCW 28 mm White PE foam Non-glued F..,g F... lb F,g F, lb T, in-lb pm... 150 0.33 9.66 0.021 0.09 0.57 200 04413.16 0.029 0.12 0.59 300 0.661816 0.040 0.16 0.54 400 0.88 24.16 0.053 0.22 0.54 600 1.32 35.16 0.078 0.31 0.52 800 1.76 47.16 0.104 0.42 0.53 Avg 0.55 Sd(n-1) 0.03 n 6 96 Table 11 (cont’d) 8-82 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 3 CW 28 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-Ib no... 150 0.33 9.16 0.020 0.08 0.54 200 0.44 10.16 0.022 0.09 0.45 300 0.66 17.16 0.038 0.15 0.51 400 0.88 23.16 0.051 0.21 0.52 600 1.32 33.16 0.073 0.30 0.49 800 1.76 46.16 0.102 0.41 0.51 Avg 0.50 Sd(n-1) 0.03 n 6 8-82 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 3 CCW 28 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb pom 150 0.33 7.56 0.017 0.07 0.45 200 0.44 10.66 0.024 0.10 0.47 300 0.66 17.16 0.038 0.15 0.51 400 0.88 22.66 0.050 0.20 0.50 600 1.32 33.16 0.073 0.30 0.49 800 1.76 44.66 0.098 0.40 0.50 Agg 0.49 Sd(n-1) 0.02 n 6 97 Table 11 (cont’d) 8-82 E, in 0.979 I, in 0.838 rs, in 0.45425 d, in 4.048 Run 4 CW 28 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb pm 150 0.33 7.38 0.016 0.07 0.44 200 0.44 11.66 0.026 0.10 0.52 300 0.66 17.16 0.038 0.15 0.51 400 0.88 23.66 0.052 0.21 0.53 600 1.32 32.66 0.072 0.29 0.49 800 1.76 47.16 0.104 0.42 0.53 Pig 0.50 Sd(n-1) 0.03 n 6 8-82 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run 4 CCW 28 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb poo... 150 0.33 8.16 0.018 0.07 0.48 200 0.44 10.16 0.022 0.09 0.45 300 0.66 16.16 0.036 0.14 0.48 400 0.88 23.66 0.052 0.21 0.53 600 1.32 33.16 0.073 0.30 0.49 800 1.76 46.16 0.102 0.41 0.51 Avg 0.49 Sd(n-1) 0.03 n 6 98 Table 11 (cont’d) 8—82 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run5 CW 28 mm White PE foam Non-glued F..,g F...lb F,g F, lb T, in-lb pg... 150 0.33 9.66 0.021 0.09 0.57 200 0.441016 0.022 0.09 0.45 300 06617.16 0.038 0.15 0.51 400 0.88 21.66 0.048 0.19 0.48 600 1.32 32.66 0.072 0.29 0.49 800 1.764566 0.101 0.41 0.51 Avg 0.50 Sd(n-1) 0.04 n 6 8-82 E, in 0.979 I, in 0.838 r,, in 0.45425 d, in 4.048 Run5 CCW 28 mm White PE foam Non-glued ng F...lb F,g F, lb T, in-Ib llacw 150 0.33 8.16 0.018 0.07 0.48 200 04411.66 0.026 0.10 0.52 300 06617.16 0.038 0.15 0.51 400 0.88 21.16 0.047 0.19 0.47 600 1.32 34.16 0.075 0.30 0.51 800 1.76 47.16 0.104 0.42 0.53 Avg 0.50 Sd(n-1) 0.02 n 6 99 Table 11 (cont’d) 8-84 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 1 CW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-lb pg... 600 1.32 11.16 0.025 0.10 0.17 800 1.76 15.16 0.033 0.14 0.17 1000 2.21 18.66 0.041 0.17 0.17 1200 2.65 21.16 0.047 0.19 0.16 1400 3.09 23.16 0.051 0.21 0.15 Avg 0.16 Sd(n-1) 0.01 n 5 8-84 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run1 CCW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-lb pm... 600 1.32 10.66 0.024 0.10 0.16 800 1.76 13.66 0.030 0.12 0.15 1000 2.21 17.16 0.038 0.15 0.15 1200 2.65 20.16 0.044 0.18 0.15 1400 3.09 22.66 0.050 0.20 0.14 Avg 0.15 Sd(n-1) 0.01 n 5 8-84 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run 2 CW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-Ib “C... 600 1.32 10.16 0.022 0.09 0.15 800 1.76 14.66 0.032 0.13 0.16 1000 2.21 20.16 0.044 0.18 0.18 1200 2.65 23.16 0.051 0.21 0.17 1400 3.09 27.16 0.060 0.24 0.17 Avg 0.17 Sd(n-1) 0.01 n 5 100 Table 11 (cont’d) 8-84 E, in 0.979 TS, in 0.45425 l, in 0.838 d, in 4.048 Run 2 CCW 28 mm Black P/SF Non—glued F.., g F... lb F, g F, lb T, in-lb pm 600 1.32 10.16 0.022 0.09 0.15 800 1.76 14.66 0.032 0.13 0.16 1000 2.21 19.66 0.043 0.18 0.18 1200 2.65 23.16 0.051 0.21 0.17 1400 3.09 28.66 0.063 0.26 0.18 Avg 0.17 Sd(n—1) 0.01 n 5 8-84 E, in 0.979 r,, in 0.45425 l, in 0.838 d, in 4.048 Run 3 CW 28 mm Black P/SF Non—glued F.., g F... lb F, g F, lb T, in-lb pg... 600 1.32 10.16 0.022 0.09 0.15 800 1.76 15.16 0.033 0.14 0.17 1000 2.21 19.66 0.043 0.18 0.18 1200 2.65 21.16 0.047 0.19 0.16 1400 3.09 29.66 0.065 0.26 0.19 Avg 0.17 Sd(n-1) 0.01 n 5 8-84 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run 3 CCW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-lb pm... 600 1.32 10.66 0.024 0.10 0.16 800 1.76 14.66 0.032 0.13 0.16 1000 2.21 17.16 0.038 0.15 0.15 1200 2.65 18.16 0.040 0.16 0.13 1400 3.09 22.16 0.049 0.20 0.14 Avg 0.15 Sd(n-1) 0.01 n 5 101 Table 11 (cont’d) 8-84 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run 4 CW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-lb pg... 600 1.32 9.66 0.021 0.09 0.14 800 1.76 13.16 0.029 0.12 0.15 1000 2.21 20.16 0.044 0.18 0.18 1200 2.65 23.66 0.052 0.21 0.18 1400 3.09 21.66 0.048 0.19 0.14 Avg 0.16 Sd(n-1) 0.02 n 5 8-84 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 4 CCW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-lb pm... 600 1.32 10.16 0.022 0.09 0.15 800 1.76 14.66 0.032 0.13 0.16 1000 2.21 19.16 0.042 0.17 0.17 1200 2.65 22.66 0.050 0.20 0.17 1400 3.09 24.66 0.054 0.22 0.16 Avg 0.16 Sd(n-1) 0.01 n 5 8-84 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run 5 CW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-lb pg... 600 1.32 10.66 0.024 0.10 0.16 800 1.76 14.66 0.032 0.13 0.16 1000 2.21 17.66 0.039 0.16 0.16 1200 2.65 21.66 0.048 0.19 0.16 1400 3.09 28.66 0.063 0.26 0.18 Avg 0.16 Sd(n-1) 0.01 n 5 102 Table 11 (cont’d) 8-84 E, in 0.979 r,, in 0.45425 l, in 0.838 d, in 4.048 Run 5 CCW 28 mm Black P/SF Non-glued F.., g F... lb F, g F, lb T, in-Ib pee... 600 1.32 10.66 0.024 0.10 0.16 800 1.76 14.16 0.031 0.13 0.16 1000 2.21 19.16 0.042 0.17 0.17 1200 2.65 19.16 0.042 0.17 0.14 1400 3.09 32.16 0.071 0.29 0.20 Avg 0.17 Sd(n-1) 0.02 n 5 8-86 E, in 0.979 r.., in 0.45425 l, in 0.838 d, in 4.048 Run1 CW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-lb pm, 600 1.32 12.16 0.027 0.11 0.18 800 1.76 15.66 0.035 0.14 0.17 1000 2.21 20.16 0.044 0.18 0.18 1200 2.65 23.16 0.051 0.21 0.17 1400 3.09 27.66 0.061 0.25 0.18 fig 0.18 Sd(n-1) 0.004 n 5 8-86 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run 1 CCW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-lb pm... 600 1.32 11.66 0.026 0.10 0.17 800 1.76 16.16 0.036 0.14 0.18 1000 2.21 20.66 0.046 0.18 0.18 1200 2.65 23.16 0.051 0.21 0.17 1400 3.09 26.66 0.059 0.24 0.17 Avg 0.18 Sd(n-I) 0.01 n 5 103 Table 11 (cont’d) 8-86 E, in 0.979 r,, in 0.45425 l, in 0.838 d, in 4.048 Run 2 CW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-lb pg... 600 1.32 13.16 0.029 0.12 0.20 800 1.76 18.66 0.041 0.17 0.21 1000 2.21 22.16 0.049 0.20 0.20 1200 2.65 25.16 0.055 0.22 0.19 1400 3.09 30.16 0.067 0.27 0.19 Avg 0.20 Sd(n-1) 0.01 n 5 8-86 E, in 0.979 r,, in 0.45425 I, in 0.838 d, in 4.048 Run 2 CCW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-Ib pm 600 1.32 14.16 0.031 0.13 0.21 800 1.76 18.66 0.041 0.17 0.21 1000 2.21 23.16 0.051 0.21 0.21 1200 2.65 25.66 0.057 0.23 0.19 1400 3.09 30.66 0.068 0.27 0.20 Avg 0.20 Sd(n-1) 0.01 n 5 8-86 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 3 CW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-lb us... 600 1.32 12.16 0.027 0.11 0.18 800 1.76 15.66 0.035 0.14 0.17 1000 2.21 21.66 0.048 0.19 0.19 1200 2.65 24.16 0.053 0.22 0.18 1400 3.09 28.16 0.062 0.25 0.18 Avg 0.18 Sd(n-1) 0.01 n 5 104 Table 11 (cont’d) 8-86 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 3 CCW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-lb pm 600 1.32 10.66 0.024 0.10 0.16 800 1.76 15.66 0.035 0.14 0.17 1000 2.21 21.16 0.047 0.19 0.19 1200 2.65 26.16 0.058 0.23 0.19 1400 3.09 26.16 0.058 0.23 0.17 Avg 0.18 Sd(n-1) 0.01 n 5 8-86 E, in 0.979 r,, in 0.45425 l, in 0.838 d, in 4.048 Run 4 CW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-Ib pg... 600 1.32 10.66 0.024 0.10 0.16 800 1.76 16.66 0.037 0.15 0.19 1000 2.21 21.16 0.047 0.19 0.19 1200 2.65 26.16 0.058 0.23 0.19 1400 3.09 27.66 0.061 0.25 0.18 Avg 0.18 Sd(n-1) 0.01 n 5 8-86 E, In 0.979 r.., in 0.45425 l, in 0.838 d, in 4.048 Run 4 CCW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-lb pm... 600 1.32 10.66 0.024 0.10 0.16 800 1.76 15.66 0.035 0.14 0.17 1000 2.21 18.16 0.040 0.16 0.16 1200 2.65 24.16 0.053 0.22 0.18 1400 3.09 27.16 0.060 0.24 0.17 Agvg 0.17 Sd(n-1) 0.01 n 5 105 Table 11 (cont’d) 8-86 E, in 0.979 r,, in 0.45425 l, in 0.838 d, in 4.048 Run 5 CW 28 mm Black PIRVTLF glued F.., g F... lb F, g F, lb T, in-Ib ac... 600 1.32 10.16 0.022 0.09 0.15 800 1.76 14.16 0.031 0.13 0.16 1000 2.21 23.66 0.052 0.21 0.21 1200 2.65 22.66 0.050 0.20 0.17 1400 3.09 25.16 0.055 0.22 0.16 Avg 0.17 Sd(n-1) 0.02 n 5 8-86 E, in 0.979 r,, in 0.45425 l, in 0.838 d, in 4.048 Run 5 CCW 28 mm Black PIRVTLF Glued F.., g F... lb F, g F, lb T, in-lb pom 600 1.32 11.16 0.025 0.10 0.17 800 1.76 17.16 0.038 0.15 0.19 1000 2.21 22.66 0.050 0.20 0.20 1200 2.65 19.66 0.043 0.18 0.15 1400 3.09 29.16 0.064 0.26 0.19 Avg 0.18 Sd(n-1) 0.02 n 5 8-87 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 1 CW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb no... 600 1.32 12.16 0.027 0.11 0.18 800 1.76 17.16 0.038 0.15 0.19 1000 2.21 23.16 0.051 0.21 0.21 1200 2.65 27.16 0.060 0.24 0.20 1400 3.09 30.16 0.067 0.27 0.19 Avg 0.19 Sd(n-1) 0.01 n 5 106 Table 11 (cont’d) 8-87 E, in 0.979 r,, in 0.45425 l, in 0.838 d, in 4.048 Run 1 CCW 28 mm White PIRVTLF Non—glued F.., g F... lb F, g F, lb T, in-lb poo... 600 1.32 11.16 0.025 0.10 0.17 800 1.76 16.16 0.036 0.14 0.18 1000 2.21 21.16 0.047 0.19 0.19 1200 2.65 26.16 0.058 0.23 0.19 1400 3.09 30.16 0.067 0.27 0.19 Avg 0.18 Sd(n-1) 0.01 n 5 8-87 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run 2 CW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb pew 600 1.32 10.66 0.024 0.10 0.16 800 1.76 15.16 0.033 0.14 0.17 1000 2.21 19.16 0.042 0.17 0.17 1200 2.65 22.66 0.050 0.20 0.17 1400 3.09 26.66 0.059 0.24 0.17 Avg 0.17 Sd(n-1) 0.01 n 5 8-87 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 2 CCW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb poo... 600 1.32 10.16 0.022 0.09 0.15 800 1.76 14.66 0.032 0.13 0.16 1000 2.21 18.66 0.041 0.17 0.17 1200 2.65 22.16 0.049 0.20 0.16 1400 3.09 26.16 0.058 0.23 0.17 Avg 0.16 Sd(n-1) 0.01 n 5 107 Table 11 (cont’d) 8-87 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 3 CW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb pg... 600 1.32 13.16 0.029 0.12 0.20 800 1.76 16.66 0.037 0.15 0.19 1000 2.21 19.66 0.043 0.18 0.18 1200 2.65 23.66 0.052 0.21 0.18 1400 3.09 27.66 0.061 0.25 0.18 Avg 0.18 Sd(n-1) 0.01 n 5 8-87 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 3 CCW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb pm 600 1.32 12.16 0.027 0.11 0.18 800 1.76 20.66 0.046 0.18 0.23 1000 2.21 21.66 0.048 0.19 0.19 1200 2.65 25.16 0.055 0.22 0.19 1400 3.09 26.66 0.059 0.24 0.17 Avg 0.19 Sd(n-1) 0.02 n 5 8-87 E, in 0.979 r3, in 0.45425 I, in 0.838 d, in 4.048 Run 4 CW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb pm 600 1.32 11.66 0.026 0.10 0.17 800 1.76 17.66 0.039 0.16 0.20 1000 2.21 19.16 0.042 0.17 0.17 1200 2.65 24.16 0.053 0.22 0.18 1400 3.09 30.16 0.067 0.27 0.19 Avg 0.18 Sd(n-1) 0.01 n 5 108 Table 11 (cont’d) 8-87 E, in 0.979 T... in 0.45425 l, in 0.838 d, in 4.048 Run 4 CCW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb pm 600 1.32 10.66 0.024 0.10 0.16 800 1.76 14.66 0.032 0.13 0.16 1000 2.21 22.66 0.050 0.20 0.20 1200 2.65 25.66 0.057 0.23 0.19 1400 3.09 29.66 0.065 0.26 0.19 Agg 0.18 Sd(n-1) 0.02 n 5 8-87 E, in 0.979 rs, in 0.45425 l, in 0.838 d, in 4.048 Run 5 CW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-lb pg... 600 1.32 13.16 0.029 0.12 0.20 800 1.76 14.16 0.031 0.13 0.16 1000 2.21 20.16 0.044 0.18 0.18 1200 2.65 23.16 0.051 0.21 0.17 1400 3.09 32.66 0.072 0.29 0.21 Avg 0.18 Sd(n-1) 0.02 n 5 8-87 E, in 0.979 rs, in 0.45425 I, in 0.838 d, in 4.048 Run 5 CCW 28 mm White PIRVTLF Non-glued F.., g F... lb F, g F, lb T, in-Ib pm... 600 1.32 10.16 0.022 0.09 0.15 800 1.76 16.16 0.036 0.14 0.18 1000 2.21 20.66 0.046 0.18 0.18 1200 2.65 26.16 0.058 0.23 0.19 1400 3.09 30.66 0.068 0.27 0.20 Avg 0.18 Sd(n-I) 0.02 n 5 109 Table 11 (cont’d) C-C1 E, in 1.3605 r,, in 0.64538 l, in 1.221 d, in 4.048 Run 1 CW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pg... 200 0.44 13.66 0.030 0.12 0.43 300 0.66 19.66 0.043 0.18 0.41 400 0.88 24.66 0.054 0.22 0.39 600 1.32 41.16 0.091 0.37 0.43 800 1.76 52.66 0.116 0.47 0.41 Avg 0.41 Sd(n-1) 0.02 n 5 C-C1 E, in 1.3605 r... in 0.64538 l, in 1.221 d, in 4.048 Run 1 CCW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pm 200 0.44 14.66 0.032 0.13 0.46 300 0.66 21.16 0.047 0.19 0.44 400 0.88 27.16 0.060 0.24 0.43 600 1.32 45.16 0.100 0.40 0.47 800 1.76 60.16 0.133 0.54 0.47 Avg 0.45 Sd(n-1) 0.02 n 5 C-C1 E, in 1.3605 r,, in 0.64538 I, in 1.221 d, in 4.048 Run 2 CW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb new 200 0.44 15.66 0.035 0.14 0.49 300 0.66 22.66 0.050 0.20 0.47 400 0.88 31.16 0.069 0.28 0.49 600 1.32 48.66 0.107 0.43 0.51 800 1.76 62.16 0.137 0.55 0.49 Avg 0.49 Sd(n-1) 0.01 n 5 110 Table 11 (cont’d) C-C1 E, in 1.3605 rs, in 0.64538 l, in 1.221 d, in 4.048 Run 2 CCW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pm... 200 0.44 18.16 0.040 0.16 0.57 300 0.66 26.16 0.058 0.23 0.55 400 0.88 33.16 0.073 0.30 0.52 600 1.32 52.16 0.115 0.47 0.55 800 1.76 66.16 0.146 0.59 0.52 Avg 0.54 Sd(n-1) 0.02 n 5 C-C1 E, in 1.3605 rs, in 0.64538 I, in 1.221 d, in 4.048 Run 3 CW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pm... 200 0.44 18.16 0.040 0.16 0.57 300 0.66 19.16 0.042 0.17 0.40 400 0.88 30.16 0.067 0.27 0.47 600 1.32 46.66 0.103 0.42 0.49 800 1.76 65.16 0.144 0.58 0.51 Avg 0.49 Sd(n-1) 0.06 n 5 C-C1 E, in 1.3605 rs, in 0.64538 l, in 1.221 d, in 4.048 Run 3 CCW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pm 200 0.44 18.66 0.041 0.17 0.59 300 0.66 21.16 0.047 0.19 0.44 400 0.88 31.66 0.070 0.28 0.50 600 1.32 51.16 0.113 0.46 0.53 800 1.76 63.66 0.140 0.57 0.50 Avg 0.51 Sd(n-1) 0.05 n 5 111 Table 11 (cont’d) C-C1 E, in 1.3605 r,, in 0.64538 l, in 1.221 d, in 4.048 Run 4 CW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-lb pa... 200 0.44 14.16 0.031 0.13 0.44 300 0.66 22.66 0.050 0.20 0.47 400 0.88 27.66 0.061 0.25 0.43 600 1.32 43.16 0.095 0.39 0.45 800 1.76 54.66 0.121 0.49 0.43 Agg 0.45 Sd(n—1) 0.02 n 5 C-C1 E, in 1.3605 rs, in 0.64538 I, in 1.221 d, in 4.048 Run 4 CCW 38 mm White PE foam glued F.., g F... lb F, g F, lb T, in-Ib pm... 200 0.44 14.66 0.032 0.13 0.46 300 0.66 17.16 0.038 0.15 0.36 400 0.88 26.16 0.058 0.23 0.41 600 1.32 44.66 0.098 0.40 0.47 800 1.76 70.16 0.155 0.63 0.55 Avg 0.45 Sd(n—1) 0.07 n 5 C-C1 E, in 1.3605 rs, in 0.64538 I, in 1.221 d, in 4.048 Run 5 CW 38 mm White PE foam Glued F.., g F... lb F, g F, lb T, in-lb It“, 200 0.44 17.16 0.038 0.15 0.54 300 0.66 19.16 0.042 0.17 0.40 400 0.88 29.66 0.065 0.26 0.47 600 1.32 38.66 0.085 0.35 0.40 800 1.76 57.16 0.126 0.51 0.45 Avg 0.45 Sd(n-1) 0.06 N 5 112 [I ~.... Table 11 (cont’d) C-C1 E, in 1.3605 rs, in 0.64538 I, in 1.221 d, in 4.048 Run 5 CCW 38 mm White PE foam Glued F.., g F... lb F, g F, lb T, in-lb pm 200 0.44 16.66 0.037 0.15 0.52 300 0.66 20.16 0.044 0.18 0.42 400 0.88 24.66 0.054 0.22 0.39 600 1.32 49.16 0.108 0.44 0.51 800 1.76 66.16 0.146 0.59 0.52 Avg 0.47 Sd(n—1) 0.06 N 5 C-CZ E, in 1.3605 r,, in 0.64538 I, in 1.221 d, in 4.048 Run 1 CW 38 mm White PE foam Norfllued F.., g F... lb F, g F, lb T, in-lb p6... 300 0.66 9.66 0.021 0.09 0.20 400 0.88 12.16 0.027 0.11 0.19 600 1.32 20.16 0.044 0.18 0.21 800 1.76 46.16 0.102 0.41 0.36 1000 2.21 61.16 0.135 0.55 0.38 A3 0.27 Sd(n-1) 0.09 N 5 C-C2 E, in 1.3605 rs, in 0.64538 I, in 1.221 d, in 4.048 Run 1 CCW 38 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb pm... 300 0.66 12.66 0.028 0.11 0.26 400 0.88 19.16 0.042 0.17 0.30 600 1.32 26.16 0.058 0.23 0.27 800 1.76 46.16 0.102 0.41 0.36 1000 2.21 61.16 0.135 0.55 0.38 Avg 0.32 Sd(n-1) 0.05 N 5 113 Table 11 (cont’d) C-CZ E, in 1.3605 r,, in 0.64538 l, in 1.221 d, in 4.048 LRun 2 CW 38 mm White PE foam Non-glued I F.., g F... lb F, g F, lb T, in-lb pg... 300 0.66 18.16 0.040 0.16 0.38 400 0.88 26.16 0.058 0.23 0.41 600 1.32 38.16 0.084 0.34 0.40 800 1.76 48.16 0.106 0.43 0.38 1000 2.21 61.16 0.135 0.55 0.38 Avg 0.39 Sd(n-1) 0.01 n 5 C-CZ E, in 1.3605 rs, in 0.64538 I, in 1.221 d, in 4.048 Run 2 CCW 38 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-Ib aw... 300 0.66 17.16 0.038 0.15 0.36 400 0.88 26.16 0.058 0.23 0.41 600 1.32 40.16 0.089 0.36 0.42 800 1.76 50.16 0.111 0.45 0.39 1000 2.21 62.16 0.137 0.55 0.39 Avgg 0.39 Sd(n-1) 0.02 n 5 C-C2 E, in 1.3605 rs, in 0.64538 l, in 1.221 d, in 4.048 Run 3 CW 38 mm White PE foam Non—glued F.., g F... lb F, g F, lb T, in-lb p.“ 300 0.66 15.16 0.033 0.14 0.32 400 0.88 25.16 0.055 0.22 0.39 600 1.32 36.66 0.081 0.33 0.38 800 1.76 49.16 0.108 0.44 0.39 1000 2.21 61.66 0.136 0.55 0.39 Avg 0.37 Sd(n-1) 0.03 n 5 114 Table 11 (cont’d) C-C2 E, in 1.3605 r,, in 0.64538 I, in 1.221 d, in 4.048 Run 3 CCW 38 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb pm... 300 0.66 16.16 0.036 0.14 0.34 400 0.88 23.16 0.051 0.21 0.36 600 1.32 40.16 0.089 0.36 0.42 800 1.76 46.66 0.103 0.42 0.37 1000 2.21 61.66 0.136 0.55 0.39 Avg 0.37 Sd(n-1) 0.03 n 5 C-CZ E, in 1.3605 rs, in 0.64538 l, in 1.221 d, in 4.048 Run 4 CW 38 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb pg... 300 0.66 15.66 0.035 0.14 0.33 400 0.88 24.16 0.053 0.22 0.38 600 1.32 38.16 0.084 0.34 0.40 800 1.76 46.16 0.102 0.41 0.36 1000 2.21 61.16 0.135 0.55 0.38 Avg 0.37 Sd(n-1) 0.03 n 5 C-C2 E, in 1.3605 rs, in 0.64538 l, in 1.221 d, in 4.048 Run 4 CCW 38 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb pm 300 0.66 18.66 0.041 0.17 0.39 400 0.88 21.66 0.048 0.19 0.34 600 1.32 39.66 0.087 0.35 0.41 800 1.76 46.16 0.102 0.41 0.36 1000 2.21 61.66 0.136 0.55 0.39 Avg 0.38 Sd(n-1) 0.03 n 5 115 Table 11 (cont’d) C-C2 E, in 1.3605 rs, in 0.64538 l, in 1.221 d, in 4.048 Run 5 CW 38 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb pew 300 0.66 17.66 0.039 0.16 0.37 400 0.88 24.16 0.053 0.22 0.38 600 1.32 39.66 0.087 0.35 0.41 800 1.76 48.16 0.106 0.43 0.38 1000 2.21 61.16 0.135 0.55 0.38 Avg 0.38 Sd(n-1) 0.02 n 5 C-C2 E, in 1.3605 rs, in 0.64538 I, in 1.221 d, in 4.048 Run 5 CCW 38 mm White PE foam Non-glued F.., g F... lb F, g F, lb T, in-lb poo... 300 0.66 18.66 0.041 0.17 0.39 400 0.88 23.16 0.051 0.21 0.36 600 1.32 32.66 0.072 0.29 0.34 800 1.76 49.16 0.108 0.44 0.39 1000 2.21 60.16 0.133 0.54 0.38 Avg 0.37 Sd(n-1) 0.02 n 5 116 Table 12 Raw Data of the Measured Application Torque and Instantaneous Removal Torque 8-81 8-82 8-83 Rep AT ISRT Rep AT ISRT Rep AT ISRT 1 13.9 7.1 1 14 12.1 1 14.1 10.6 2 13.9 6.3 2 14.6 11 2 14.4 11.1 3 13.7 7.7 3 14.1 10 3 14.2 10.6 4 13.8 6.5 4 13.9 10.9 4 14.7 10 5 13.9 5.4 5 13.8 11.8 5 13.5 10.7 Avg 13.84 6.6 avg 14.08 11.16 avg 14.18 10.6 Sd 0.09 0.87 sd 0.31 0.83 sd 0.44 0.39 ISRT/AT 0.4769 ISRT/A 0.7926 ISRT/A 0.7475 T T 8-84 8-85 8-86 Rep AT ISRT Rep AT ISRT Rep AT ISRT 1 14 10.8 1 14 13.6 1 13.9 9.7 2 13.8 11.3 2 14 13.4 2 14.3 8.8 3 14.4 11.3 3 14 12.6 3 14.1 10 4 13.9 11.6 4 14.2 11.8 4 14.1 10.7 5 14.4 11.1 5 14.2 12.6 5 14.3 9.6 Avg 14.1 11.22 avg 14.08 12.8 avg 14.14 9.76 so 0.28 0.29 sd 0.11 0.72 sdT 0.17 0.69 . ISRT/AT 0.7957 ISRT/A 0.9091 ISRT/A 0.6902 T T 8-87 8-88 Rep AT ISRT Rep AT ISRT 1 14.2 12.4 1 14.2 12.8 2 14.3 12.9 2 14 11 3 14 13 3 14 12.4 4 14 12.6 4 14.2 10.7 5 14.2 12.8 5 14 10.4 Avg 14.14 12.74 avg 14.08 11.46 Sd 0.13 0.24 sd 0.11 1.07 ISRT/A 0.9010 ISRT/A 0.8139 T T 117 Table 12 (cont’d) C-C1 C-CZ Rep AT ISRT Rep AT ISRT 1 19.2 10.5 1 18.8 16.3 2 19.4 13.1 2 18.9 16.6 3 19.7 13.1 3 18.9 16.3 4 19.2 14.4 4 18.9 16 5 19 10.1 5 19.2 16.2 Avg 19.3 12.24 avg 18.94 16.28 Sd 0.26 1.85 sd 0.15 0.22 ISRT/AT 0.6342 ISRT/A 0.8596 T 118 Table 13 Raw Data of the Measured Application Torque and Immediate Removal Torque 8-81 8-82 8-83 Rep AT lRT Rep AT lRT Rep AT lRT 1 14 5.7 1 14.1 10.1 1 13.8 9.2 2 14 5.8 2 14 9.2 2 13.9 8.7 3 13.8 6.3 3 14.6 9.2 3 13.9 9.1 4 14 7.5 4 13.9 8.7 4 14.4 8.9 5 14 6.5 5 14.2 9.2 5 14.2 9.2 _av_g 13.96 6.36 avgg 14.16 9.28 avg 14.04 9.02 sd 0.09 0.72 sd 0.27 0.51 sd 0.25 0.22 lRT/AT 0.4556 lRT/AT 0.6554 lRT/AT 0.6425 8-84 8-85 8-86 k 0.7387 Rep AT lRT Rep AT lRT Rep AT lRT 1 14 9.3 1 14.1 9.3 1 13.8 9.5 2 14.1 8.1 2 13.9 8 2 14.2 8.4 3 14.2 8 3 13.9 9.5 3 13.8 8.4 4 14.2 8.2 4 13.9 9 4 14.3 8.1 5 14 8.7 5 13.8 9.1 5 14 8.9 avg 14.1 8.46 avg 13.92 8.98 avg 14.02 8.66 E 0.10 0.54 sd 0.11 0.58 sd 0.23 0.55 lRT/AT 0.6000 lRT/AT 0.6451 lRT/AT 0.6177 8-87 8-88 Rep AT lRT Rep AT lRT 1 13.9 10.2 1 13.8 10.5 2 13.7 9.2 2 13.8 10.2 3 13.8 10 3 14 10.7 4 14.1 8.6 4 13.9 8.6 5 13.9 10.6 5 14.3 9.4 a_vg 13.88 9.72 avg 13.96 9.88 sd 0.15 0.81 sd 0.21 0.87 lRT/AT 0.7003 lRT/AT 0.7077 119 Table 13 (cont’d) C-C1 C-CZ Rep AT lRT Rep AT lRT 1 19.4 8.6 1 19.3 12.2 2 19 9.1 2 19.4 13 3 19.4 9.9 3 18.6 12.9 4 18.9 9.1 4 19.7 13.5 5 18.8 9 5 19.3 13.2 2‘19 19.1 9.14 avg 19.26 12.96 sd 0.28 0.47 sd 0.40 0.48 lRT/AT 0.4785 lRT/AT 0.6729 120 Table 14 The Predicted Removal Torque, T Calculated Using AT from Table 12 Rep B-B1 B-BZ B-BS B-B4 B-B5 B-B6 B-B7 B-BB C-C1 C-C2 A 12.29 12.41 12.23 10.50 10.57 10.19 10.55 10.48 16.99 16.44 12.29 12.94 12.32 10.57 10.42 10.49 10.40 10.48 16.64 16.52 12.11 12.50 12.32 10.65 10.42 10.19 10.48 10.63 16.99 15.84 4 12.20 12.32 12.76 10.65 10.42 10.56 10.70 10.55 16.55 16.78 12.29 12.23 12.59 10.50 10.35 10.34 10.55 10.86 16.46 16.44 Avg 12.23 12.48 12.45 10.57 10.44 10.36 10.54 10.60 16.72 16.40 Sd 0.08 0.28 0.22 0.07 0.08 0.17 0.11 0.16 0.25 0.34 Note: T’ :L- 26% Table 15 The Predicted Removal Torque, T’ Calculated Using AT from Table 13 Rep B-B1 B-BZ B-B3 B-B4 B-B5 B-B6 B-B7 B-B8 C-C1 C-CZ 12.37 12.50 12.50 10.50 10.50 10.27 10.78 10.78 16.81 16.01 12.37 12.41 12.76 10.35 10.50 10.56 10.86 10.63 16.99 16.10 12.20 12.94 12.59 10.80 10.50 10.42 10.63 10.63 17.25 16.10 12.37 12.32 13.03 10.42 10.65 10.42 10.63 10.78 16.81 16.10 5 12.37 12.59 11.97 10.80 10.65 10.56 10.78 10.63 16.64 16.35 Avg 12.34 12.55 12.57 10.57 10.56 10.44 10.74 10.69 16.90 16.13 Sd 0.08 0.24 0.39 0.21 0.08 0.12 0.10 0.08 0.23 0.13 Note: T’ i 26% 121 II: Table 16 k.‘ and kr for Equations (18) and (19) Note: ka and kr j: 26% Treatment kal kr 8-81 0.48 0.42 8-82 0.49 0.44 8-83 0.49 0.44 8-84 0.22 0.17 8-85 0.22 0.17 8-86 0.21 0.16 8-87 0.23 0.18 8-88 0.23 0.18 C-C1 0.44 0.38 C-C2 0.37 0.31 122 BIBLIOGRAPHY 123 BIBLIOGRAPHY 1. 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