CHARACTERISTICS AND PREDICTION OF THE LOW TEMPERATURE INDIRECT TENSILE STRENGTHS OF MICHIGAN ASPHALT MIXTURES By Michael Krcmarik A THESIS Submitted to Michigan State University in partial fulfillment of the requirements for the degree of Civil Engineering – Master of Science 2013 ABSTRACT CHARACTERISTICS AND PREDICTION OF THE LOW TEMPERATURE INDIRECT TENSILE STRENGTHS OF MICHIGAN ASPHALT MIXTURES By Michael Krcmarik Thermal cracking is the predominant flexible pavement distress in northern climates, causing transverse cracking perpendicular to the direction of traffic. The indirect tensile (IDT) strength test is currently the most widely used method to characterize thermal cracking susceptibility and is an input to the Pavement ME Design software (formerly known as the Mechanistic- Empirical Design Guide (MEPDG). In Pavement ME Design when laboratory IDT strength testing data is not available to designers it is predicted using mixture volumetrics and performance grade (PG) of the binder. The purpose of this research is to examine the IDT strength characteristics of flexible pavement mixtures commonly used by the Michigan Department of Transportation (MDOT) and to develop improved prediction methods for IDT strength. Laboratory testing of 62 unique MDOT mixtures showed Pavement ME Design software generally over predicted IDT strength. Three models were developed to improve the accuracy of IDT strength prediction. The first model consists of local calibration of the current IDT strength Pavement ME Design predictive model for MDOT mixes. The second model consists of a new statistical model developed based on job mix information to predict low temperature IDT strength. The third model consists of an artificial neural network developed to predict low temperature strength from job mix information. All three models showed increased prediction performance when compared to Pavement ME Design IDT strength prediction. With these models, a more accurate low temperature prediction of IDT strength is available to pavement designers in Michigan using readily available job mix information. TABLE OF CONTENTS LIST OF TABLES .......................................................................................................................... v LIST OF FIGURES ....................................................................................................................... vi 1. INTRODUCTION ...................................................................................................................... 1 1.1 Objective................................................................................................................................ 3 1.2 Outline ................................................................................................................................... 3 2. LITERATURE REVIEW ........................................................................................................... 4 2.1 Motivation ............................................................................................................................. 4 2.2 Background of the Indirect Tensile Strength Test ................................................................ 4 2.3 Current Indirect Tensile Strength Testing Procedure ............................................................ 7 2.4 Calculation of Indirect Tensile Strength According to AASHTO T-322 ........................... 10 2.5 Calculation of Indirect Tensile Strength without Deformation Monitoring........................ 11 2.6 Determination of Fracture Work from Indirect Tensile Strength Testing........................... 12 2.7 Relevance of Indirect Tensile Strength to Pavement ME Design ....................................... 14 2.8 Pavement ME Design IDT Strength Prediction .................................................................. 16 2.9 Factors Affecting Mixture Indirect Tensile Strength .......................................................... 17 3. METHODS ............................................................................................................................... 19 3.1 Introduction ......................................................................................................................... 19 3.2 Mixtures Used ..................................................................................................................... 19 3.3 Specimen Preparation .......................................................................................................... 23 3.4 Indirect Strength Testing Procedures .................................................................................. 24 3.4.1 Testing Temperature ..................................................................................................... 24 3.4.2 Use of LVDTs .............................................................................................................. 24 3.4.3 Environmental Chamber ............................................................................................... 25 4. RESULTS OF LABORATORY INDIRECT TENSILE TESTING ........................................ 27 4.1 Indirect Tensile Strength of Michigan Mixtures ................................................................. 27 4.2 Fracture Work of Michigan Mixtures ................................................................................. 30 4.3 MDOT Mix Designation and IDT Strength ........................................................................ 38 4.4 Superpave PG and IDT Strength ......................................................................................... 40 4.5 Warm Mix Asphalt IDT Properties ..................................................................................... 44 5. INDIRECT TENSILE STRENGTH PREDICTION MODELS............................................... 47 5.1 Introduction to Indirect Tensile Strength Prediction for Pavement ME Design ................. 47 5.2 Model Evaluation ................................................................................................................ 49 5.3 Local Calibration of Pavement ME Design Strength Prediction Model ............................. 50 5.4 Linear Strength Prediction Model ....................................................................................... 55 5.5 Artificial Neural Network Prediction Model ...................................................................... 62 5.5.1 Structure of the IDT Strength ANN ............................................................................. 63 5.5.2 Overview of IDT Strength Prediction with the ANN ................................................... 63 iii 5.5.2 Training of the IDT Strength ANN .............................................................................. 65 5.5.3 Testing of the IDT Strength ANN ................................................................................ 68 6. CONCLUSIONS AND RECOMMENDATIONS ................................................................... 70 APPENDICES .............................................................................................................................. 72 APPENDIX A: MIX PROPERTIES AND VOLUMETRICS OF MIXTURES TESTED ...... 73 APPENDIX B: IDT STRENGTH, FRACTURE WORK, AND VOLUMTERICS OF SPECIMENS TESTED ............................................................................................................. 85 REFERENCES ........................................................................................................................... 102 iv LIST OF TABLES Table 1 HMAs tested for IDT strength ......................................................................................... 20 Table 2 HMAs tested for IDT strength (GGSP and LVSP Mixtures) .......................................... 22 Table 3 HMAs tested for IDT strength (SUPERPAVE) – Mixtures that do not follow MDOT specifications but are permitted to be used ................................................................................... 23 Table 4 HMAs tested for IDT strength (GGSP and LVSP Mixtures) - Mixtures that do not follow MDOT specifications but are permitted to be used ...................................................................... 23 Table 5 Summary of IDT strength values for the State of Michigan asphalt mixtures ................ 28 Table 6 Summary of total work values for the State of Michigan asphalt mixtures .................... 31 Table 7 Summary of pre fracture work values for the State of Michigan asphalt mixtures ......... 33 Table 8 Summary of post fracture work values for the State of Michigan asphalt mixtures ....... 35 Table 9 Binder and Mixture Properties of 36 MDOT Mixtures used in Michigan Calibration of the Pavement ME Design Strength Prediction Model Developed by Witczak ............................ 51 Table 10 Comparison of the original and Michigan calibrated Pavement ME Design IDT strength Model Calibration Coefficients..................................................................................................... 52 Table 11 Comparison of model performance evaluation parameters measured for Original Pavement ME Design and Calibrated IDT strength prediction models for 36 MDOT asphalt mixtures......................................................................................................................................... 55 Table 12 MDOT JMF parameters found to be significantly correlated with measured IDT strength using a Pearson Correlation analysis. Correlation significance, either at the .01 or .05 level, and the relationship of the parameter, either positive (+) or negative (-), is also listed ...... 56 Table 13 Comparison of performance criteria for the original Pavement ME Design and linear IDT strength prediction models for commonly used MDOT asphalt mixtures ............................ 61 Table 14 Overview of specimens used and correlation coefficients for each stage of IDT ANN development .................................................................................................................................. 69 Table 15 Mixture properties and volumterics of mixtures tested ................................................. 74 Table 16 IDT Strength, Fracture Work, and Air Voids of Specimens Tested .............................. 86 v LIST OF FIGURES Figure 1 Examples of typical thermal cracking distress in flexible pavements evidenced by transverse cracking in the direction perpendicular to travel. For interpretation of the references to color in this and all other figures, the reader is referred to the electronic version of this thesis. ... 1 Figure 2 Development of stress in a diametrically loaded specimen during the IDT strength test 5 Figure 3 IDT strength test specimen at failure................................................................................ 6 Figure 4 Overview of the IDT strength specimen fabrication and testing process ......................... 9 Figure 5 Typical (Y-X) versus time curve depicting first peak time ............................................ 10 Figure 6 Typical IDT stress versus strain curve depicting pre and post energy ........................... 13 Figure 7 IDT test system consisting of an axial loading device with external environmental chamber ......................................................................................................................................... 26 Figure 8 Total fracture work versus IDT strength relationship .................................................... 38 Figure 9 Laboratory measured IDT strength for MDOT Mix ESAL designation categories for leveling and top course pavement layers ...................................................................................... 39 Figure 10 Laboratory measured total fracture work for MDOT Mix ESAL designation categories for leveling and top course pavement layers................................................................................. 40 Figure 11 IDT strength versus Low Temperature PG relationship............................................... 41 Figure 12 IDT strength for high PG characterization of Michigan asphalt mixtures ................... 41 Figure 13 Fracture work for low temperature Superpave PG characterization of Michigan asphalt mixtures......................................................................................................................................... 42 Figure 14 Fracture work for high temperature Superpave PG characterization of Michigan asphalt mixtures ............................................................................................................................ 43 Figure 15 IDT strength for comparable WMA and HMA mixtures ............................................. 44 Figure 16 IDT fracture work for comparable WMA and HMA mixtures .................................... 45 Figure 17 IDT post fracture work for comparable WMA and HMA mixtures ............................ 46 vi Figure 18 Effect of IDT strength input in Pavement ME Design Level 3 thermal cracking analysis for a 4”, PG 58-22 flexible pavement constructed in Detroit, Michigan. ....................... 48 Figure 19 Original Pavement ME Design IDT Strength Model for 36 MDOT mixtures with respect to the LOE ........................................................................................................................ 53 Figure 20 Michigan Calibrated Pavement ME Design IDT Strength Model for 36 MDOT mixtures with respect to the LOE ................................................................................................. 54 Figure 21 IDT strength predicated by Pavement ME Design software versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures ......................................... 59 Figure 22 IDT strength predicated during calibration by newly developed linear model versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures ....... 60 Figure 23 IDT strength predicated during testing by newly developed linear model versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures ....... 60 Figure 24 IDT strength predicated for all specimens by newly developed linear model versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures ....... 61 Figure 25 Structure of the ANN model developed for prediction of IDT strength for Michigan asphalt mixtures ............................................................................................................................ 63 Figure 26 Reduction in mean squared error of laboratory measured and ANN predicted IDT strength values during training, validation, and testing stages of ANN development .................. 66 Figure 27 ANN predicted IDT strength versus measured IDT strength (base 10) for the training, validation, testing, and all data used in ANN development .......................................................... 67 Figure 28 ANN Predicated versus measured IDT strength values for all mixtures used in ANN development .................................................................................................................................. 68 vii 1. INTRODUCTION Thermal cracking is the predominant pavement distress in the northern United States and Canada. At low temperatures, cooling of a flexible pavement causes contraction of the aggregate and asphalt binder, creating thermal stresses which manifest as transverse cracking perpendicular to the direction of travel (Figure 1). Thermal cracking leads to additional pavement deterioration mechanisms including water seeping into the base/subbase, pumping, frost heave, and ultimately deterioration of the road leading to premature maintenance. Figure 1 Examples of typical thermal cracking distress in flexible pavements evidenced by transverse cracking in the direction perpendicular to travel. For interpretation of the references to color in this and all other figures, the reader is referred to the electronic version of this thesis. The identification and evaluation of mix design factors than can increase thermal cracking resistance is of extreme interest to state agencies seeking to improve pavement performance. The low temperature indirect tensile (IDT) strength is one measure of an asphalt mixture’s resistance to thermal cracking and is measured by the IDT strength test. The IDT strength test is currently the most widely used thermal cracking mixture characterization method. 1 The low temperature IDT strength test is conducted by applying displacement controlled loading along the direction of diameter in a cylindrical specimen until failure. The stress at failure is taken as the low temperature IDT strength. Low temperature IDT strength is directly related to the expected thermal cracking pavement performance in the field. Based on this concept the Pavement ME Design software (i.e., M-E PDG) utilizes semi-mechanistic and semiempirical models to predict pavement distresses over time, such as thermal cracking. As a result of research under NCHRP Project 1-37A, the Pavement ME Design software is the most recently developed design guide for newly constructed and rehabilitated pavement designs. The Pavement ME Design software requires traffic, climate, and material inputs to predict pavement distresses and accurate measurement of these inputs is necessary for successful prediction. For thermal cracking prediction in flexible pavements, the Pavement ME Design software requires material inputs of mixture IDT strength and creep compliance values to predict thermal cracking per unit length over time. The IDT strength and creep compliance characterization of the asphalt mixture is required for Levels 1, 2, and 3. Inputs into the Pavement ME Design are classified according to a three level system (Levels 1, 2, and 3), which allow pavement engineers to select the level of design accuracy. A Level 1 analysis requires the most detailed characterization of material inputs and can generally be thought to predict pavement distresses most accurately. A Level 3 analysis requires the least detailed characterization of material inputs; as a result the accuracy of the distress predictions can be low. Many state transportation agencies, including the Michigan Department of Transportation (MDOT), do not have testing programs to measure the required Pavement ME Design Level 1 material inputs for thermal cracking analysis and they are instead predicted by Pavement ME Design using predictive equations at the expense of accuracy. 2 1.1 Objective The first objective of this study was to characterize the IDT strength and fracture work of asphalt mixtures commonly used in the State of Michigan. It is important to understand the low temperature fracture properties and if they can be predicted from or are related to current pavement design frameworks, such as Superpave Performance Grading or MDOT mix designation. The second objective was to examine the accuracy of the predictive equations used by the Pavement ME Design software in predicting low temperature IDT strength and develop improved prediction equations/models if necessary. This is important for accurate prediction of asphalt thermal cracking distress and subsequently successful implementation of the Pavement ME Design software by MDOT. 1.2 Outline This thesis is organized as follows: Chapter 2 presents a literature review on the background of the IDT creep and strength tests and prediction of IDT strength in Pavement ME Design software. Second, a discussion on the relevance of IDT strength to the Pavement ME Design software and how it is used in thermal cracking prediction is given. Finally, Chapter 2 also reviews current research on mix design factors and volumetrics influencing IDT strength. Chapter 3 presents the materials used in this research and the testing protocol followed. Chapters 4 and 5 present the results of the IDT strength laboratory testing and development of IDT strength predictive models, respectively. Chapter 6 presents the conclusions of this study and recommendations for future work. 3 2. LITERATURE REVIEW 2.1 Motivation Thermal cracking is the predominant asphalt pavement distress in northern climates such as the State of Michigan. As the Pavement ME Design becomes state of the practice for the design of new and rehabilitated pavements it is in the best interest of transportation agencies to accurately characterize material inputs in order to successfully predict pavement distresses such as thermal cracking. Review of literature on asphalt mixtures used in the State of Michigan showed a need for low temperature mixture characterization for use in pavement design. Additionally preliminary analysis of Pavement ME Design IDT strength prediction showed poor prediction performance for Michigan mixtures. This study aims to characterize the low temperature strength properties of Michigan asphalt mixtures. Secondly this study aims to predict these low temperature strength properties. Accurate prediction of material properties such as IDT strength is important for successful thermal cracking distress prediction and subsequent successful implementation of the Pavement ME Design software. 2.2 Background of the Indirect Tensile Strength Test A material’s IDT strength is a measure of its tensile strength when loaded diametrically across a circular specimens’ cross-section. Figure 2 illustrates the loading scheme and resulting stress distribution within the IDT strength test sample. 4 Load Load Compression Compression Tension Tension Y σσ Xx σσyY X X Y Stress distribution acrossdiameter diameter Stress distribution across Load Load Figure 2 Development of stress in a diametrically loaded specimen during the IDT strength test Loading applied along the circular specimens’ diameter causes tensile forces to develop perpendicular to the direction of loading, ultimately resulting in a tensile failure (Figure 3). The IDT strength test was first used to determine the tensile strength of wood and rock materials in what is commonly known as the Brazilian Test [26]. In 1943 Carneiro [13] applied the IDT strength test to concrete and it is still used as the primary method to determine concrete tensile strength today. In the early 1990’s work began by Roque [8] to apply the IDT test to asphalt mixtures and as a result the first procedure for low temperature IDT creep and strength 5 characterization of asphalt mixtures was developed under the first Strategic Highway research Program (SHRP) [7][8]. As a result of this work the procedure was then codified as an AASHTO standard, AASHTO T-322, “Standard Method of Test for Determining the Creep Compliance and Strength of Hot-Mix Asphalt (HMA) Using the Indirect Tensile Test Device” [1]. In the late 1990’s the IDT strength test underwent further examination by the Federal Highway Administration (FHWA) during the development of Superpave mix design protocol. Due to its accuracy and durability, the IDT strength and creep test was identified as a simple performance test for low temperature cracking in HMA mix design. The IDT strength and creep was then also selected as a materials characterization test in NCHRP Project 1-37A due to its ability to predict a mixture’s resistance to thermal cracking as evidenced by its good correlation to field thermal cracking data [10]. Figure 3 IDT strength test specimen at failure 6 Today the IDT strength test is still the most widely used strength test to characterize a mixture’s resistance to thermal cracking. Other tests exist to characterize the thermal cracking resistance of asphalt mixtures each with their own advantages and disadvantage and include the Thermal Stress Restrained Specimen Test (TSRST) [21], Semi-Circular Bend (SCB) Test [24], Modified IDT, and Disk-Shaped Compact Tension (DCT) Test [27]. These methods also measure mixture tensile strength to characterize thermal cracking resistance, but differ mostly in specimen geometry, deformation monitoring methods, and loading application in an attempt to rectify perceived shortcomings in the IDT creep and strength test [27]. Yet currently the IDT creep and strength tests are still considered the most promising parameters for predicting the low temperature performance of asphalt mixtures [10]. 2.3 Current Indirect Tensile Strength Testing Procedure The standard test method for the IDT strength is the AASHTO T-322 “Determining the Creep Compliance and Strength of Hot-Mix Asphalt (HMA) Using the Indirect Tensile Test Device.” The AASHTO T-322 contains detailed procedures to determine tensile creep compliance, tensile strength, and Poisson’s ratio of an HMA mixture [1]. The summary of the method to determining the tensile strength, commonly known as the IDT strength, is as follows: Bulk laboratory molded specimens are compacted from loose mixture in a Superpave Gyratory Compactor (SGC). Cylindrical specimens are then cut from the SGC compacted specimens to a diameter of 150 9 mm and to a height of 38 to 50 mm (Figure 4). Bulk Specific Gravity and air voids of each specimen are determined and only specimens meeting air voids of 7 .5% are selected for testing. Once specimens are fabricated to geometric and volumetric criteria two linear variable differential transducers (LVDTs) are attached to each of the two specimen’s faces with the use of mounting gauges and epoxy (Figure 4). Specimens are then conditioned in an 7 environmental chamber at the test temperature for 3 1 hours prior to testing. A test temperature of 0°C or less is used for thermal cracking analysis, however if the analysis is used for Superpave design, test temperatures of 0, -10, and -20°C are recommended. After conditioning, the specimen is placed into a testing frame located inside an Indirect Tensile Test System (Figure 4, Step 3). The IDT Test System consists of an axial loading device, environmental chamber, and a control and data acquisition system. At the test temperature, load is applied to the specimen at a rate of 12.5 mm of vertical ram movement per minute. During load application vertical and horizontal deformations on both faces of the specimen and the load magnitude are recorded. Displacement controlled loading is applied until the load starts to decrease, at which point strength test is complete. The desired failure mode consists of a vertical crack running along the length of the specimen’s diameter in line with the direction of loading (Figure 3 and Figure 4). 8 Step 1) Bulk specimens are compacted from loose mixture samples using the SGC Step 2) Compacted specimens are cut to dimension and volumetric properties measured Step 3) Specimens are mounted with LVDTs and conditioned at the testing temperature Step 4) Load is applied until failure (LVDTs removed for display purposes) Figure 4 Overview of the IDT strength specimen fabrication and testing process 9 2.4 Calculation of Indirect Tensile Strength According to AASHTO T-322 AASHTO T-322 defines failure as the point when vertical deformations (Y) minus horizontal deformations (X) (as measured by the LVDTs) reach a maximum value. This time is called first peak time and the load at this time is called the first failure load (Figure 5). Determination of peak failure time 50 Side 1 Y-X (μm) 40 Side 2 Side 2 Y-X peaks first 30 20 10 t 0 0 1 2 Time (seconds) 3 peak 4 Figure 5 Typical (Y-X) versus time curve depicting first peak time The failure load is then used along with specimen geometry to determine the tensile strength. The procedure is as follows. 1. Determine failure time, tf, for both faces of the specimen, defined as the time when vertical deformation minus horizontal deformation reaches a maximum value. Take the shortest tf. 2. Obtain the failure load, Pf, at time tf. 3. Calculate the IDT strength, St. (1) 10 Where, bn = average thickness of the specimen Dn = average diameter of the specimen 2.5 Calculation of Indirect Tensile Strength without Deformation Monitoring Under NCHRP 530 report [10] AASHTO T-322 was thoroughly examined in an effort to first validate and secondly determine possible improvements to the test. One of the suggested improvements proposed in NCHRP 530 report was IDT strength testing without the use of LVDTs to monitor deformations. LVDTs were initially incorporated into AASHTO T-322 because the precise moment of failure during the IDT test is difficult to determine due to the often slow specimen failure and ability of the specimen to carry significant load even after cracks become visible along the specimen face. Despite the accuracy and precision of the exact failure moment determination with the LVDTs testing at state agencies, the FHWA, and regional Superpave Centers reported feasibility issues with using the LVDTs. LVDTs were found to be difficult to keep in place and due to the sometimes explosive nature of specimen failure, the expensive and delicate LVDTs were at risk to be damaged during testing, potentially jeopardizing overall reliability and accuracy of the IDT strength test. As a result of feedback from testing centers, an empirical relationship was found between the true (corrected) and unninstrumented (uncorrected) strength values and evaluated in NCHRP 530 report [10] (Equation 2). The empirical equation relating corrected and uncorrected IDT strength values was found to be accurate and able to predict true strength reasonably well from uninstrumented IDT strength as compared to LVDT instrumented testing. For practical purposes the IDT strength testing that serves at the basis of this thesis did not employ LVDTs during testing and Equation 11 2, developed by NCHRP-530 researchers, was used to estimate the true strength (instrumented) from the uninstrumented strength. The strength at maximum load is termed the uncorrected strength (Equation 2). True Tensile Strength (psi) = [0.781 x Uncorrected IDT Strength (psi)] + 38 (2) 2.6 Determination of Fracture Work from Indirect Tensile Strength Testing The IDT strength test can also be used to measure a mixture’s fracture energy [22] [25] and fracture work [39]. Fracture energy of a mixture is defined as the area under the stress versus strain curve while similarly fracture work is the area under the load versus horizontal displacement curve. Total fracture energy consists of pre-peak energy (fracture energy measured until failure), and post-peak fracture energy (fracture energy measured after failure) depicted in Figure 6 [40]. 12 Typical pre and post fracture ernergies 450 Specimen Failure 400 Pre Fracture Energy 350 Stress (psi) 300 250 Post Fracture Energy 200 150 100 50 0 0 400 800 1200 Strain (με) 1600 2000 2400 Figure 6 Typical IDT stress versus strain curve depicting pre and post energy Pre-peak fracture energy is associated with crack initiation while post-peak fracture energy is associated with crack propagation [40]. High pre-peak fracture energy would be indicative of greater resistance to thermal cracking initiation, while high post-peak fracture energy would be associated with a lower rate of thermal cracking propagation. A mixture high in fracture energy, pre or post, would generally be expected to exhibit lower rates of thermal cracking compared to a mixture with lower fracture energy. In this thesis fracture work was used to characterize mixture thermal cracking resistance instead of fracture energy. Fracture work measured by the IDT test has been shown to correlate well with field performance whereas fracture energy has been shown not to correlate well with field performance [39]. This is in part due to fracture work’s ability to capture the entire postpeak behavior whereas fracture energy often cannot due to limits in the range of LVDT 13 measurements. Another advantage of fracture work is the elimination of LVDT instrumentation during testing. Vertical ram movement has been shown to be no different that LVDT measured horizontal displacement [39]. This enables rapid testing and eliminates LVDT damage. For these reasons the use of fracture work was used in this thesis as an additional method to characterize thermal cracking susceptibility of Michigan mixtures. 2.7 Relevance of Indirect Tensile Strength to Pavement ME Design Pavement ME Design is the latest pavement design guide developed as a result of research completed under NCHRP 1-37A. In the Pavement ME Design distresses are predicted over a design period based on material properties, climate, traffic, and design geometry. Pavement engineers input a design pavement cross section and can predict pavement distresses over time and modify their design accordingly. Pavement ME Design predicts thermal cracking in flexible pavements using the Thermal Cracking (TC) Model first developed by Hiltunen and Roque [17] [36]. The TC Model takes into account material inputs, climate, and design geometry to predict the amount of thermal cracking per length of pavement over time. For example, a typical MDOT HMA pavement constructed in Northern Michigan may be predicted to exhibit thermal cracking distress of 500 feet per mile after 20 years. The amount of thermal cracking in the TC Model is predicted in three steps. First thermal stress distribution due to cooling is calculated. Second, crack propagation is modeled. And lastly the amount of cracking visible on the pavement surface is calculated [28] [40]. Mixture IDT strength is used as an input into the calculation of crack propagation portion of the TC Model and is discussed subsequently. 14 Crack growth rate in the TC Model is governed using the Paris Law, given by the following equation [28]: n ΔC = A(ΔK) (3) where: ΔC = change in crack length ΔK = change in the stress intensity factor A, n = regression parameters The change in the stress intensity factor, ΔK, is determined through a subroutine program called CRACKTIP, a finite element program used to calculate the stress at the tip of a single vertical thermal crack [17]. A and n are regression parameters originally derived by Schapery [35] for nonlinear viscoelastic materials and related to creep compliance, IDT strength, and fracture work [35]. A and n can be empirically related to mixture strength, IDT strength, and creep compliance through the following relationships [35]. (4) Where: E = mixture stiffness, psi σm = mixture IDT strength, psi n= m = slope of the linear portion of the log compliance-log time relationship determined from the IDT creep test 15 In summary, the IDT strength is directly used as an input into calculating the A parameter and used in calculation of crack propagation in the Pavement ME Design TC Model. The accuracy of the thermal cracking model is therefore directly dependent on the accuracy of the models used for estimating creep compliance and tensile strength, which is the subject of this thesis. 2.8 Pavement ME Design IDT Strength Prediction In the TC Model subroutine of Pavement ME Design, IDT strength at -10°C is a direct input in Level 1 and Level 2 analysis, often measured by universities or private testing facilities as most state agencies do not have their own testing programs in place. For Level 3 analysis IDT strength at -10°C is still required but is estimated from the binder PG and mixture volumterics. Initially IDT strength was predicated based solely on binder PG, i.e. any mixture containing PG 58-28 would have an IDT strength of 400 psi while any mixture containing PG 64-34 would have an IDT strength of 475 psi. This initial predictive model was found to provide a biased estimate and high variance in predicting IDT strength [6]. Final modification and revision of the TC Model by Witczak et al [6] under NCHRP 9-19 revised the IDT strength prediction subroutine of the TC Model based on correlations with PG and volumetric and mixture properties [6]. IDT strength was found to correlate well with air voids, voids filled with asphalt (VFA), the Penetration at 77°F, and the A intercept of the RTFO conditioned binder temperatureviscosity relationship. Based on these relationships, the following empirical equation was developed. 16 2 2 St = 7416.712 – 114.016Va – 0.304Va -122.592VFA + 0.704VFA + 405.71log (Pen77) - 2039.296log(ARTFO) (5) Where: St = Indirect tensile strength at -10°C (psi) Va = Air Voids, % VFA = Voids Filled with Asphalt, % Pen77 = Penetration at 77°F ARTFO = Intercept of RTFO conditioned binder Viscosity-Temperature relationship Binder material parameter ARTFO is not directly input into Pavement ME software, instead it is predicted from binder PG. Pen77 is also not required and is predicted from binder PG. Global calibration of the IDT strength subroutine in the TC Model was completed using 31 data points. Goodness of fit statistics Se/Sy (standard error of estimate/standard deviation), 2 and correlation coefficient (R ) were 0.68 and 0.62, respectively [6]. 2.9 Factors Affecting Mixture Indirect Tensile Strength Much work has been done on low temperature characterization of asphalt binder, while less work has been done on low temperature characterization of the asphalt mixture. Relatively few studies have examined the effects of mixture properties and volumetric influences on the low temperature IDT strength. Because of the use of IDT strength in thermal cracking resistance 17 characterization in Pavement ME Design it is important to understand the mixture and volumetric properties that affect IDT strength and thus directly impact thermal cracking susceptibility. NCHRP 530 reported IDT strength values correlated well with voids filled with asphalt (VFA). Low temperature cracking research by Zborowsk and Kaloush [40] showed that crumb rubber modified mixtures exhibited a lower IDT strength and higher fracture energy values as compared to conventional HMA mixtures. In 2011 the National Asphalt Pavement Association in their Warm Mix Asphalt (WMA) best practices report hypothesized that as a result of lower production and placement temperatures WMA mixtures would be softer and thus lead to greater resistance to thermal cracking regardless of their respective WMA additive [16]. Li et al. [25] examined the effect of binder type, binder, modifier, aggregate type, asphalt content, and air voids on the fracture work and fracture toughness of 28 asphalt mixtures as measured by the IDT strength test. Aggregate type, air voids, and high PG for a constant PG low limit were found to have a significant impact on both fracture work and toughness, while an increase in percent binder was not found to be a significant factor. Fracture work was found to increase as test temperature increased while fracture toughness was found to decrease as test temperature increases [25]. In a 2011 study on the effect of Reclaimed Asphalt Pavement (RAP) on IDT strength values Huang et al. reported that generally increasing the percentage of RAP in an HMA mixture resulted in greater IDT strengths and lower toughness indices as did increasing the long term aging of a mixture [18]. 18 3. METHODS 3.1 Introduction This study was part of a larger comprehensive research effort to characterize asphalt mixtures commonly used in the State of Michigan, for MDOT implementation of Pavement ME Design. In this study 62 different asphalt mixtures were characterized using the IDT strength test to determine IDT strength, total fracture work, pre-peak fracture work, and post-peak fracture work. 3.2 Mixtures Used Mixtures used in this study consisted of 58 unique HMA and 4 unique WMA mixtures obtained as loose mixture samples by MDOT personal from MDOT pavement projects across the State of Michigan (North, Grand, Bay, Southwest and University Regions, Metro Region, and Superior Region). Mix design volumetrics and aggregate gradations were also provided by MDOT for each mixture. A description of mixtures tested in this thesis is shown in Table 1 through Table 4, where mixtures tested are highlighted in grey. 19 M HS M HS M HS E30 E30 E50 E50 E10 E10 Top North, Grand, Bay, Southwest and University Regions (NGBSU) 64-22 1 64-22 2A 70-28P 3 70-28P 4 70-28P 64-22 1 64-22 2B 76-28P 6 76-28P 7 76-28P 64-22 9 64-22 10 70-28P 11 70-28P 12 70-28P 64-22 9 64-22 10 76-28P 14 76-28P 15 76-28P 58-22 17 58-22 18A 64-28 19 64-28 20 64-28 58-22 17 58-22 18B 70-28P 22 70-28P 23 70-28P 20 HMA# Leveling/Top Binder PG Leveling HMA# Base Binder PG Base HMA# 5 Binder PG 4 HMA# 3 Binder PG 3 HMA# 2 Binder PG Mix Type Layer: Mix No: Table 1 HMAs tested for IDT strength 5 8 13 16 21 24 M HS M HS M HS M HS M HS M HS M HS M HS M HS M HS M HS M HS North, Grand, Bay, Southwest and University Regions (NGBSU) E3 58-22 25 58-22 26A 64-28 27 64-28 28 64-28 E3 58-22 25 58-22 26B 70-28P 30 70-28P 31 70-28P E03 58-22 33 58-22 34 58-28 35 58-28 36 58-28 E03 58-22 33 58-22 34 64-28 38 64-28 39 64-28 E1 58-22 41 58-22 42 58-28 43 58-28 44 58-28 E1 58-22 41 58-22 42 64-28 46 64-28 47 64-28 Metro Region E30 64-22 1 64-22 2A 70-22P 89 70-22P 90 70-22P E30 64-22 1 64-22 2B 76-22P 92 76-22P 93 76-22P E50 64-22 9 64-22 10 70-22P 95 70-22P 96 70-22P E50 64-22 9 64-22 10 76-22P 98 76-22P 99 76-22P E10 58-22 17 *58-22 18A 64-22 101 64-22 102 64-22 E10 58-22 17 58-22 18B 70-22P 104 70-22P 105 70-22P E3 58-22 25 58-22 26A 64-22 107 64-22 108 64-22 E3 58-22 25 58-22 26B 70-22P 110 70-22P 111 70-22P E03 58-22 33 58-22 34 58-22 113 58-22 114 58-22 E03 58-22 33 58-22 34 64-22 116 64-22 117 64-22 E1 58-22 41 58-22 42 58-22 119 58-22 120 58-22 E1 58-22 41 58-22 42 64-22 122 64-22 123 64-22 Superior Region E10 58-28 53 58-28 54 58-34 55 58-34 56 58-34 E10 58-28 53 58-28 54 64-34P 58 64-34P 59 64-34P E3 58-28 61 58-28 62 58-34 63 58-34 64 58-34 E3 58-28 61 58-28 62 64-34P 66 64-34P 67 64-34P E03 58-28 69 58-28 70 58-34 71 58-34 72 58-34 E03 58-28 69 58-28 70 64-34P 74 64-34P 75 64-34P 21 HMA# Top Binder PG Leveling/Top HMA# Leveling Binder PG Base HMA# Lay er: Base Binder PG 5 HMA# 4 Binder PG 3 HMA# 3 Binder PG 2 Mix Type Mi x N o: Table 1 (cont’d) 29 32 37 40 45 48 91 94 97 100 103 106 109 112 115 118 121 124 57 60 65 68 73 76 M E1 58-28 77 HS E1 58-28 82 Note: M=Mainline, HS=High Stress 58-28 58-28 Superior Region 78 58-34 79 83 64-34P 84 58-34 64-34P 80 85 58-34 64-34P 81 86 Binder PG HMA# Top Binder PG Leveling/Top HMA# Leveling Binder PG Base HMA# Base HMA# 5 Binder PG 4 HMA# 3 Binder PG Mix No: 3 Mix Type: 2 Layer: Table 1 (cont’d) Table 2 HMAs tested for IDT strength (GGSP and LVSP Mixtures) HMA Type Layer: Region: Leveling/Top North, Grand, Bay, Southwest and University Regions (NGBSU) Mix Binder PG Type M GGSP 70-28P HS GGSP 76-28P M LVSP 58-28 HS LVSP 64-28 Note: M=Mainline, HS=High Stress Metro Superior HMA# Binder PG HMA# Binder PG HMA# 49 50 51 52 70-22P 76-22P 58-22 64-22 125 126 127 128 - - 58-34 64-34P 87 88 22 Table 3 HMAs tested for IDT strength (SUPERPAVE) – Mixtures that do not follow MDOT specifications but are permitted to be used HMA Type Mix No: 2 3 Layer: Base Base Mix Binder Binder HMA# HMA# Type PG PG M E10 58-28 200 HS E10 HS E30 M E3 58-28 205 M E1 M E1 Note: M=Mainline, HS=High Stress 4 Leveling/Top Binder HMA# PG 5 Top Binder HMA# PG 70-22P 64-22 70-22P 202 204 64-22 64-22 206 207 203 Table 4 HMAs tested for IDT strength (GGSP and LVSP Mixtures) - Mixtures that do not follow MDOT specifications but are permitted to be used HMA Type: Layer: Leveling/Top Region: NGBSU Metro Superior Mix Binder HMA# Binder HMA# Binder HMA# Type M ASCRL 64-28 201 Note: M=Mainline 3.3 Specimen Preparation All specimens where compacted according to AASHTO PP60, “Preparation of Cylindrical Performance Test Specimens Using the Superpave Gyratory Compactor (SGC)”, to an air void value of 7 .5%, as determined according to the AASHTO T 166-11 “Bulk Specific Gravity of Compacted Hot Mix Asphalt (HMA) Using Saturated Surface-Dry Specimens.” For each unique mixture 3 replicates were generally prepared. A limited number of mixtures had more or less than 3 replicates due to limits in amount of loose mixture available and variability when reaching the target air void content. Each specimen was wet sawed to dimensions of approximately 150 mm diameter and 38 mm height and checked for correct air void content. A 23 total of 204 specimens were tested with the IDT strength test method for this study. Exact specimens dimensions, air void contents, and number of replicates for each mixture are listed in Appendix A. 3.4 Indirect Strength Testing Procedures Each specimen was tested for IDT strength in accordance with AASHTO T-322. Due to testing recommendations described in NCHRP 530 and equipment constraints, a few important changes were made in this study and they are listed in the subsequent sections. 3.4.1 Testing Temperature IDT testing in this study was conducted at -10°C, which is the test temperature required for IDT strength input into Pavement ME Design but differs from AASHTO T-322 requirements. Testing temperature in AASHTO T-322 is recommended based on low temperature PG, PGXX28 and PG XX-22 are recommended at -10°C while PG XX-16 and stiffer binders are recommended at 0°C. In Pavement ME Design the -10°C testing temperature was selected to represent the undamaged tensile strength of an asphalt mixture in Pavement ME Design as testing in SHRP A-005 showed that peak strength always occurred at temperatures lower than 10°C [6]. Thus testing at -10°C may be considered an accurate and conservative measure of a mixture’s “undamaged” tensile strength. The term “undamaged” herein corresponds to the newly constructed asphalt mixture (i.e. no aging or damaged has yet occurred). 3.4.2 Use of LVDTs As per recommendations put forth in NCHRP 530 and discussed previously, LVDTs were not used in this study. The corrected, or LVDT instrumented, strength of each specimen 24 was determined using Equation 2, an empirical relationship found to estimate reasonably well corrected strength using uncorrected (uninstrumented) strength [10]. 3.4.3 Environmental Chamber The final modification, actually a limitation, is that specimens were tested in an IDT Test System without an environmental chamber. Due to the IDT Test System chamber inability to maintain a stable test temperature specimens were conditioned and held in an external chamber placed immediately next to the IDT Test System (Figure 7). At the time of testing, each specimen was immediately transferred from the external environmental chamber to the IDT Test System loading frame and loaded to failure in less than 60 seconds from leaving the external environmental chamber. In order to minimize temperature loss during the 60 second transfer process, a dummy specimen with an internal thermocouple was transferred from the external chamber to the testing area. It was observed that the dummy specimen did not lose more than 1°C during this process. 25 Figure 7 IDT test system consisting of an axial loading device with external environmental chamber 26 4. RESULTS OF LABORATORY INDIRECT TENSILE TESTING 4.1 Indirect Tensile Strength of Michigan Mixtures An overview of the average laboratory measured IDT strength for the 62 MDOT asphalt mixtures tested at -10°C as a part of 27 this study is shown in Table 5. Table 5 Summary of IDT strength values for the State of Michigan asphalt mixtures Mix No: 3 4 5 Layer: Base Leveling/Top Top IDT Strength, -10°C IDT Strength, -10°C IDT Strength, -10°C Traffic HMA # Strength HMA # Strength HMA# Strength SD CV SD CV SD CV (psi) (psi) (%) (psi) (psi) (%) (psi) (psi) (%) E30 E30 E10 E10 E10 E10 E3 E3 E3 E3 E3 E3 E1 E1 2A 2B 18A 18B 200 477 362 343 463 22 21 49 30 5 6 14 7 26A 26B 26C 62 400 338 346 413 19 29 12 19 5 9 3 5 4 483 18 4 20A 20C 23 452 395 462 32 23 15 7 6 3 28A 28B 31A 31B 64 67 44 47 483 416 442 470 388 402 405 433 15 20 36 11 45 20 27 4 3 5 8 2 12 5 7 1 E03 28 20B 21 24A 24B 29A 29B 32A 32B 65 448 454 372 498 399 426 460 453 362 19 19 27 16 12 22 19 8 10 4 4 7 3 3 5 4 2 3 45 48 346 422 34 21 10 5 37 455 20 4 Table 5 (cont’d) Mix No: Layer: Mix GGSP GGSP LVSP LVSP LVSP LVSP ASCRL 2E3 LVSP Miscellaneous Miscellaneous IDT Strength, -10°C HMA Strength SD CV # (psi) (psi) (%) 49A 49C 51A 51B 51C 127 201 205 208 387 336 347 405 379 389 276 321 425 14 16 40 14 12 40 7 37 18 4 5 12 4 3 10 3 12 4 Mix No: Layer: Traffic E50 E30 E30 E10 E10 E10 E10 E3 E3 E3 E1 E1 E1 4 Leveling/Top IDT Strength, -10°C HMA Strength # (psi) SD (psi) CV (%) 90A 203 102 105 455 451 487 449 0 13 17 32 0 3 4 7 67 108 111 80 85 402 467 512 409 403 20 15 10 15 11 5 3 2 4 3 29 5 Top IDT Strength, -10°C HMA# Strength (psi) SD (psi) CV (%) 97 204 508 560 5 12 1 2 103 202 209A 209B 68 109 112 81 86 206 427 512 453 419 410 480 533 357 417 468 70 8 9 31 24 28 9 0 16 22 16 2 2 7 6 6 2 0 4 5 The average IDT strength of all mixtures was 426 psi. The lowest recorded IDT strength was 276 psi, measured from mix 201 an Asphalt Stabilized Crack Relief Layer (ASCRL) mixture. The highest IDT strength recorded was 560 psi, measured from mix 204 a MDOT designated 5E30 High Stress mixture. Major state and highway mixtures used in the State of Michigan are designated using a two part nomenclature system. The first part of the designation details the location in the pavement system in which the mix will be used (base, leveling, leveling/top, or top course). The second part of the designation is termed the mix type and details the expected design traffic value in millions of ESALs. For instance a mix designated 5E30 would be used as a top course and is designed to withstand 30 million ESALs. The IDT strength values for each of the ESAL design categories was examined to investigate the use of the MDOT mixture classification systems ability to be used as a thermal cracking resistance parameter during design. In Table 5 mixtures with greater IDT strength are generally designated as Mix No. 4 and 5 while mixtures with the lower IDT strength are generally designated as Mix No. 2 and 3, GGSP, and LVSP. 4.2 Fracture Work of Michigan Mixtures It is recalled that fracture work of a mixture is defined as the area under the load versus vertical deformation curve and can be reported as total fracture work (Figure 6), which consists of pre-peak work (fracture work measured until failure), and post-peak fracture work (fracture work measured after failure). Measured total, pre, and post fracture work for the mixtures tested in this study are given in Table 6. 30 Table 6 Summary of total work values for the State of Michigan asphalt mixtures Base Leveling/Top Top Total Work, -10°C Total Work, -10°C Total Work, -10°C Layer: Traffic HMA # Total Work (lb*in.) SD (lb*in.) CV (%) HMA # Total Work (lb*in.) SD (lb*in.) CV (%) E30 E30 E10 E10 E10 E10 E3 E3 E3 E3 E3 E3 E1 E1 E03 2A 2B 18A 18B 200 280 419 365 273 242 75 92 164 87 11 27 22 45 32 5 4 415 53 13 20A 20C 23 269 362 446 61 86 63 23 24 14 26A 26B 26C 62 412 430 349 508 0 11 63 97 0 3 18 19 28A 28B 31A 31B 64 67 44 47 225 185 281 283 246 522 226 245 45 33 72 32 77 85 45 42 20 18 26 11 31 16 20 17 31 HMA# Total Work (lb*in.) SD (lb*in.) CV (%) 20B 21 24A 24B 29A 29B 32A 32B 65 341 281 527 459 280 202 327 406 324 24 42 68 84 11 23 42 79 40 7 15 13 18 4 12 13 20 12 45 48 37 323 213 515 40 48 154 12 22 30 Table 6 (cont’d) Mix No: Layer: Miscellaneous Miscellaneous Total Work, -10°C Mix HMA # GGSP GGSP LVSP LVSP LVSP LVSP ASCRL LVSP 49A 49C 51A 51B 51C 127 201 208 Total SD Work (lb*in.) (lb*in.) 499 1014 544 215 294 307 232 174 141 258 130 47 27 98 83 22 Mix No: Layer: CV (%) Traffic 28 25 24 22 9 32 36 13 E50 E30 E30 E10 E10 E10 E10 E3 E3 E3 E1 E1 E1 4 5 Leveling/Top Total Work, -10°C HMA # Total SD Work (lb*in.) (lb*in.) CV (%) 90A 203 102 105 182 337 343 312 0 60 81 58 0 18 23 19 67 108 111 80 85 522 302 338 514 622 85 65 9 96 147 16 22 3 19 24 32 Top Total Work, -10°C HMA# Total Work (lb*in.) SD (lb*in) CV (%) 97 204 258 383 28 70 11 18 103 202 209A 209B 68 109 112 81 86 206 333 185 200 196 405 241 238 193 538 178 212 21 41 52 40 46 20 0 116 20 64 11 20 27 10 19 8 0 22 11 Table 7 Summary of pre fracture work values for the State of Michigan asphalt mixtures Mix No: Layer: 3 4 5 Base Leveling/Top Top Pre Work, -10°C Pre Work, -10°C Pre Work, -10°C Traffic HMA # Pre Work (lb*in.) SD (lb*in.) CV (%) HMA # Pre Work (lb*in.) SD (lb*in.) CV (%) E30 E30 E10 E10 E10 E10 E3 E3 E3 E3 E3 E3 E1 E1 E03 2A 2B 18A 18B 200 275 261 228 244 242 68 29 36 47 11 25 11 16 19 5 4 300 30 10 20A 20C 23 264 247 320 53 33 4 20 14 1 26A 26B 26C 62 247 220 247 265 0 17 23 36 0 8 9 14 28A 28B 31A 31B 64 67 44 47 225 183 254 279 202 253 226 245 45 29 38 28 42 35 45 42 20 16 15 10 21 14 20 17 33 HMA# Pre Work (lb*in.) SD (lb*in.) CV (%) 20B 21 24A 24B 29A 29B 32A 32B 65 263 281 287 335 260 198 291 275 274 37 42 17 17 24 20 20 37 8 14 15 6 5 9 10 7 13 3 45 48 37 252 213 254 2 48 56 1 22 22 Table 7 (cont’d) Mix No: Miscellaneous Layer: Miscellaneous Mix No: Layer: Pre Work, -10°C 4 5 Leveling/Top Top Pre Work, -10°C HMA # Pre Work, -10°C Mix HMA # Pre Work (lb*in.) SD (lb*in.) CV (%) Traffic GGSP 49A 260 13 5 E50 GGSP 49C 200 24 12 E30 90A 182 0 0 LVSP 51A 226 29 13 E30 203 289 60 21 LVSP 51B 215 47 22 E10 102 297 28 LVSP 51C 236 24 10 E10 105 297 35 LVSP 127 243 37 15 ASCRL 201 180 20 LVSP 208 174 22 HMA# Pre Work (lb*in.) SD (lb*in.) CV (%) 97 258 28 11 204 377 60 16 9 103 218 41 19 12 202 185 21 11 E10 209A 200 41 20 11 E10 209B 192 47 24 13 E3 67 253 35 14 68 292 26 9 E3 108 298 58 19 109 241 46 19 E3 111 321 19 6 112 238 20 8 E1 80 294 32 11 81 193 0 0 E1 85 254 31 12 86 287 33 12 206 178 20 11 E1 34 Pre Work (lb*in.) SD (lb*in.) CV (%) Table 8 Summary of post fracture work values for the State of Michigan asphalt mixtures Mix No: Layer: 3 Base Post Work, -10°C 4 5 Leveling/Top Post Work, -10°C Top Post Work, -10°C Traffic HMA # Post Work (lb*in.) SD (lb*in.) CV (%) HMA # Post Work (lb*in.) SD (lb*in.) CV (%) E30 E30 E10 E10 E10 E10 E3 E3 E3 E3 E3 E3 E1 E1 E03 2A 2B 18A 18B 200 5 158 137 30 0 9 77 144 46 0 173 49 105 155 0 4 115 32 28 20A 20C 23 5 115 125 8 96 61 173 83 49 26A 26B 26C 62 165 210 102 243 0 8 49 130 0 4 48 54 28A 28B 31A 31B 64 67 44 47 0 2 27 4 43 269 0 0 0 5 37 7 50 108 0 0 0 200 136 173 116 40 0 0 35 HMA# Post Work (lb*in.) SD (lb*in.) CV (%) 20B 21 24A 24B 29A 29B 32A 32B 65 78 0 240 123 20 4 35 131 50 27 0 78 90 35 5 41 43 49 35 0 32 73 173 122 116 32 98 45 48 37 71 0 261 41 0 210 58 0 80 Table 8 (cont’d) Mix No: Miscellaneous Mix No: 4 5 Layer: Miscellaneous Layer: Leveling/Top Top Post Work, -10°C Mix HMA # GGSP 49A 239 GGSP 49C LVSP Post SD Work (lb*in.) (lb*in.) Post Work, -10°C HMA # Post SD Work (lb*in.) (lb*in.) Post Work, -10°C CV (%) Traffic 144 60 E50 813 247 30 E30 90A 0 0 0 51A 318 157 49 E30 203 49 49 101 LVSP 51B 0 0 0 E10 102 46 53 LVSP 51C 59 14 25 E10 105 15 31 LVSP 127 64 67 106 ASCRL 201 52 63 LVSP 208 0 0 CV (%) HMA# Post SD Work (lb*in.) (lb*in.) CV (%) 97 0 0 0 204 6 11 173 116 103 115 193 168 200 202 0 0 0 E10 209A 0 0 0 123 E10 209B 4 7 173 0 E3 67 269 108 40 68 112 48 43 E3 108 4 7 200 109 0 0 0 E3 111 16 28 173 112 0 0 0 E1 80 221 123 56 81 0 0 0 E1 85 367 178 48 86 251 148 59 206 0 0 0 E1 36 The average total fracture work of all mixtures was 340 lb*in. The lowest total fracture work was 174 lb*in., measured from mix 208 a Low Volume Superpave (LVSP) mixture. The highest total fracture work recorded was 1014 lb*in., measured from mix 49C a Gap Graded Superpave (GGSP) mixture. A comparison of the pre and post fracture work for all 62 mixtures tested in this study is depicted in Table 7 and Table 8. The average pre fracture work was 250 lb*in and the average post fracture work was 91 lb*in. The greatest pre fracture work was 377 lb*in., measured from mix 204 (5E30 High Stress). The lowest pre fracture work recorded was 174 lb*in, measured from mix 208 (LVSP). The highest post fracture work recorded was 813 lb*in., measured from mix 49C (GGSP). The lowest post fracture work recorded was 0 lb*in. Post fracture work of a mixture was generally less than pre fracture work and 16 of the 62 mixtures tested in this study had no measured post fracture work. The relationship between total fracture work and IDT strength is shown in Figure 8. While there is high scatter in the data, a general trend exists as IDT strength increases total fracture work decreases. This trend is reasonable as softer mixes can generally be expected to exhibit greater fracture work and lower IDT strength, while stiffer mixes have greater IDT strength and lower fracture work. 37 Total Fracture Work (lb*in) Total Fracture Work versus IDT Strength 1200 1000 800 600 400 200 0 0 100 200 300 400 500 600 IDT Strength (psi) Figure 8 Total fracture work versus IDT strength relationship 4.3 MDOT Mix Designation and IDT Strength The IDT strength values for each of the ESAL design categories was examined to investigate the use of the MDOT mixture classification systems ability to be used as a thermal cracking resistance parameter during design. Figure 9 shows the relationship between ESAL and IDT strengths of the asphalt mixtures tested. As shown, the IDT strength generally increases with the design ESAL of the mixtures. However a clear relationship is not visible. Some of the mixtures designated with ESAL of 1 million have higher IDT strength than mixtures designated with ESALs of 10, 30, and 50 million. This is meaningful because besides ESAL, there are many other factors affecting the IDT strength. A clear trend should not be anticipated since there are many variables (e.g., aggregate gradation, PG, VMA, VFA...etc.) that play a role in IDT strength. 38 IDT Strength of MDOT Mix Designation ESAL's IDT Strength (psi) 600 500 400 300 200 100 0 0 10 20 30 40 50 MDOT Mix ESAL Designation 60 Figure 9 Laboratory measured IDT strength for MDOT Mix ESAL designation categories for leveling and top course pavement layers Figure 10 shows the relationship between MDOT Mix ESAL designation and total fracture work. As shown, even though there is significant scatter in the data, a general decrease in fracture work is observed with increasing ESAL. As was seen with mixture IDT strength a clear trend should not be anticipated since there are many variables (e.g., aggregate gradation, PG, volumetrics) that affect a 39 mixture’s fracture work. Total Fracture Work (lb*in.) Total Fracture Work of MDOT Mix Designation ESAL's 700 600 500 400 300 200 100 0 0 10 20 30 40 50 60 MDOT Mix ESAL Designation Figure 10 Laboratory measured total fracture work for MDOT Mix ESAL designation categories for leveling and top course pavement layers 4.4 Superpave PG and IDT Strength Superpave performance grading (PG) is a binder characterization system developed to relate binder performance to the climatic conditions in which it will be utilized. For the PG grading process, binder undergoes a battery of tests including Rolling Thin Film Oven (RTFO), Pressure Aging Vessel (PAV), Rotational Viscometer (RV), Dynamic Shear Rheometer (DSR), Bending Beam Rheometer (BBR), and Direct Tension Tester (DDT). Based on the results of these tests, a PG is determined consisting of a high grade; the average seven-day maximum pavement temperature (°C), and a low grade; the minimum expected pavement temperature (°C) likely to be experienced. For instance, in the northern US, a binder graded PG 58-40 would be expected to outperform a PG 58-16 binder in regards to thermal cracking due to its greater low 40 PG classification. The IDT strength of the Michigan mixtures used in this study are depicted as a function their low PG (-22, -28, or -34) and their high PG (58, 64, or 70) in Figure 11 and Figure 12, respectively. IDT Stregnth (psi) IDT Strength at Superpave Low PG 600 500 400 300 200 100 0 16 22 28 34 40 Low PG (-) Figure 11 IDT strength versus Low Temperature PG relationship IDT Strength at Superpave High PG IDT Strength (psi) 600 500 400 300 200 100 0 52 58 64 70 76 High PG Figure 12 IDT strength for high PG characterization of Michigan asphalt mixtures 41 As shown, while there is scatter in the data, IDT strength generally decreases with an increase in low PG. This is somewhat meaningful since as low PG increases, the binder becomes softer (and less brittle). Soft binder perhaps leads to low IDT strength. Figure 12 shows the relationship between the high PG and IDT strength, where an increase in IDT strength is observed with increasing high PG. This is consistent with the trend with low PG where stiffer binder (higher the high PG) results in higher IDT strength. The relationship between total fracture work and low and high PG is shown in Figure 13 and Figure 14, respectively. As low PG increases total fracture work generally increases, although there is significant scatter in the data. This is somewhat expected as at a greater low PG the softer binder (less brittle) should exhibit greater fracture work. There is no clear relationship between high PG and total fracture work, as little difference is seen in total fracture work for Total Fracture Work (lb*in) different high PG (Figure 14). Total Fracture Work at Superpave Low PG 1200 1000 800 600 400 200 0 16 22 28 Low PG (-) 34 40 Figure 13 Fracture work for low temperature Superpave PG characterization of Michigan asphalt mixtures 42 Total Fracture Work (lb*in) Total Fracture Work at Superpave High PG 1200 1000 800 600 400 200 0 52 58 64 High PG 70 76 Figure 14 Fracture work for high temperature Superpave PG characterization of Michigan asphalt mixtures This is evidence of two important characteristics of low temperature performance characterization of asphalt mixtures. Firstly, although the Superpave PG system is an improvement upon binder classification methods binders can still have significantly different performance characteristics within a PG designation. Secondly IDT strength of an asphalt mixture is not a function of solely the type of binder used in mixture design. IDT strength cannot be evaluated based on PG or MDOT mix designation alone. Other mixture components such as aggregate source and gradation, volumetric, and mixture properties must be considered when examining the IDT strength of an asphalt mixture. Pavement engineers should use caution when anticipating increased IDT strength as a result of increasing the low temperature PG magnitude and should instead utilize laboratory testing or IDT strength prediction models to examine the effect of mixture design on thermal cracking resistance. 43 4.5 Warm Mix Asphalt IDT Properties A number of warm mix asphalt (WMA) mixtures where characterized with the IDT strength test in this study. A comparison of their IDT strength and total fracture work is shown in Figure 15 and Figure 16. Comparison of WMA and HMA mixtures was made between mixtures having similar PG, percent binder, and gradations, i.e. mixture 2A (HMA) was compared with mixture 2B (WMA) and mixture 209A (HMA) was compared to mixture 209B (WMA)(Appendix A). Mixture 208 (WMA) was not examined in this analysis, as it did not have a comparable HMA mixture. IDT Strength (psi) Comparison of WMA and HMA IDT Strength 500 400 300 HMA 200 WMA 100 0 51 2 Mixture 209 Figure 15 IDT strength for comparable WMA and HMA mixtures As shown in Figure 15, the WMA mixtures had lower IDT strength values as compared to their similar HMA mixtures. Figure 16 shows a comparison of total fracture work for the similar WMA and HMA mixtures. Generally it is shown that WMA mixtures tested in this study have higher total fracture work as compared to their similar HMA mixtures. 44 Total Fractrue Work (lb*in.) Comparison of WMA and HMA Total Fracture Work 500 400 HMA HMA 300 WMA WMA 200 100 0 51 2 Mixture 209 Figure 16 IDT fracture work for comparable WMA and HMA mixtures A comparison of post fracture work for WMA and HMA mixtures is shown in Figure 17. It is shown that all WMA mixtures have a greater post fracture work as compared to their similar HMA mixtures. It is noted that all HMA mixtures where shown to have zero or nominal post fracture work, a property that correlates to crack growth and propagation. When compared to tested HMA mixtures similar WMA mixtures tested in this study may be thought to exhibit slower rates of thermal cracking growth. 45 Post Fractrue Work (lb*in.) Comparison of WMA and HMA Post Fracture Work 500 400 HMA HMA 300 WMA WMA 200 100 0 51 2 Mixture 209 Figure 17 IDT post fracture work for comparable WMA and HMA mixtures 46 5. INDIRECT TENSILE STRENGTH PREDICTION MODELS 5.1 Introduction to Indirect Tensile Strength Prediction for Pavement ME Design In Pavement ME Design thermal cracking distress prediction directly depends on accurate material characterization, i.e. IDT strength at -10°C and creep compliance. Over prediction of IDT strength in Level 3 analysis of the Pavement ME Design can lead to higher thermal cracking rates while under prediction can lead to over designed pavements, both costly to state transportation agencies. Figure 18 depicts a preliminary sensitivity analysis of IDT strength input on thermal cracking prediction in Pavement ME Design. For a scenario of a 4” flexible pavement lift (PG 58-22) constructed in Detroit, MI the amount of thermal cracking was determined as a function of different IDT strength values. An IDT strength of 100 psi was used as it is the lower boundary limit of IDT strength input into Pavement ME Design while an IDT strength of 500 psi was used as it was generally a typical upper limit of IDT strength of the mixtures tested in this study. In Figure 18 it is shown that the amount of thermal cracking varies with IDT strength and thermal cracking prediction is dependent on the IDT strength value input into Pavement ME Design software. To successfully predict thermal cracking in Pavement ME Design it is necessary to accurately determine material inputs such as IDT strength. If testing is not possible or feasible, an accurate predictive equation for IDT strength is necessary to improve the predictions of Pavement ME Design. 47 Impact of IDT Strength on Pavement ME Design Level 3 Thermal Cracking Prediciton Thermal Cracking (ft/mi) 100 psi Tensile Strength 500 psi Tensile Strength 1800 1600 1400 1200 1000 800 600 400 200 0 0 5 10 Time (yrs) 15 20 Figure 18 Effect of IDT strength input in Pavement ME Design Level 3 thermal cracking analysis for a 4”, PG 58-22 flexible pavement constructed in Detroit, Michigan. In this study three models were developed to improve IDT strength prediction for Michigan mixtures; (i) a locally calibrated Pavement ME Design IDT strength model, (ii) a newly developed linear IDT strength model, and (iii) an artificial neural network (ANN) based model. The development of each IDT model is explained and then evaluated for prediction performance with respect to current Pavement ME Design IDT strength prediction. Increased IDT strength prediction performance has the potential to firstly increase Level 3 thermal cracking prediction accuracy with the use of more accurate material inputs. Secondly calibration or development of a model with adequate prediction performance could be utilized to predict IDT strength for Level 1 and 2 Pavement ME Design analyses, which are currently measured by laboratory testing. Lastly development of a model that utilizes inputs readily obtainable by 48 pavement designers and does not require costly and time consuming laboratory testing would be advantageous to state agencies. 5.2 Model Evaluation The performance of a Michigan calibrated Pavement ME Design IDT strength model and a newly developed IDT linear regression model were evaluated using goodness-of-fit statistics, visual inspection with respect to the line of equality (LOE), and local bias statistics. Goodness2 of-fit statistics include Se/Sy and R and are calculated as follows. ∑ ̂ ∑ ̅ √ √ (6) (7) ( ) Where: Se = Standard error of estimate, Sy = Standard deviation, 2 R = Correlation coefficient, y = Measured IDT strength, ̂ = Predicted IDT strength, ̅ = Mean value of measured IDT strength, 49 (8) n = Sample size k = Number of independent variables in the model Se/Sy is a measure of prediction improvement over the empirical model, a smaller Se/Sy 2 ratio is indicative of improved prediction by the model. The R is a measure of model accuracy, a value closer to 1 indicates better estimation by the model [31]. Evaluation by visual inspection is accomplished by examining the plotted measured versus predicted values with respect to the LOE. If the plotted values are fairly equally distributed around the LOE then the empirical model will generally exhibit good correlation to the measured data [30]. Slope and intercept are a measure of local bias in the empirical models and were calculated by fitting an unconstrained line of best fit to the measured versus predicted data in Microsoft Excel. Local bias statistics can indicate patterns of over prediction or under prediction by the empirical model that may not be discerned by either goodness-of-fit statistics or visual inspection [30]. 5.3 Local Calibration of Pavement ME Design Strength Prediction Model The first effort to improve Pavement ME Design IDT strength prediction performance was local calibration of the original IDT equation developed by Witczak et al [6] (Equation 5) for calculation of IDT strength in the TC Model. 36 of the 62 MDOT mixtures tested in this study were used in the local calibration process since only 36 of the binders where available for Penetration testing. It is noted that Penetration testing is an input to the Pavement ME IDT strength predictive model. Also, only these 36 mixtures had available binder characterization data, ARTFO and VTS, a required input into the Pavement ME Design IDT strength predictive 50 model. Air void and Penetration Grade values for the 36 mixtures used in the local calibration are listed inTable 9. ARTFO and VTS binder properties, measured as part of a larger material characterization project at Michigan State University, are listed in Table 9. Table 9 Binder and Mixture Properties of 36 MDOT Mixtures used in Michigan Calibration of the Pavement ME Design Strength Prediction Model Developed by Witczak Sample ID 2A 4 18B 20B 21 26A 26B 28B 29B 31A 31B 32A 37 44 45 47 48 49A 62 65 67 68 86 102 103 108 109 111 112 127 200 202 Pen77 Average (0.1 mm) 55.3 61.7 42.3 55.0 68.7 63.0 74.7 49.3 69.7 74.3 52.0 49.7 67.3 66.7 111.3 63.0 51.3 77.3 67.0 141.0 103.3 80.3 129.7 49.7 56.0 50.7 58.0 55.0 40.3 53.3 58.0 33.3 ARTFO VFA (%) Va (+-.5) (%) 9.550 7.519 9.935 8.201 8.604 10.265 9.697 9.926 10.207 7.783 8.146 7.819 9.817 8.494 11.701 8.170 9.066 7.553 10.039 10.220 7.540 7.795 7.611 9.540 9.978 9.709 9.605 7.616 7.904 10.162 8.720 9.903 71.98 70.01 70.51 68.66 68.30 68.40 68.56 69.32 68.31 68.62 68.91 67.36 68.60 69.82 68.27 69.86 68.30 69.37 72.39 67.98 71.82 70.35 68.44 70.49 70.03 70.58 70.59 70.10 69.47 69.63 69.89 67.96 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 51 Table 9 (cont’d) Sample ID 204 205 206 Pen77 Average (0.1 mm) 33.3 71.0 36.7 ARTFO VFA (%) Va (+-.5) (%) 8.017 10.119 9.388 68.49 70.85 71.14 7.00 7.00 7.00 For local calibration coefficients of the original Pavement ME Design IDT strength model (Equation 5) were varied using Microsoft Excel Solver package to reduce the sum of the squares between measured and Pavement ME Design predicted IDT strengths. Coefficient labeling of the original Pavement ME Design IDT strength model is shown in Equation 9. 2 2 St = C1 + (C2)Va + (C3)Va + (C4)VFA + (C5)VFA + (C6)log (Pen77) + (C7)log(ARTFO) (9) Values of the original Pavement ME Design IDT strength model coefficients before and after Michigan calibration are listed in Table 10. Table 10 Comparison of the original and Michigan calibrated Pavement ME Design IDT strength Model Calibration Coefficients Coefficient C1 C2 C3 C4 C5 C6 C7 IDT Prediction Model Michigan Original Pavement Calibrated Witczak ME Design Witczak Pavement ME Design 7416.7120 6377.5873 -114.0160 -112.9216 -0.3040 -0.3039 -122.5920 -122.5112 0.7040 0.8589 405.7100 -246.1319 -2039.2960 -346.4313 52 It is of note that the coefficient assigned to the Pen77 parameter changes both sign and magnitude (Table 10) in local calibration with the Michigan mixes. This is reasonable as softer binders are generally expected to have higher penetration and lower IDT strength. Thus the higher Pen 77 in the Michigan calibrated model the lower predicted IDT strength will be. Comparison of the measured versus predicted IDT strength values for the original and Michigan calibrated IDT strength models are plotted in Figure 19 and Figure 20, respectively. Visual inspection of the original Pavement ME Design IDT strength model shows points are poorly distributed with respect to the LOE while after calibration points are fairly well distributed along the LOE. Predicted IDT Strength (psi) 600 Uncalibrated Pavement ME Design IDT Strength Model 500 400 300 200 100 0 0 200 400 Measured IDT Strength (psi) 600 Figure 19 Original Pavement ME Design IDT Strength Model for 36 MDOT mixtures with respect to the LOE 53 Michigan Calibrated Pavement ME Design IDT Strength Model Predicted IDT Strength (psi) 600 500 400 300 200 100 0 0 200 400 Measured IDT Strength (psi) 600 Figure 20 Michigan Calibrated Pavement ME Design IDT Strength Model for 36 MDOT mixtures with respect to the LOE Table 11 overviews the performance evaluation criteria before and after local calibration. The Michigan calibrated Pavement ME Design model shows increased performance with a lower standard error of estimate/standard deviation, Se/Sy = 0.0598, and higher correlation coefficient, 2 R = 0.663, as compared to the original Pavement ME Design model. Local bias statistics, unconstrained slope and intercept, of the Michigan calibrated model are 0.5939 and 178.48, respectively, indicating a tendency of the calibrated model to under predict IDT strength. 54 Comparison of the original Pavement ME Design model before and after calibration shows substantially increased distribution around the LOE. Table 11 Comparison of model performance evaluation parameters measured for Original Pavement ME Design and Calibrated IDT strength prediction models for 36 MDOT asphalt mixtures Model Performance Measure R IDT Prediction Model Original Calibrated 0.000 0.598 4.436 0.663 Poorly distributed -0.0402 283.87 Well distributed 0.5939 178.48 2 Se/Sy Visual Inspection (LOE) Unrestrained Slope Unrestrained Intercept 5.4 Linear Strength Prediction Model The second effort to improve Pavement ME Design IDT strength prediction performance was development of new model using linear regression techniques. IBM © SPSS © Statistics software (SPSS) was used to perform a statistical analysis on variables with a potential impact on IDT strength. The purpose of the statistical analysis was to firstly determine if there was a relationship between measured IDT strength and mix design properties and volumetrics. Secondly, determine if the relationship is positive or negative. And thirdly determine the strength of the relationship between the two variables. Once the relationship of the mix design and volumetric variables to IDT strength was determined, linear regression was performed with parameters that significantly correlated to IDT strength to develop a linear model. In addition to a possible increase in IDT prediction performance, the advantage of such a model is the ease of 55 obtaining the input parameters. All inputs are readily obtainable by engineers via a MDOT Job Mix Formulas (JMFs) and do not require costly and often time consuming laboratory testing. A JMF is a document provided to the paving contractor containing detailed mix design information including mixture properties, volumetrics, gradation, compaction and placement temperatures, and other important mix information. A Pearson correlation analysis was performed using SPSS to determine which JMF variables where significantly correlated to IDT strength. When determining significant relationships, the p-value statistic was used. If the p-value is less than 0.05 then the correlation coefficient is considered to be significant at the 0.05 level and if the p-value is less than 0.01 then the correlation coefficient is considered to be significant at the 0.01 level. JMF parameters having a significance at least 0.05 were used in construction of a linear IDT strength model for this study. Table 12 summarizes the JMF parameters that correlated significantly with laboratory measured IDT strength, their respective p-values, and type of relationship (positive or negative). Table 12 MDOT JMF parameters found to be significantly correlated with measured IDT strength using a Pearson Correlation analysis. Correlation significance, either at the .01 or .05 level, and the relationship of the parameter, either positive (+) or negative (-), is also listed Correlated JMF Variable Polymer Modified High PG Low PG Fines/Asphalt Ratio Angularity % Passing 1/2" % Passing 3/8" % Passing #4 % Passing #8 % Passing #100 % Passing #200 % Air Voids Correlation Significance 0.01 0.01 0.01 0.05 0.01 0.01 0.01 0.01 0.05 0.05 0.05 --56 Relationship + + + + + + + + --- It is of note that laboratory measured IDT strength correlated with not only asphalt binder parameters (Polymer Modification, High and Low PG), but also with aggregate parameters (% Passing 1/2”, 3/8”, #4, #8, #100, and #200 sieves and the Fines/Asphalt Ratio). This is evidence that aggregate gradation is also a significant factor influencing low temperature IDT strength in addition to asphalt binder properties. For development of a linear Pavement ME Design IDT strength predictive equation, significantly correlated JMF parameters (Table 12) were assigned coefficients (Equation 10) and then varied using Microsoft Excel Solver package to reduce the sum of the squares between laboratory measured and linear model predicted IDT strengths. Due to the small range of air voids tested in this study, 6.5 – 7.5%, air voids were not found to be significantly correlated to IDT strength. However the importance of accounting for the effect of air voids on IDT strength is recognized and thus is included as a parameter in the linear strength predictive equation. St = C1 + C2PM + C3PGHigh + C4PGLow + C5ANG + C6FAR + C7P1/2” + C8P3/8” + C9P#4 + C10P#8 + C11P#100 + C12P#200 + C13AV (10) The value of the parameter coefficients and the resulting linear model is shown in Equation 11. St = -9.901 + 20.737PM + 2.674PGHigh - 6.407PGLow + .669ANG + 356.593FAR + 1.027P1/2” + 2.517P3/8” – 3.768P#4 + 5.151P#8 + 3.452P#100 – 62.733P#200 - .017AV (11) 57 Where: PM = Polymer Modification Factor, either 1 for polymer modified or 0 for unmodified binder PGHigh = Magnitude of high PG PGLow = Magnitude of low PG ANG = Angularity, % FAR = Fines/Asphalt Ratio P1/2” = Percent passing the 1/2” sieve P3/8” = Percent passing the 3/8” sieve P#4 = Percent passing the #4 sieve P#8 = Percent passing the #8 sieve P#100 = Percent passing the #100 sieve P#200 = Percent passing the #200 sieve AV = Percent Air Voids Comparison of the measured versus predicted IDT strength values for the original Pavement ME Design and linear IDT strength models are plotted in Figure 21 and Figure 24, respectively. It is noted that predicted Pavement ME Design IDT strength in Figure 21 is the software output IDT strength, as opposed to prediction by the original IDT equation developed by Witczak et al [6] used in the previous section. The main difference is that binder properties, 58 ARTFO and Pen77, are predicted from PG. For output of IDT strength prediction in Pavement ME Design the PG, design air voids (%), and effective binder content, Pbe (%) are entered into the design guide software and IDT strength is immediately calculated. Visual inspection of the original Pavement ME Design IDT strength model shows points are poorly distributed with respect to the LOE while for the linear IDT strength model points are fairly well distributed along the LOE. Predicted IDT Stregnth (psi) Prediction of IDT Strength by Pavement ME Design Software 1000 900 800 700 600 500 400 300 200 100 0 0 200 400 600 800 Measured IDT Strength (psi) 1000 Figure 21 IDT strength predicated by Pavement ME Design software versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures Development of a linear IDT strength predictive model was accomplished using all specimens tested in this study (202 mixtures). A comparison of measured versus predicted IDT strengths for calibration, testing, and all stages is shown in Figure 22, Figure 23, and Figure 24 respectively. 59 Predicted IDT Strength (psi) Linear Calibration, R2 = 0.679 600 500 400 300 200 100 0 0 100 200 300 400 500 600 Measured IDT Strength (psi) Figure 22 IDT strength predicated during calibration by newly developed linear model versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures Predicted IDT Strength (psi) Linear Testing, R2 = 0.509 600 500 400 300 200 100 0 0 100 200 300 400 500 600 Measured IDT Strength (psi) (psi) Figure 23 IDT strength predicated during testing by newly developed linear model versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures 60 Predicited IDT Stren(lb*in) Linear All, R2 = .648 600 500 400 300 200 100 0 0 100 200 300 400 Measured IDT Strength (psi) 500 600 Figure 24 IDT strength predicated for all specimens by newly developed linear model versus laboratory measured IDT strength for commonly used State of Michigan asphalt mixtures A comparison of model performance evaluation criteria for the original Pavement ME Design and linear IDT strength models are listed in Table 13 along with the number of unique sample used for each stage of development. Table 13 Comparison of performance criteria for the original Pavement ME Design and linear IDT strength prediction models for commonly used MDOT asphalt mixtures Model Performance Measure Unique Samples R 2 Se/Sy IDT Predictive Equation Pavement ME Cal. Test All 62 161 40 201 0.006 0.679 0.509 0.648 6.954 0.594 0.887 0.615 61 The linear IDT strength model shows increased performance with a lower standard error 2 of estimate/standard deviation, Se/Sy = 0.615, and higher correlation coefficient, R = 0.648, as compared to the original Pavement ME Design model. Local bias statistics, unconstrained slope and intercept, of the Michigan calibrated model are 0.69 and 130.24, respectively, indicating a trend of the calibrated model to under predict IDT strength as was seen in the Michigan calibrated Pavement ME Design IDT strength model discussed previously. 5.5 Artificial Neural Network Prediction Model The third effort to improve Pavement ME Design IDT strength prediction performance was development of an Artificial Neural Network (ANN) using the strength and mix design properties and volumetrics data in this study. An ANN can most simply be defined as a computational model used to predict a desired output from a set of inputs. Unlike regression techniques, the ANN concept is modeled after living neural networks, giving it the capability to learn and recognize patterns. Inputs into an ANN are assigned weights and thresholds which are varied by functions in a network of layers within the ANN. Ultimately the ANN adjusts the weights and thresholds within the layers to predict a desired output. First used in the field of computer science ANNs are now used widely in the field of civil engineering [5], including pavement engineering. In the pavement engineering field ANNs have been employed to successfully estimate pavement layer thickness [15], IDT strength [14], reflective cracking [9], base layer moduli [33], roughness and permeability [11] [32], and rutting and fatigue distresses [19]. Notably, ANN modeling techniques have also been employed in the Pavement ME Design [6]. 62 5.5.1 Structure of the IDT Strength ANN The ANN developed for the prediction of IDT strength in this study consists of a feed forward (back propagation) network of one hidden layer and one output layer (Figure 25). This structure was determined through a trial and error using the readily available MATLAB neural network toolbox [12]. Figure 25 Structure of the ANN model developed for prediction of IDT strength for Michigan asphalt mixtures 5.5.2 Overview of IDT Strength Prediction with the ANN Forward computation of IDT strength, y, in this ANN model was determined from the following 15 inputs hereby referred to as p, a 15 x1 input vector. Inputs into the ANN developed as part of this study were the following: 63 PM = Polymer Modification Factor, either 1 for polymer modified binder or 0 for unmodified binder PGHigh = Magnitude of high PG PGLow = Magnitude of low PG ANG = Angularity, % FAR = Fines/Asphalt Ratio P1/2” = Percent passing the 1/2” sieve P3/8” = Percent passing the 3/8” sieve P#4 = Percent passing the #4 sieve P#8 = Percent passing the #8 sieve P#16 = Percent passing the #16 sieve P#30 = Percent passing the #30 sieve P#100 = Percent passing the #100 sieve P#200 = Percent passing the #200 sieve RAP = Percent Recycled Asphalt Pavement (RAP) AV = Percent Air Voids The process of forward computation in an ANN is completed according to the following steps. H Step 1) The output of the hidden layer, a a 15 x 1 vector, is computed using Equations 12 and 13. H H H n =W p+b 64 (12) H H a = tansig(n ) (13) Where: (14) And: H W = The matrix weight vector, 12 x 14 H b = The bias vector of the hidden layer, 12 x 1 H Step 2) With the output hidden layer, a , the output of the output layer, y, is computed using Equation 15 and 16. o o H o n =W a +b o y = purelin(n ) (15) (16) Where: o W = The matrix weight vector, 1 x 12 o b = The bias constant of the output layer, 12 x 1 5.5.2 Training of the IDT Strength ANN The ANN was then trained with laboratory measured IDT strength data gathered from testing of all 62 unique MDOT mixtures used in this study. To increase training accuracy, 65 individual IDT strength tests, generally 3 replicates for each mixture, were used in the ANN training procedure resulting in a total of 183 data points. For the training procedure, weights and biases are varied randomly and repeatedly until the predicted output (i.e. IDT strength) approaches the measured IDT strength, such that difference between the two is minimized. Error minimization is measured as the mean square error between measured and predicted IDT strength and decreases as the number of repetitions increases (Figure 26). Figure 26 Reduction in mean squared error of laboratory measured and ANN predicted IDT strength values during training, validation, and testing stages of ANN development 66 Figure 27 ANN predicted IDT strength versus measured IDT strength (base 10) for the training, validation, testing, and all data used in ANN development 2 Performance of the trained ANN was evaluated with the goodness-of-fit statistic, R , and 2 visual inspection with respect to the LOE. R for the trained IDT strength ANN was 0.828 and data points were fairly well distributed around the LOE (Figure 27). 67 5.5.3 Testing of the IDT Strength ANN Final validation of the IDT strength ANN was completed using 20 individual IDT strength tests set aside from the original 201 strength tests used in the training and validation steps. These 20 tests were input into the IDT ANN feed forward computation model and the predicted versus measured IDT strength values where evaluated (Figure 27). The IDT strength 2 2 ANN showed an acceptable correlation coefficient, R = 0.806, for testing (Figure 27). R for all IDT strength ANN data was 0.835 and data points were fairly well distributed around the LOE (Figure 28). A summary of specimens used and correlation coefficients for each step of ANN ANN Predicted IDT Strength (psi) development and is shown in Table 14. Measured Versus ANN Predicted IDT Strength, R2 = 0.835 600 500 400 300 200 100 0 0 100 200 300 400 Measured IDT Strength (psi) 500 600 Figure 28 ANN Predicated versus measured IDT strength values for all mixtures used in ANN development 68 Table 14 Overview of specimens used and correlation coefficients for each stage of IDT ANN development ANN Development Stage # Unique Tests R Training 160 0.828 Validation 21 0.904 Testing 20 0.806 All 201 0.835 69 2 6. CONCLUSIONS AND RECOMMENDATIONS Accurate low temperature material characterization is critical for successful design of flexible pavements such that they resist thermal cracking in the field. The indirect tensile (IDT) strength of an asphalt mixture is an important parameter used in characterization of its thermal cracking resistance. This research investigated the IDT strength characteristics of numerous asphalt mixtures commonly used in the State of Michigan. The research program also included investigation of the ability of Pavement ME Design Guide in predicting IDT strength of the asphalt mixtures from the constituent properties in Level 3 analysis. In an effort to improve IDT strength prediction for use in Pavement ME Design Guide, new IDT strength predictive models were developed. First, the current Pavement ME Design Guide IDT strength predictive model was locally calibrated with the Michigan mixtures tested in this study. Second a new IDT strength predictive model was developed using linear regression techniques. Lastly, an Artificial Neural Network (ANN) was trained and validated using the Michigan mixtures. All inputs in the newly developed and ANN IDT strength models can easily be obtained by designers from mix design Job Mix Formulas (JMFs). Based on the foregoing, the following major conclusions were drawn:  In 62 different Michigan mixtures tested, a wide variety of IDT strength and fracture work values were observed. The IDT strength and fracture work were affected by factors such as the aggregate gradation, binder PG, and aggregate angularity of the asphalt mixtures.  Direct relationship between the IDT strength as well as fracture work to binder Performance Grade (PG) and MDOT mixture designation was not observed. Generally, stiff binders resulted in higher low temperature IDT strength and lower fracture work. 70  Level 3 IDT strength predictions of Pavement ME Design Guide were very poor for the Michigan asphalt mixtures. All three predictive models developed in this study showed improved IDT strength prediction performance as compared to Pavement ME Design Guide Level 3 IDT strength prediction. It is recommend that pavement designers in the State of Michigan exercise caution when relying on low PG or MDOT mix designation as a method to increase or decrease IDT strength and when using the IDT strength predictive equation in Pavement ME Design Guide Level 3 thermal cracking analysis. To determine mixture low temperate IDT strength, the models developed in this study should be used instead (depending on the inputs available). 71 APPENDICES 72 APPENDIX A: MIX PROPERTIES AND VOLUMETRICS OF MIXTURES TESTED 73 Table 15 Mixture properties and volumterics of mixtures tested Measured Corrected Peak Sample Tensile Tensile ID Strength Strength (psi) (psi) 2A 562 477 2B 414 362 (WMA) 4 570 483 18A 391 343 18B 544 463 20A 530 452 20B 524 448 20C 457 395 21 533 454 Polymer FE Modified Post (1-yes, 0(lb*in) no) PG High Grad e PG Low Grad e RAP (%) Mix Type Pb (%) (JMF) 0 64 22 17 3E30 4.90 158 0 64 28 17 3E30 4.90 300 228 244 255 263 247 281 115 137 30 3 78 115 0 1 0 0 0 0 0 0 70 58 58 64 64 64 64 28 22 22 28 28 28 28 16 19 19 18 20 20 21 4E30 3E10 3E10 4E10 5E10 4E10 5E10 4E10 High Stress 5E10 5E10 3E3 3E3 3E3 4E3 4E3 5E3 5E3 4E3 4E3 5E3 5E3 High Stress 5.31 5.20 5.04 5.23 5.53 5.58 6.01 FE Total (lb*in) FE Pre (lb*in) 280 275 5 419 261 415 365 273 258 341 362 281 23 542 462 446 320 125 1 70 28 16 24A 24B 26A 26B 26C 28A 28B 29A 29B 31A 31B 32A 428 589 463 384 394 570 484 462 496 518 553 540 372 498 400 338 346 483 416 399 426 442 470 460 527 459 412 430 349 225 185 280 202 281 283 327 287 335 247 220 247 225 183 260 198 254 279 291 240 123 165 210 102 0 2 20 4 27 4 35 0 1 0 0 0 0 0 0 0 1 1 1 70 70 58 58 58 64 64 64 64 70 70 70 28 28 22 28 28 28 28 28 28 28 28 28 16 19 19 24 28 21 19 16 21 19 21 16 32B 531 453 406 275 131 1 70 28 22 74 4.94 6.29 5.78 5.60 5.30 5.43 5.40 5.43 5.99 5.92 5.62 5.40 5.99 6.08 Table 15 (cont’d) Measured Corrected Peak Sample Tensile Tensile ID Strength Strength (psi) (psi) 44 470 405 45 395 346 Polymer FE Modified Post (1-yes, 0(lb*in) no) FE Total (lb*in) FE Pre (lb*in) 226 323 226 252 0 71 PG High Grad e PG Low Grad e RAP (%) 0 0 58 58 28 28 25 24 Mix Type Pb (%) (JMF) 47 506 433 245 245 0 0 64 28 25 48 491 422 213 213 0 0 64 28 30 49A 49B 51A 51B 51C (WMA) 62 64 65 447 382 396 470 387 336 347 405 499 1014 544 215 260 200 226 215 239 813 318 0 1 1 0 0 70 70 58 58 28 28 28 28 0 0 15 30 4E1 5E1 4E1 High Stress 5E1 High Stress GGSP GGSP LVSP LVSP 437 379 294 236 59 0 58 28 15 LVSP 5.60 480 448 415 413 388 362 508 246 324 265 202 274 243 43 50 0 0 0 58 58 58 28 34 34 10 19 20 4.89 5.40 6.00 67 466 402 522 253 269 1 64 34 15 68 476 410 405 292 112 1 64 34 17 80 81 85 474 409 467 409 357 403 537 193 622 295 193 254 241 0 367 0 0 1 58 58 64 34 34 34 21 20 17 86 486 417 538 287 251 1 64 34 21 90 534 455 182 182 0 1 70 22 18 3E3 4E3 5E3 4E3 High Stress 5E3 High Stress 4E1 5E1 4E1 HS 5E1 High Stress 4E30 75 5.35 5.98 5.29 5.91 6.18 6.12 6.24 5.36 5.10 5.46 5.45 5.66 5.48 6.14 4.98 Table 15 (cont’d) Measured Corrected Peak Sample Tensile Tensile ID Strength Strength (psi) (psi) 102 575 487 103 498 427 Polymer FE Modified Post (1-yes, 0(lb*in) no) FE Total (lb*in) FE Pre (lb*in) 343 333 297 218 46 115 PG High Grad e PG Low Grad e RAP (%) 0 0 64 64 22 22 20 19 Mix Type Pb (%) (JMF) 105 526 449 312 297 15 1 70 22 14 108 109 549 566 467 480 302 241 298 241 4 0 0 0 64 64 22 22 20 18 111 607 512 338 321 16 1 70 22 20 112 634 533 238 238 0 1 70 22 19 127 200 201 202 450 570 304 606 389 483 276 512 307 242 232 185 243 242 180 185 64 0 52 0 0 0 0 0 58 58 64 64 22 28 28 22 23 25 203 529 451 337 289 49 1 70 22 14 204 668 560 383 377 6 1 70 22 15 205 206 208 WMA 209 HMA 209 WMA 363 551 321 468 178 178 0 0 0 58 64 28 22 25 15 4E10 5E10 4E10 High Stress 4E3 5E3 4E3 High Stress 5E3 High Stress LVSP 3E10 ASCRL 5E10 4E30 High Stress 5E30 High Stress 2E3 5E1 496 425 174 174 0 0 64 22 30 LVSP 5.60 532 453 200 200 0 0 64 22 21 5E10 6.21 487 419 196 192 4 0 64 22 21 5E10 6.21 76 21 5.20 5.60 5.08 5.21 5.50 5.31 5.80 5.43 5.20 3.30 6.03 4.99 5.80 4.90 5.40 Table 15 (cont’d) Sample ID 2A 2B (WMA) 4 18A 18B 20A 20B 20C 21 23 24A 24B 26A 26B VMA Angulari VFA % Air ty 13.9 4 14.0 2 15.0 4 14.1 6 13.5 2 15.0 5 14.9 7 14.8 3 16.3 4 14.4 0 16.0 4 15.9 4 14.1 7 13.8 0 78.4 7 78.6 7 73.5 1 78.8 1 77.8 1 73.4 9 73.2 8 76.4 0 75.5 8 75.6 9 75.0 6 78.0 4 78.8 3 78.1 7 Gmm Gmb Gb Gse Gsb Pbe Fines/ Asphalt Ratio Crushed Face 1 1-1/2" 3.00 46.00 2.545 2.469 1.027 2.755 2.728 4.55 1.100 99.60 100.00 3.00 46.00 2.508 2.433 1.029 2.708 2.691 - 0.960 98.30 100.00 4.00 45.30 2.510 2.410 1.025 2.732 2.686 4.70 1.040 94.90 100.00 3.00 46.00 2.534 2.458 1.018 2.760 2.715 4.62 1.130 99.70 100.00 3.00 41.30 2.502 2.427 1.023 2.710 2.665 - 0.990 92.30 100.00 4.00 45.20 2.506 2.406 1.029 2.722 2.684 4.72 1.000 85.90 100.00 4.00 45.00 2.485 2.386 1.029 2.710 2.651 4.73 1.230 92.30 100.00 3.50 45.20 2.489 2.402 1.032 2.715 2.663 - 0.940 92.70 100.00 4.00 45.30 2.481 2.382 1.029 2.727 2.676 5.33 1.010 94.80 100.00 3.50 46.00 2.578 2.488 1.030 2.796 2.763 - 0.950 92.70 100.00 4.00 45.40 2.426 2.329 1.031 2.668 2.599 5.33 1.090 95.50 100.00 3.50 45.00 2.531 2.422 1.030 2.779 2.737 - 1.070 86.60 100.00 3.00 45.00 2.538 2.462 1.018 2.785 2.708 4.62 1.130 99.50 100.00 3.00 42.10 2.490 2.415 1.020 2.709 2.653 4.55 0.960 96.90 100.00 77 Table 15 (cont’d) Sample ID 28A 28B 29A 29B 31A 31B 32A 32B 37 44 45 47 48 49A VMA Angulari VFA % Air ty 14.7 5 15.0 6 15.7 4 16.0 7 15.2 7 14.7 1 15.7 1 16.2 0 16.5 2 15.0 7 16.2 2 14.8 8 16.0 2 17.5 9 72.8 7 73.4 4 74.5 9 75.1 1 73.7 6 72.8 1 74.5 4 75.3 1 75.7 8 73.4 6 75.3 8 73.1 2 75.0 3 77.3 5 Gmm Gmb Gb Gse Gsb Pbe Fines/ Asphalt Ratio Crushed Face 1 1-1/2" 4.00 41.20 2.471 2.372 1.028 2.686 2.632 4.66 1.160 90.40 100.00 4.00 41.70 2.490 2.390 1.028 2.711 2.661 4.76 1.070 90.40 100.00 4.00 43.40 2.457 2.359 1.028 2.696 2.632 5.12 1.060 90.60 100.00 4.00 43.00 2.463 2.364 1.028 2.700 2.650 5.24 0.930 76.60 100.00 4.00 41.20 2.471 2.372 1.017 2.701 2.642 4.83 0.970 95.00 100.00 4.00 41.20 2.472 2.373 1.031 2.686 2.632 4.66 1.160 90.40 100.00 4.00 43.40 2.458 2.360 1.031 2.696 2.632 5.12 1.060 90.60 100.00 4.00 41.70 2.450 2.352 1.017 2.696 2.636 5.27 0.950 94.80 100.00 4.00 42.60 2.494 2.395 1.032 2.743 2.696 5.39 1.090 93.80 100.00 4.00 42.10 2.475 2.376 1.020 2.692 2.648 4.75 0.930 88.50 100.00 4.00 42.40 2.454 2.356 1.020 2.695 2.644 5.29 1.020 97.20 100.00 4.00 42.60 2.504 2.404 1.029 2.722 2.675 4.66 1.140 85.50 100.00 4.00 41.90 2.474 2.375 1.029 2.713 2.661 5.21 1.170 92.80 100.00 4.00 48.90 2.535 2.434 1.025 2.808 2.771 5.72 1.430 100.00 100.00 78 Table 15 (cont’d) Sample ID 51A 51B 51C (WMA) 62 64 65 67 68 80 81 85 86 90 97 VMA Angulari VFA % Air ty 16.5 1 14.7 2 15.3 7 14.1 7 15.0 0 16.1 0 15.4 0 15.7 8 15.2 0 16.1 1 15.2 0 16.0 0 14.7 3 15.9 75.8 0 76.2 2 77.3 3 78.8 2 73.3 0 75.2 0 74.1 0 75.6 5 73.7 0 75.2 0 77.0 0 81.2 0 76.2 3 74.8 Gmm Gmb Gb Gse Gsb Pbe Fines/ Asphalt Ratio Crushed Face 1 1-1/2" 4.00 - 2.474 2.375 1.032 2.727 2.667 5.44 0.860 98.90 100.00 3.50 - 2.483 2.396 1.024 2.701 2.659 - 1.080 74.70 100.00 3.50 - 2.468 2.382 1.024 2.693 2.657 - 0.880 95.40 100.00 3.00 42.90 2.589 2.512 1.032 2.807 2.783 4.59 0.760 98.40 100.00 4.00 41.00 2.462 2.364 1.023 2.679 2.629 4.74 0.950 75.30 100.00 4.00 43.20 2.468 2.369 1.023 2.712 2.655 5.24 0.910 81.80 100.00 4.00 42.10 2.565 2.463 1.026 2.789 2.764 4.75 1.050 96.30 100.00 4.00 42.80 2.537 2.436 1.026 2.773 2.734 4.96 1.050 94.70 100.00 4.00 41.80 2.511 2.411 1.026 2.740 2.688 4.77 1.170 89.30 100.00 4.00 42.80 2.523 2.422 1.026 2.765 2.724 5.13 1.130 88.80 100.00 3.50 43.20 2.497 2.410 1.033 2.721 2.686 - 1.080 87.70 100.00 3.50 42.50 2.471 2.397 1.033 2.718 2.678 - 1.020 75.00 100.00 3.50 47.00 2.547 2.458 1.023 2.763 2.739 - 1.200 97.00 100.00 4.00 46.00 2.537 2.436 1.023 2.776 2.738 1.240 99.80 100.00 79 Table 15 (cont’d) Sample ID 102 103 105 108 109 111 112 127 200 VMA 14.9 6 16.0 6 15.2 3 15.0 5 16.0 8 15.0 9 16.3 9 15.2 3 13.7 0 201 202 203 204 205 16.1 9 14.8 5 15.7 7 13.2 3 Angulari VFA % Air ty 73.2 5 75.1 0 73.7 4 73.4 3 75.1 2 73.5 0 75.5 9 73.7 4 78.2 2 75.3 6 73.0 7 74.6 3 77.3 2 Gmm Gmb Gb Gse Gsb Pbe Fines/ Asphalt Ratio Crushed Face 1 1-1/2" 4.00 46.00 2.550 2.448 1.027 2.776 2.729 4.60 1.220 99.50 100.00 4.00 45.00 2.498 2.398 1.027 2.730 2.697 5.17 1.160 92.30 100.00 4.00 46.00 2.536 2.434 1.025 2.753 2.726 4.73 1.160 95.50 100.00 4.00 46.00 2.541 2.439 1.027 2.765 2.722 4.65 1.220 97.90 100.00 4.00 45.00 2.493 2.393 1.027 2.719 2.695 5.18 1.240 98.60 100.00 4.00 46.00 2.544 2.443 1.025 2.775 2.724 4.66 1.220 99.20 100.00 4.00 45.00 2.489 2.389 1.025 2.729 2.692 5.31 1.150 99.80 100.00 4.00 - 2.522 2.421 1.022 2.754 2.701 4.74 1.180 93.50 100.00 3.00 43.20 2.513 2.438 1.024 2.731 2.678 4.50 1.130 82.00 100.00 - 3.30 2.734 1.026 2.835 2.775 2.54 1.090 100.00 100.00 4.00 45.60 2.482 2.383 1.031 2.728 2.672 5.29 1.140 95.20 100.00 4.00 47.00 2.510 2.410 1.025 2.717 2.689 4.62 1.190 99.30 100.00 4.00 47.00 2.524 2.423 1.025 2.774 2.710 4.98 1.230 99.80 100.00 3.00 42.10 2.502 2.427 1.020 2.704 2.660 4.31 1.052 95.90 100.00 80 Table 15 (cont’d) Sample ID 206 208 WMA 209 HMA 209 WMA VMA Angulari VFA % Air ty 16.0 8 14.7 5 15.8 9 15.8 9 75.1 3 76.2 7 77.9 7 77.9 7 Gmm Gmb Gb Gse Gsb Pbe Fines/ Asphalt Ratio Crushed Face 1 1-1/2" 4.00 45.00 2.503 2.403 1.027 2.727 2.709 5.16 1.250 97.90 100.00 3.50 - 2.461 2.375 1.034 2.680 2.630 - 0.920 85.00 100.00 3.50 45.00 2.476 2.389 1.209 2.730 2.664 - 0.920 95.00 100.00 3.50 45.00 2.476 2.389 1.209 2.730 2.664 - 0.920 95.00 100.00 81 Table 15 (cont’d) Sample ID 2A 2B (WMA) 4 18A 18B 20A 20B 20C 21 23 24A 24B 26A 26B 26C 28A 28B 29A 29B 31A 31B 32A 32B 37 44 45 47 1/2" 3/8" No. 4 No. 8 No. 16 No. 30 No. 50 No. 100 No. 200 100.00 100.00 83.00 72.30 47.30 34.90 26.00 18.20 9.30 6.10 5.00 100.00 100.00 88.10 77.10 57.60 40.90 27.70 19.50 12.70 7.50 4.50 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 98.80 84.50 88.80 98.80 93.40 93.20 100.00 91.60 100.00 100.00 88.10 89.80 86.10 98.90 90.10 100.00 100.00 93.90 98.90 100.00 100.00 100.00 93.70 100.00 93.50 88.60 73.40 84.30 89.50 90.40 88.60 99.20 83.00 95.70 97.80 78.40 80.70 80.70 89.60 84.40 97.90 96.90 87.80 89.60 97.90 96.70 92.50 86.20 96.60 87.10 73.20 49.40 65.80 71.10 83.40 73.50 83.60 68.30 80.10 86.80 52.60 63.60 63.30 71.50 71.20 80.30 77.40 72.00 71.50 80.30 77.80 70.10 73.30 77.40 76.40 56.30 34.70 46.20 53.50 56.20 54.00 66.30 50.00 58.00 61.80 33.00 46.30 49.00 57.00 55.70 59.60 59.00 56.70 57.00 59.60 58.20 58.60 54.80 57.80 57.20 38.00 25.70 33.90 36.30 36.70 40.70 46.50 35.90 39.90 44.30 22.10 35.60 41.40 46.30 44.20 44.90 46.40 43.90 46.30 44.90 45.10 50.30 41.80 45.10 41.30 25.20 20.20 25.50 23.50 25.60 30.80 31.20 25.60 28.70 32.30 15.60 26.60 32.60 35.90 32.20 32.90 33.20 32.60 35.90 32.90 34.20 41.10 30.60 34.40 29.90 14.70 11.50 16.30 13.10 15.80 19.40 17.30 14.40 16.20 18.30 10.90 13.90 14.20 15.60 16.10 15.20 16.10 16.30 15.60 15.20 191.00 21.90 16.10 18.60 16.60 7.80 6.90 7.40 7.40 8.40 8.60 8.70 6.80 7.70 9.00 7.20 6.50 6.20 7.00 7.40 7.20 7.10 6.90 7.00 7.20 7.40 8.70 6.60 8.00 8.00 4.90 5.20 4.40 4.70 5.80 4.60 5.40 4.30 5.80 5.60 5.20 4.40 4.50 5.40 5.10 5.40 4.90 4.70 5.40 5.40 5.00 5.90 4.40 5.40 5.30 1" 3/4" 100.00 100.00 98.10 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 82 Table 15 (cont’d) Sample ID 1" 3/4" 1/2" 3/8" No. 4 No. 8 No. 16 No. 30 No. 50 48 49A 49B 51A 51B 51C (WMA) 62 64 65 67 68 80 81 85 86 90 97 102 103 105 108 109 111 112 127 200 201 202 203 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 100.00 99.90 96.00 100.00 100.00 100.00 94.60 96.10 94.80 91.90 91.20 86.50 95.00 100.00 95.90 100.00 98.20 100.00 93.70 100.00 98.20 100.00 98.50 100.00 99.30 98.70 100.00 98.90 100.00 92.50 88.90 59.50 100.00 96.40 99.70 70.00 79.70 83.20 84.80 85.70 76.10 86.90 97.40 84.30 95.40 89.90 97.40 84.40 97.00 85.60 99.70 88.60 99.90 88.30 87.30 99.60 87.60 99.90 86.80 82.60 30.20 99.70 87.10 83.30 26.60 31.80 58.70 72.40 71.40 56.90 72.50 75.20 64.80 73.60 69.30 75.20 66.40 80.20 63.60 77.70 65.10 75.90 63.00 65.10 75.60 66.50 75.80 79.20 65.00 14.70 84.10 52.30 63.00 20.50 22.10 44.60 57.20 56.70 45.40 56.70 56.70 56.20 59.90 54.00 56.40 53.50 62.20 44.20 53.90 45.00 54.70 42.20 46.50 51.40 47.30 54.90 58.50 48.40 11.50 66.70 33.60 49.80 16.60 17.80 35.90 45.40 43.90 34.40 43.50 42.50 45.00 47.80 41.10 43.60 42.60 47.80 31.00 37.20 30.30 39.10 28.10 32.30 36.50 33.90 39.20 43.20 34.10 9.10 46.80 22.40 83 36.70 13.00 14.40 27.40 35.50 30.80 23.10 32.20 31.10 30.90 33.90 30.00 31.00 26.90 33.80 22.00 26.20 21.50 29.50 19.40 23.30 27.40 24.40 29.10 32.60 22.50 7.20 31.50 15.90 20.00 10.40 11.80 14.00 19.50 14.80 14.60 15.50 15.50 20.10 21.60 18.60 16.80 11.20 18.20 14.00 14.80 13.50 18.00 12.90 14.90 17.60 15.80 18.20 20.90 12.00 6.00 16.60 10.90 No. 100 9.20 8.90 9.70 7.10 7.90 7.30 6.10 6.20 6.60 8.20 8.80 8.40 8.60 7.00 8.20 7.50 9.10 7.80 9.80 7.70 8.10 9.60 8.20 8.40 10.30 7.30 4.60 8.70 7.10 No. 200 6.10 8.20 8.10 4.70 5.20 4.50 3.50 4.50 4.80 5.00 5.20 5.60 5.80 5.40 5.70 5.60 6.20 5.60 6.00 5.50 5.70 6.40 5.70 6.10 5.60 5.10 3.60 6.00 5.50 Table 15 (cont’d) Sample ID 1" 205 206 208 WMA 209 HMA 209 WMA 100.00 100.00 100.00 100.00 100.00 3/4" 1/2" 90.00 73.50 100.00 100.00 100.00 94.20 100.00 100.00 100.00 100.00 3/8" No. 4 No. 8 No. 16 No. 30 No. 50 69.70 99.70 86.10 97.80 97.80 57.40 78.00 65.20 77.60 77.60 44.50 53.90 48.70 52.70 52.70 35.30 38.60 39.40 37.40 37.40 84 25.50 29.10 32.40 25.90 25.90 12.60 18.00 15.60 14.20 14.20 No. 100 5.90 9.60 6.40 7.30 7.30 No. 200 4.40 6.40 4.50 4.90 4.90 APPENDIX B: IDT STRENGTH, FRACTURE WORK, AND VOLUMTERICS OF SPECIMENS TESTED 85 Table 16 IDT Strength, Fracture Work, and Air Voids of Specimens Tested Mix 2A 2B 4 18A 18B 20A 20B Sample 2A-1-A 2A-3-A 2A-1-B 2B-2-A 2B-3-B 2B-2-C 4-1-A 4-3-A 4-1-B 4-3-B 18-2-2 18-1-B 18-1-C 18-3-C 18B-2A 18B-1B 18B-2B 18B-3B 20A-3A 20A-1B 20A-3B 20B-1A 20B-3A 20B-1B 20B-3B VA (%) 7.6 7.3 7.2 6.6 7.4 7.1 7.1 7.1 7.1 6.9 7.4 7.4 6.4 6.6 IDT IDT Strength Strength Average (psi) (psi) 452.5 495.9 477 482.2 380.5 365.8 362 338.5 497.2 459.5 483 478.0 497.3 276.8 338.1 343 368.4 388.8 6.7 450.4 6.4 466.8 SD (psi) CV (%) 22.19 4.65 21.28 5.88 18.13 3.75 48.81 14.2 3 Total FE (lb*in.) 291.0 349.2 201.0 392.7 521.7 343.6 359.5 419.0 466.1 387.6 191.2 516.5 Total FE Average (lb*in) Total FE SD (lb*in) 280 74.63 419 91.98 415 53.42 365 163.8 5 273 87.41 269 60.82 341 23.58 387.2 290.3 463 30.26 6.54 7.3 431.2 232.5 7.4 502.6 183.8 7.0 454.5 338.7 7.1 418.4 7.1 482.8 240.4 6.6 438.8 336.0 7.4 469.5 452 32.24 7.14 227.5 309.1 448 19.15 4.28 6.8 456.2 361.1 7.0 425.9 356.0 86 Table 16 (cont’d) Mix 20C 21 23 24A 24B 26A Sample 20C-1A 20C-3A 20C-3B 21-3-B 21-1-B 21-1-D 23A-1A 23A-2A 23A-3A 24-1-B 24-3-B 24A-1A 24A-3A 24B-3A 24B-1A 24B-1B 24B-3B 26A-1A 26A-1B VA (%) IDT IDT Strength Strength Average (psi) (psi) SD (psi) CV (%) Total FE (lb*in.) 7.4 369.6 7.4 401.6 7.2 413.1 391.0 7.4 7.3 7.2 472.0 456.4 433.8 301.6 309.1 232.7 6.7 459.0 7.5 448.6 6.7 477.3 391.4 6.6 6.8 343.4 367.3 565.6 602.9 6.6 408.3 6.9 368.9 462.8 7.1 483.2 441.6 7.0 490.2 403.2 7.5 520.9 407.3 6.9 499.1 582.3 7.7 413.1 412.0 7.4 386.1 Total FE Average (lb*in) Total FE SD (lb*in) 362 86.00 281 42.12 446 63.20 527 68.00 459 84.25 412 0.00 430.2 395 22.55 454 19.19 5.71 4.23 265.6 430.2 462 14.50 372 26.90 498 16.39 400 19.05 3.14 7.23 515.0 477.1 3.29 4.77 - 87 Table 16 (cont’d) Mix 26B 26C 28A 28B 29A Sample 26B-1B 26B-3B 26B-2C 26B-3C 26C-1A 26C-2A 26C-3A 28A-1A 28A-1B 28A-3B 28B-1A 28B-3A 28B-1B 28B-3B 29A-3A 29A-3B 29A-1B IDT Strength Average (psi) VA (%) IDT Strength (psi) 7.5 315.6 7.7 359.2 7.3 309.8 7.7 367.3 443.0 7.2 347.0 417.5 7.2 333.4 6.5 356.8 335.4 7.5 492.4 192.1 7.2 490.7 7.3 465.4 276.1 7.1 429.6 192.8 7.5 416.7 7.4 430.1 7.2 387.1 182.3 7.4 410.7 276.5 7.3 387.5 7.3 397.4 SD (psi) CV (%) Total FE (lb*in.) Total FE Average (lb*in) Total FE SD (lb*in) 430 11.29 349 62.66 225 44.97 185 32.71 280 11.20 435.0 29.4 8 338 11.7 7 346 15.1 1 483 20.1 6 416 11.6 5 399 418.6 8.72 422.4 3.40 3.13 294.5 206.3 222.7 4.85 143.6 2.92 292.3 270.7 88 Table 16 (cont’d) Mix 29B 31A 31B 32A 32B 37 Sample 29B-1A 29B-2A 29B-1B 29B-3B 31A-1A 31A-2A 31A-3A 31B-3A 31B-1A 31B-1B 32A-1A 32A-2A 32A-1B 32A-3B 32B-1A 32B-3A 37-3-B 37-2-1A 37-1-B IDT Strength Average (psi) VA (%) IDT Strength (psi) 6.7 454.5 7.3 402.1 6.9 418.5 7.2 427.9 223.7 6.6 475.1 210.7 7.1 404.3 6.5 447.2 354.4 6.9 474.9 307.5 7.4 478.4 7.2 457.4 294.6 7.0 449.8 316.4 7.7 445.5 6.9 486.7 7.0 456.3 372.1 7.1 458.6 350.0 6.9 447.1 7.4 7.1 7.6 431.8 465.4 466.4 SD (psi) CV (%) Total FE (lb*in.) Total FE Average (lb*in) Total FE SD (lb*in) 202 23.31 281 71.88 283 31.62 327 41.99 406 79.50 515 153.9 2 169.5 21.9 4 426 35.6 7 442 11.2 5 470 18.6 1 460 453 8.15 212.2 5.15 202.2 8.07 2.39 279.3 247.4 345.0 4.05 273.9 1.80 462.4 19.7 2 455 89 4.34 603.9 603.9 337.3 Table 16 (cont’d) Mix 44 45 47 48 49A 49C 51A Sampl e 44A-1C 44A-3C 44A-2C 45-3-A 45-1-A 45-1-B 47-1-A 47-2-A 48-1-A 48-3-A 49A-2A 49A-3A 49A-1B 49A-3B 49C-2A 49C-3A 49C-1B 49C-3B 51A-1A 51A-3A 51A-2A IDT Strength Average (psi) VA (%) IDT Strength (psi) 6.6 387.2 6.7 435.4 7.5 392.1 7.6 7.1 6.8 6.7 7.6 7.3 7.3 325.7 327.6 385.0 436.2 429.9 436.4 406.6 7.5 367.9 6.7 388.7 6.4 401.1 7.1 391.5 687.2 7.0 332.8 1295 6.6 346.9 7.4 350.6 7.4 315.5 956.5 7.5 305.0 692.1 7.2 384.7 7.5 351.3 SD (psi) CV (%) Total FE (lb*in.) Total FE Average (lb*in) Total FE SD (lb*in) 226 44.80 323 39.73 245 41.76 213 47.67 499 140.70 1014 257.63 544 130.05 200.2 26.5 5 405 6.56 200.3 277.8 346 33.7 1 9.74 433 4.45 1.03 422 21.1 0 5.01 319.2 364.6 285.5 215.0 274.1 179.1 246.5 414.3 14.0 1 387 15.9 4 336 40.0 2 347 371.4 3.62 521.4 4.74 789.4 11.5 3 450.1 488.7 90 Table 16 (cont’d) Mix 51B 51C 62 64 65 76 68 Sample 51B-2A 51B-1B 51B-3B 51C-1A 51C-3A 51C-1B 51C-3B 62-1-A 62-3-A 62-2- B 64-3-1 64A-1E 64A-3E 64A-1D 65-1-A 65-2-A 65-3-A 67-1/41A 67-1/43 67-1/42 68-3-B 68-1-B 68-1-D 68-3-D IDT Strength Average (psi) VA (%) IDT Strength (psi) 7.2 402.1 7.1 421.0 6.6 393.0 191.1 7.6 376.9 321.4 7.3 391.2 7.1 364.0 7.0 385.8 6.4 7.0 7.3 7.6 390.4 425.3 422.0 423.3 6.6 421.6 6.6 379.6 7.5 326.9 6.9 7.5 7.0 371.0 351.1 363.9 6.6 415.6 6.7 411.6 7.4 379.0 7.5 7.2 7.1 7.5 402.1 444.8 393.2 398.6 SD (psi) CV (%) Total FE (lb*in.) Total FE Average (lb*in) Total FE SD (lb*in) 215 47.31 294 26.60 508 96.68 246 76.78 324 40.40 522 85.32 405 40.21 270.0 14.2 8 405 11.8 9 379 3.52 185.4 304.5 3.13 258.5 293.1 19.2 7 413 4.67 434.5 617.5 472.0 163.0 208.5 45.3 7 388 11.7 0 339.4 271.8 10.1 0 362 2.79 369.2 291.4 311.4 451.4 20.0 9 402 5.00 498.2 616.9 23.6 8 410 91 5.78 370.4 373.9 454.6 420.2 Table 16 (cont’d) Mix 80 81 85 86 90A 97 102 Sample 80-1-A 80-2-A 80-1-B 80-3-B 81-1-1 85A-3A 85A-1B 85A-3B 86A-1A 86A-3A 86A-2B 86A-3B 90A-1B 97A-1A 97A-2A 97A-3A 102A-3B 102A-1C 102A-3C IDT Strength Average (psi) VA (%) IDT Strength (psi) 6.4 7.1 7.1 7.1 7.4 428.8 400.0 409.1 396.4 357.4 7.5 407.2 6.8 411.0 7.4 390.9 787.9 7.6 432.6 490.0 7.4 423.4 SD (psi) CV (%) 409 14.5 2 3.55 357 0.00 0.00 Total FE (lb*in.) 552.7 628.7 463.4 413.0 192.9 Total FE Average (lb*in) Total FE SD (lb*in) 514 95.58 193 0.00 622 147.4 8 538 116.3 5 182 0.00 258 28.31 343 80.52 506.5 10.6 8 403 16.0 7 417 2.65 570.7 411.8 3.85 6.8 418.4 565.8 6.8 394.9 6.4 455.3 6.8 511.9 7.8 502.9 7.1 508.2 269.3 6.4 470.8 281.0 6.5 505.4 6.8 485.1 685.1 455 0.00 0.00 181.6 225.8 508 4.53 17.4 0 487 0.89 3.57 278.9 314.0 434.0 92 Table 16 (cont’d) Mix 103 105 108 109 111 112 Sample 103A-1B 103A-2B 103A-3E 103A-1E 105A-2B 105A-3B 105A-1C 105A-3C 108-1-B 108A-1B 108A-2B 108A-3B 109-4/2 109-1-A 109-3-A 111A-1B 111A-2B 111A-3B 112-1-A 112-3-A 112-1-B 112-3-B VA (%) IDT Strength (psi) 6.7 364.9 7.1 368.8 IDT Strength Average (psi) SD (psi) CV (%) Total FE (lb*in.) Total FE Average (lb*in) Total FE SD (lb*in) 333 211.6 4 312 58.18 302 64.87 241 46.34 338 9.25 238 19.56 634.1 70.1 6 427 16.4 4 326.0 7.6 500.1 7.6 473.7 171.7 7.5 409.0 387.9 6.5 486.6 7.1 444.7 7.4 456.5 325.5 7.4 476.7 272.4 6.5 475.6 32.1 2 449 200.2 255.4 7.15 280.2 297.1 15.3 3 467 3.29 7.3 470.0 393.1 7.2 444.0 7.6 6.9 7.3 449.0 504.1 486.3 6.5 509.7 7.5 523.2 6.7 502.9 347.9 7.0 7.2 7.1 7.5 545.2 535.4 527.1 525.6 211.4 252.0 234.6 253.3 243.5 28.0 9 480 5.85 206.8 222.4 293.7 330.0 10.3 7 512 533 9.03 93 2.03 1.69 334.7 Table 16 (cont’d) Mix 127 200 201 202 203 204 205 206 Sample VA (%) 127-1-B 7.3 127-3-B 7.4 127-17.3 C 200-1-A 7.0 200-3-A 7.3 200-1-B 7.2 201A-110.8 A 201A-211.6 A 201A-310.6 A 202A-26.6 A 202A-37.2 A 202A-16.6 B 202A-37.0 B 203-1-A 7.3 203-3-A 7.4 203A-17.0 A 203A-37.1 A 204-1-3 7.3 204-1-1 7.3 204A-37.5 A 205-2-1 7.0 205-2-2 7.1 205-2-3 7.5 206-1-A 7.3 206-3-A 7.0 206-1-B 7.5 IDT Strength (psi) 432.7 354.8 IDT Strength Average (psi) 39.7 2 389 380.5 506.6 475.0 468.2 SD (psi) 20.4 6 483 CV (%) 10.2 0 4.23 271.4 271.6 Total FE (lb*in.) 200.8 393.2 252.9 242.5 230.2 276 7.29 2.65 163.0 513.1 172.6 500.2 194.9 512 8.40 1.64 512.2 162.8 520.5 209.3 447.7 464.9 272.9 311.3 13.3 1 451 2.95 434.1 97.67 242 11.39 232 82.95 185 21.12 353.3 337 59.69 383 70.27 - - 178 20.35 412.2 11.7 0 2.09 321 37.4 9 11.6 7 468 21.5 2 4.60 560 566.7 359.0 284.0 320.7 483.4 477.9 443.7 307 323.7 207.9 566.8 546.5 Total FE SD (lb*in) 326.5 284.1 457.5 Total FE Average (lb*in) 94 366.4 322.6 460.1 201.3 167.7 164.6 Table 16 (cont’d) Mix 208 209 A 209 B Sample 208A-1A 208A-2A 208A-3A 209A-3A 209A-1B 209A-3B 209B-1B 209B-1A 209B-3B IDT Strength Average (psi) VA (%) IDT Strength (psi) 6.6 431.9 7.3 439.4 7.0 405.0 189.7 7.1 463.6 154.5 7.2 449.3 7.4 446.4 233.4 6.8 418.7 244.3 7.6 387.4 7.3 449.5 SD (psi) CV (%) Total FE (lb*in.) Total FE Average (lb*in) Total FE SD (lb*in) 174 22.21 200 40.93 196 51.92 158.3 18.0 9 425 453 9.23 31.0 6 419 4.25 2.04 7.42 - 212.7 141.0 202.0 95 Table 16 (cont’d) Mix Total FE CV (%) 2A 26.62 2B 21.94 4 12.88 18A 44.88 18B 31.96 20A 22.62 20B 6.92 20C 23.74 21 14.98 23 14.19 24A 12.90 Pre FE (lb*in.) 291.0 333.8 201.0 281.9 274.3 227.5 282.4 284.0 334.5 262.1 191.2 230.1 290.7 268.6 232.5 183.8 324.9 227.5 240.4 236.7 235.3 263.9 315.3 216.3 242.5 282.7 301.6 309.1 232.7 323.7 321.0 316.0 300.6 263.3 298.7 284.1 Pre FE Average (lb*in) Pre FE SD (lb*in) Pre FE CV (%) 275 67.79 24.63 261 29.47 11.28 300 29.64 9.87 228 35.52 15.59 244 46.69 19.14 264 52.91 20.02 263 37.40 14.23 247 33.44 13.53 281 42.12 14.98 320 3.92 1.23 287 17.22 6.01 96 Post Post FE Post FE Average FE SD (lb*in.) (lb*in) (lb*in) 0.0 15.3 0.0 110.8 247.4 116.1 77.1 135.0 131.6 125.5 0.0 286.5 96.4 21.7 0.0 0.0 13.8 0.0 0.0 99.3 73.9 97.2 40.7 213.9 23.1 108.3 0.0 0.0 0.0 106.5 194.0 75.4 265.0 339.6 178.4 178.6 Post FE CV (%) 5 8.84 173.21 158 77.35 48.92 115 32.47 28.35 137 143.59 104.58 30 45.76 154.93 5 7.96 173.21 78 27.24 35.03 115 95.59 83.04 0 0.00 0.00 125 61.48 49.07 240 77.69 32.32 Table 16 (cont’d) Total FE CV (%) Pre FE (lb*in.) 24B 18.37 320.4 328.3 360.2 332.6 26A 0.00 26B 2.63 26C 17.95 28A 20.00 28B 17.65 29A 4.00 29B 11.54 31A 25.53 31B 11.17 32A 12.85 32B 19.57 Mix 246.7 221.7 210.9 205.1 243.1 258.0 220.3 261.6 192.1 206.3 276.1 192.8 213.6 143.6 182.3 276.5 231.6 270.7 169.5 212.2 195.6 212.9 210.7 267.1 284.3 296.0 247.4 294.6 316.4 275.9 273.9 299.6 249.0 301.2 Pre FE Average (lb*in) Pre FE SD (lb*in) Pre FE CV (%) 335 17.31 5.16 247 0.00 0.00 220 16.73 7.60 247 22.92 9.29 225 44.97 20.0 0 183 29.38 16.0 5 260 24.41 9.40 198 20.33 10.2 9 254 38.48 15.1 5 279 27.64 9.90 291 20.34 6.98 275 36.93 13.4 2 97 Post FE SD (lb*in) Post FE CV (%) 123 89.72 72.81 165 0.00 0.00 210 7.51 3.58 102 49.36 48.16 0 0.00 0.00 2 4.56 200.0 0 20 35.03 173.2 1 4 5.30 122.1 8 27 37.48 136.5 0 4 6.65 173.2 1 35 40.90 115.5 3 131 42.57 32.47 Post Post FE FE Average (lb*in.) (lb*in) 121.2 74.9 47.0 249.7 165.3 213.3 207.7 217.3 200.0 159.5 74.2 73.8 0.0 0.0 0.0 0.0 9.1 0.0 0.0 0.0 60.7 0.0 0.0 0.0 6.6 10.8 0.0 12.2 70.2 11.5 0.0 0.0 0.0 69.1 0.0 72.5 101.0 161.2 Table 16 (cont’d) Mix Total FE CV (%) 37 29.89 44 19.82 45 12.29 47 17.07 48 22.40 49A 28.22 49C 25.42 51A 23.92 51B 21.96 51C 9.04 62 19.03 64 31.25 Pre FE (lb*in.) 221.5 221.5 318.1 200.2 200.3 277.8 250.8 251.0 254.4 215.0 274.1 179.1 246.5 249.4 277.1 251.6 261.4 220.4 206.8 173.2 193.9 234.1 249.6 270.0 185.4 191.1 262.2 249.5 215.4 215.2 302.8 230.9 259.8 163.0 208.5 258.1 180.3 Pre FE SD (lb*in) Pre FE CV (%) 254 55.79 21.9 9 226 44.80 19.8 2 252 2.04 0.81 245 41.76 213 47.67 260 12.63 4.86 200 24.30 12.1 4 226 28.75 12.7 3 215 47.31 21.9 6 236 23.97 10.1 7 265 36.18 13.6 8 202 41.52 20.5 1 Pre FE Average (lb*in) 98 17.0 7 22.4 0 Post FE SD (lb*in) Post FE CV (%) 261 209.7 0 80.26 0 0.00 0.00 71 41.35 58.18 0 0.00 0.00 0 0.00 0.00 239 144.1 1 60.37 813 247.4 0 30.41 318 156.7 2 49.33 0 0.00 0.00 59 14.46 24.58 243 130.3 1 53.52 43 50.06 115.8 6 Post Post FE FE Average (lb*in.) (lb*in) 382.4 382.4 19.1 0.0 0.0 0.0 68.5 113.7 31.1 0.0 0.0 0.0 0.0 164.9 94.2 269.9 425.8 1074.6 582.6 783.2 498.2 215.9 239.0 0.0 0.0 0.0 59.2 55.0 43.1 77.9 131.7 386.6 212.1 0.0 0.0 81.4 91.5 Table 16 (cont’d) Mix Total Pre FE CV FE (%) (lb*in.) 65 12.47 76 16.34 68 9.93 80 18.58 81 0.00 85 23.72 86 21.62 90A 0.00 97 10.97 102 23.48 103 63.56 105 18.63 264.7 280.5 278.0 245.2 291.2 223.0 287.4 313.1 311.3 257.7 299.5 248.3 322.3 304.2 192.9 273.1 270.8 219.0 293.7 316.8 298.3 239.0 181.6 225.8 278.9 269.3 281.0 280.7 329.4 233.4 267.0 200.2 171.7 326.3 255.4 280.2 325.5 Pre FE Average (lb*in) Pre FE SD (lb*in) Pre FE CV (%) 274 8.47 3.09 253 34.81 13.7 5 292 25.93 8.87 294 31.73 10.8 1 193 0.00 0.00 254 30.63 12.0 5 287 33.48 11.6 7 182 0.00 0.00 258 28.31 10.9 7 297 28.01 9.43 218 41.22 18.9 0 297 35.05 11.8 1 99 Post FE SD (lb*in) Post FE CV (%) 50 48.84 98.45 269 108.1 5 40.20 112 48.28 42.97 221 123.0 1 55.70 0 0.00 0.00 367 177.7 0 48.37 251 147.9 0 58.87 0 0.00 0.00 0 0.00 0.00 46 53.45 116.3 2 115 192.5 3 167.5 4 15 30.78 200.0 0 Post Post FE FE Average (lb*in.) (lb*in) 104.5 10.9 33.5 206.2 207.0 393.9 82.9 60.8 143.3 162.5 253.2 380.3 141.1 108.8 0.0 233.4 299.9 569.0 196.3 95.1 267.5 446.0 0.0 0.0 0.0 0.0 0.0 33.2 104.6 400.7 59.0 0.0 0.0 61.6 0.0 0.0 0.0 Table 16 (cont’d) Mix Total FE CV (%) 108 21.51 109 19.23 111 2.74 112 8.22 127 31.83 200 4.71 201 35.82 202 11.42 203 17.69 204 18.35 206 11.44 Pre FE (lb*in.) 272.4 297.1 378.4 243.5 206.8 222.4 293.7 330.0 334.7 299.2 211.4 252.0 234.6 253.3 200.8 258.8 270.4 252.9 242.5 230.2 201.3 163.0 175.3 172.6 194.9 162.8 209.3 272.9 209.6 338.8 332.8 366.4 322.6 441.9 201.3 167.7 164.6 Pre FE Average (lb*in) Pre FE SD (lb*in) Pre FE CV (%) 298 57.98 19.4 6 241 46.34 19.2 3 321 19.30 6.01 238 19.56 8.22 243 37.26 15.3 1 242 11.39 4.71 180 19.57 10.8 8 185 21.12 11.4 2 289 60.45 20.9 5 377 60.36 16.0 1 178 20.35 11.4 4 100 Post FE SD (lb*in) Post FE CV (%) 4 7.38 200.0 0 0 0.00 0.00 16 28.10 173.2 1 0 0.00 0.00 64 67.47 106.2 3 0 0.00 0.00 52 63.40 122.6 8 0 0.00 0.00 49 49.29 100.8 3 6 10.53 173.2 1 0 0.00 0.00 Post Post FE FE Average (lb*in.) (lb*in) 0.0 0.0 14.8 0.0 0.0 0.0 0.0 0.0 0.0 48.7 0.0 0.0 0.0 0.0 0.0 134.3 56.2 0.0 0.0 0.0 122.4 0.0 32.6 0.0 0.0 0.0 0.0 0.0 101.7 14.5 79.4 0.0 0.0 18.2 0.0 0.0 0.0 Table 16 (cont’d) Mix Total FE CV (%) 208 12.76 209 A 20.44 209 B 26.52 Pre FE (lb*in.) 158.3 189.7 154.5 212.7 233.4 232.8 141.0 202.0 Pre FE SD (lb*in) Pre FE CV (%) 174 22.21 12.7 6 200 40.93 20.4 4 192 46.76 24.3 6 Pre FE Average (lb*in) 101 Post FE (lb*in.) 0.0 0.0 0.0 0.0 0.0 11.4 0.0 0.0 Post FE Average (lb*in) Post FE SD (lb*in) Post FE CV (%) 0 0.00 0.00 0 0.00 0.00 4 6.58 173.2 1 REFERENCES 102 REFERENCES [1] AASHTO PP 60-09 Preparation of Cylindrical Performance Test Specimens Using the Superpave Gyratory Compactor (SGC), in AASHTO PP 60-09. 2011, American Association of State Highway and Transportation Officials, Washington, D.C. 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