THE EFFECT OF FATiGUE STRESS ON SHEAR IN WOOD Thain fa: the 00am 96 Ph. D. MECHiGAN STATE UNWERSITY £93m Dennis Suflivan 1958 tweets This is to certify that the thesis entitled THE EFFECT a“ FATIGUES'I'RBSS WSHEAR IN WOOD presented by John Demis Sullivan has been accepted towards fulfillment of the requirements for Ph. D. degree in Forest Products V1 [Major professor O—l69 LIBRARY Michigan State University THE EFFECT OF FATIGUE STRESS ON SHEAR IN WOOD BY John Dennis Sullivan AN ABSTRACT Submitted to the School of Graduate Studies of Michigan State University of.Agriculture and Applied Science in partial fulfillment of the requirements for the degree of DOCTOR OF PHILOSOPHY Department of Forest Products 1958 ABSTRACT The research reported here was conducted primarily to study the effect of fatigue loads on wood in shear parallel to the grain on a tangential plane. To the best of the author's knowledge, this research is the first of its kind. Samples of white fir, western hemlock, and Douglas-fir were tested under static loads and under fatigue loads in shear parallel to the grain. Moisture content was held constant and the specific gravity of the wood directly adjacent to the plane of failure was measured. Data were recorded and analysis was accomplished with the use of acceptable statistical systems. The results of the research are summarized in the following list: 1. Wood can be made to fail by fatigue loading in shear parallel to the grain on a tangen- tial plane. 2. There is a linear relationship between shear stress and Specific gravity at the line of failure for samples tested in static shear parallel to the grain on a tangential plane. There is a significant regression of stress level and specific gravity at the line of failure on the number of cycles to failure in shear parallel to the grain on a tangen- tial plane. A. linear relationship exists between shear stress enui specific gravity at the line of failure .hl wood tested by fatigue loading in shear parallel to the grain on a tangen- tial plane. The early springwood offers the least re- sistance to loading in shear parallel to the grain on a tangential planeo The stress level at failure for fatigue shear samples is less than for samples of the same species, with comparable specific gravity values, tested under static loads. THE EFFECT OF FATIGUE STRESS ON SHEAR IN WOOD By John Dennis Sullivan A THESIS Submitted to the School of Graduate Studies of Michigan State University of Agriculture and Applied Science in partial fulfillment of the requirements for the degree of DOCTOR OF PHILOSOPHY Department of Forest Products 1958 ii ACKNOWLEDGEMENTS The writer desires to express his appreciation to Dr. A. J. Panshin for his guidance and criticism in the preparation of this report. The guidance offered by Dr. R. Swenson, Dr. W. Baten, Dr. 0. Suchsland, Dr. P. Koch, and Dr. J. Creighton is also deeply appreciated. The author wishes to acknowledgment his indebtedness to Dr. C. 0. Harris for the use of testing equipment and to Mr. B. Radcliffe for the photographic work. TABLE 9}: CONTENTS ACKNOWLEDGEMENTS . . . . . . . LIST OF TABLES . . . . or. . . LIST OF ILLUSTRATIONS . . . . INTRODUCTION . . . . . . . . . Historical Notes . . . . Statement of the Problem EXPERIMENTAL PROCEDURE . . . . Selection and Preparation Static Testing . . . . . Fatigue Testing . . . . Determination of Moisture Determination of Specific ANALYSIS AND RESULTS . . . . . Specific Gravity Moisture Content : : . : Static Failure . . . . . Fatigue Failure . . . . . DISCUSSION OF RESULTS . . . . Specific Gravity . . . . Moisture Content . . . . Static Failure . . . . . Fatigue Failure . . . . . CONCLUSIONS . . . . . . . . . Theories of Fatigue Failure Secondary Stresses . HYStereSiS e o o e 0 Molecular Slip . . . Application of Failure Theor e of Samples Content : : Gravity . . O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O i s . . . iii Page ii iv Table of Contents.- Continued. Page SUMMARY . . . . . O O O O O O O O O O O O O O 69 APPENDICES . . . . . O O O O O O O C O O O O O 71 Appendix 1. List of Apparatus . . . . . 71 Appendis 11. Data . . . . . . . . . . . 73 LITERATURE CITED . . . O O O O O O O O O O O O 79 gs: 9_1=_ TABLES Table Page 1. Summary of Specific Gravity Analysis . . 27 2. Summary of Moisture Content Analysis . . 28 3. Summary of Regression Analysis for Static Samples . . . . . . . . . . . . . 29 4. Summary of Multiple Regression Analysis for Fatigue Samples . . . . . . . . . . . 40 APPENDIX II a. Static Data Recorded for all White Fir smpleSQQooeoooeeooooooe73 b. Static Data Recorded for the Western Hemlock Samples . . . . . . . . . . . . . 74 c. Static Data Recorded for the Samples of Douglas-fir . . . . . . . . . . . . . 75 d. Fatigue Data for White Fir . . . . . . . 76 e. Fatigue Data for Western Hemlock . . . . 77 f. Fatigue Data for Douglas-fir . . . . . . 78 LIST g_1_=_ ILLUSTRATIONS Figure 1. Test Sample used for Static and Fatigue Testing (photograph) . . . . 2. Sonntag Fatigue Machine and Load Multiplier (photograph) . . . . . . . 3. Calibration Curves for the Fatigue Machine . . . . . . . . . . . . . . . 4. Fatigue Loading Cycle (photograph) . 5. Stress Relaxation in Fatigue Samples 6. Calibration Curve for Velumeter . . . 7. Mercury Displacement Volumeter (photograph) . . . . . . . . . . . . 8. Regression Curve of Shear Stress on Specific Gravity for White Fir . . . 9. Regression Curve of Shear Stress on Specific Gravity for Western Hemlock 10. Regression Curve of Shear Stress on Specific Gravity for Douglas-fir . . 11. Regression Curves of Shear Stress on Specific Gravity for all Three Species Tested . . . . . . . . . . . 12. Migration of Static Failure Line (photograph) . . . . . . . . . . . . 13. Straight Line Shear Failure (photograph) . . . . . . . . . . . . 14. Failure Away from Plane of Maximum Shear Stress (photograph) . . . . . . vi Page 15 16 18 19 23 25 31 32 33 34 36 37 38 List of Illustrations.-Continued. Figure Page 15. S-N Curve for White Fir . . . . . . . . . 42 16. S-N Curve for Western Hemlock . . . . . . 43 17. S-N Curve for Douglas-fir . . . . . . . . 44 18. S-N Curves for all Species Tested . . . . 45 THE EFFECT OF FATIGUE STRESS ON SHEAR IN WOOD INTRODUCTION HISTORICAL NOTES The fatigue strength or the endurance limit of a material has been defined as the maximum stress that can be applied repeatedly for a specified number of stress cycles without producing rupture of the material (2h). Actual testing to induce a fatigue type failure was conducted in Germany in 1829 on mine-hoist chains (15). The first-recorded, fatigue research was followed initially by workers in France, Germany, and England to the end of the nineteenth century when the research in fatigue spread all over the world. From the early interest in metals, fatigue analysis was extended to plastics, glass, rubber, flax, and wood. The normal method of fatigue testing involves the application of a cyclic load on the material in question. Depending upon the type of analysis being conducted, the stress may vary from zero to maximum in one direction or it can involve complete reversal of stresses. The end result of fatigue research is usually expressed graphically to show the relationship 1 of stress level to number cn‘ cycles to failure. Throughout the remainder of this paper this curve will be called the SuN curve. Fatigue research in metals revealed a scattering of data along the S-N curveo This variation induced the use of statistical analysis to establish values of fatigue strength at certain levels of probability (31)(ll). The stress levels used in such testing were based on a percent of the static load at failure for the same material. This design system produced admirable results for isotropic materials. For anisotropic materials, however, the same design has led to extreme variation of data about the S-N curve. The reason for the vari- ation lies in the numerous factors that influence all the strength properties of wood regardless of the loading method. Research into the fatigue properties of wood has been somewhat limited to compression and bending for plywood and for solid wood specimens (20)(19)(2l) (8)(18)(22)o An intensive search of the literature revealed only one investigator who worked directly on fatigue failure in shear parallel to the grain (23). This research was conducted on glued-shear specimens. The failure occurred primarily in the wood adjacent to the glue line; however; the number of samples so tested was considered inadequate by that investigator. Previous studies of fatigue in wood have had widely varying results. The S-N curves were approxi- mately the same shape in these studies, inn; they varied considerably iJI their height (Hi the stress scale for identical species. All the workers appeared to have their results limited by an insufficient number of samples and by a large amount of variation from the S~N curve. Another factor common to these investigations was the complete absence of statistical significance h] the results. This factor led the author of this paper to the assumption that perhaps these previous researchers had not taken some fundamental sources of error under consideration. These sources of error could be occasioned by such variables as specific gravity, moisture content, temperature, residual stresses, and damping capacity. STATEMENT OF THE PROBLEM The primary object of this research was to study the effect of fatigue loading on wood in shear parallel to the grain. This would obviously be possible only if a testing method could be developed that would induce failure in wood subjected to fatigue loading. The secondary object of the problem was to obtain an S~N curve with a minimum amount of variance. It was the authoris opinion that a large source of error could be eliminated if specific gravity could either be accurately measured or held as a constant. Since it is virtually impossible to hold Specific gravity of wood constant from one sample to another, the only remaining alternative was to measure specific gravity as accurately as possible. Since failure was to be related to specific gravity, it seemed natural to assume that the specific gravity at the exact point of failure would be a better measure than would be the average specific gravity of an entire sample. This assumption immediately posed two questions: In which strength property of wood can the line of failure be exactly located, and how is the Specific gravity at the point of failure to be measured accu- rately? Shear strength was selected because it is simple to locate the failure line in shear and because no previous fatigue research had been conducted on solid wood specimens in shear fatigue. The problem was then conducted with the solution of the following objectives in mind: 1. To induce failure by fatigue in shear parallel to the grain for solid samples of wood. To accurately measure specific gravity at the line of failure for Specimens tested. To Show the effect of specific gravity on the fatigue strength of wood in shear parallel to the grain on a tangential plane. To show the effect of specific gravity on the static strength of wood hi shear parallel to the grain on a tangential plane. To obtain S-N curves with a minimum amount of experimental variation for several wood species. To compare the shear strength of wood under static loads to the shear strength of wood subjected to fatigue loads. To obtain statistical significance wherever possible for the objectives listed above. EXPERIMENTAL PROCEDURE The procedures used in this experiment were devised to minimize or eliminate experimental error. Standard testing methods were applied wherever such methods were applicable to the apparatus available. A detailed list of apparatus is shown in Appendix I of this report. Preliminary testing showed that some modification of certain pieces of apparatus was necessary or that different equipment would have to be used. The appropriate modifications and the de- sign of new equipment are described in detail in later portions of this experimental procedure. The experimental procedure, as described in this paper and as used in the research, includes preparation of samples, static testing, fatigue testing, deter- mination of moisture content, and determination of specific gravity. SELECTION AND PREPARATION OF SAMPLES The wood species selected for experimentation were white fir (52123 grandis [Dougl.] Lindl.), western hemlock (18333 heterophylla [Raf. ] Sarg. ), and Douglas-fir (Pseudotsugg menziesii [Mirb.] Franco). Throughout the remainder of this report the common names, white fir, western hemlock, and Douglas-fir, will be applied to the samples of the respective wood species. The identity of all stock from which the samples were obtained was confirmed by microscopic inspection. Coniferous tree species were used because of their relatively low resistance to failure in shear parallel to the grain direction. White fir, western hemlock, and Douglas-fir were selected because they were readily available in the dimensions desired and because these species are widely used in the various forest products industries. Douglas-fir wood, which is characterized in! the presence of small, sparsely distributed resin canals, was tested as a portion of this project because it was assumed that the small size and number of resin canals would not significantly affect the results. The stock was carefully scrutinized to detect any abnormalities that could influence the strength of the samples. Any evidence of brashness, compression wood, grain deviation, seasoning checks, or decay resulted in the elimination of such material for use as sample stock. The stock eventually used for samples was defect-free, straight-grained wood. The white fir was used to determine the plane of minimum resistance to shear parallel to the grain. Stock with wide growth increments CAppendix I, No. l) was used in order to place the plane of maximum shear in different Positions in the growth increments of different samples. Western hemlock and Douglas-fir stock were selected from material cut from large, slow grown trees with very narrow growth increments (Appendix 1, No. 2 and No. 3). Such material insured the close proximity of the plane of least resistance to the plane of maximum shear stress parallel to the grain. It was assumed that all the samples of western hemlock and Douglas-fir would then fall at the weakest point in the wood. Preliminary testing showed thatithe shape of the shear specimen could have a pronounced effect on the magnitude of stress at failure. The ideal shear specimen is characterized by shear only, without bending moments on the plane of maximum shear. Unfortunately, bending moments cannot be eliminated; they can only be minimized (7)(32). The design of the shear block specimen used for all samples tested in this research is shown on the following page in Figure 1. The most obvious advantage of the H-shapedsample is that the stresses that induce failure by cleavage are minimal at the plane of greatest shearing stress. Test samples for static testing as well as for fatigue testing were machined to form and dimension on a band-saw (Appendix I, No. LI). All sammes were Figure 1. Photograph of test sample used for static and fatigue testing. The sample in the picture is about two- thirds of the actual size. 10 cut to the same shape and the same dimensions within the limits of accuracy of the machine. The interior faces of the testing-head groove in the samples were machined to be as nearly parallel as possible. In addition, the testing-head surface (A in Figure l), the lower surface cu‘ the shear section (B in Figure l), and the plane of the supports (C in Figure l) were made mutually parallel within the machining accuracy of the band-saw. All samples were fashioned to make the plane of maximum shear tangent to the growth increments in order to avoid the possibility of failure across more than one growth increment. .Matching fatigue samples were cut from material ad- jacent in a tangential direction to the static samples. The testing-head groove for each matched pair of samples was cut into the same growth increment in an attempt to have identical material along the planes of maximum shear. The samples were marked to insure their identity. After machining, all test samples were conditioned to a moisture content of about twelve percent. The purpose of the conditioning period was to minimize error induced by changes in moisture content. The shear area of each sample was measured and recorded. After conditioning, the samples were placed in polyethylene bags to reduce the rate of change of 11 moisture in the wood. The samples were stored until the mechanical tests were conducted. STATIC TESTING All static testing was performed on a Baldwin- Emery, SR-h Testing Machine (Appendix I, No. S). The samples were tested at amachine speed of 0.02h inches per minute (i). The testing head was the same that was used for fatigue testing. A small, flexible rubber strip was inserted between the testing head and the specimen to obtain uniform distribution of the load. Samples were supported on a universal bearing to minimize the effect of horizontal components of the load. As static loading progressed on a sample, it was closely inspected to determine the position of initial failure. Samples were excluded from further considera- tion when the initial failure was other than in shear parallel to the grain at the plane of maximum shear. A.common type of failure was in cleavage occurring at the vertical center of the load-bearing section. All samples that failed initially due to cleavage exhibited secondary failure in shear parallel to the grain. These samples were not included in the analysis because the load-bearing section was not horizontally continuous after cleavage. In addition, the magnitude of the bending moment across the plane of maximum l2 shear was different iuxmi one such sample to another. Approximately thirty percent of the original number of static samples were rejected because of failure in cleavage. The samples in which the initial failure occurred in shear parallel to the grain at the plane of maximum shear were considered for further analysis. The line of failure was inSpected for the presense of any ab- normalities that may have influenced the resistance of the sample to the load. Samples were eliminated if the failure plane was characterized by grain deviation, pin knots, decay, or accumulations of resin. The latter consideration applied only to the Douglas-fir samples. This inspection eliminated about five percent of the original samples in Douglas-fir and western hemlock and about fifteen percent in white fir. The data recorded for each acceptable samples were the stress 'at failure and the position of the line of failure with respect to the summerwood and springwood (Appendix 11, Tables a, b, and c). FATIGUE TESTING All fatigue testing was performed on a Sonntag fatigue testing machine. (Appendix 1, No. 6). The machine consisted of a large stationary platen and a smaller reciprocating platen. The oscillating force was produced through the reciprocating platen by means 13 of an unbalanced rotating mass operating at a constant speed of 1800 cycles per minute. The machine was capable of operating either with or without a static preload. To satisfy the requirements of this research the machine was to be operated on the tension side with the vibratory load fluctuating from zero to the maximum load desired. It was therefore necessary to place a static preload one-half the magnitude of the total load on the sample. Preliminary testing showed that the maximum load capacity of the machine was not sufficiently high to satisfy the testing requirements of this research. Therefore a load multiplier was designed that was capable of delivering the loads desired. Fortunately, a torsion load multiplier for the Sonntag machine was available for study as a prototype (2). The torsion fixture was a fixed-pivot lever arm designed to produce an alternating torque from an alternating force. It was obvious that the use of a freely-pivoting lever arm would produce a large alternating force from a relatively small alternating force. This was the principle that was used in the design of the load multiplier for this problem. One pivot was rigidly attached to the reciprocating platen and the second pivot was securely fastened to the stationary Platen. The exact position of the test 11+ specimen on the stationary platen between the pivots determined the load multiplication factor of the fixture. A photograph of the Sonntag machine with the attached fixture is shown in Figure 2 on the following page. Additional preliminary testing revealed that the load multiplier required calibration of load for complete satisfaction. Strain gages (Appendix 1, No. 7) were cemented to opposite sides of the rear pivot post. The purpose for the opposite placement of gages' was to compensate for bending of the post. Predeter- mined tensile, static loads of incresing magnitude were applied and the strain was measured with a strain amplifier (Appendix 1, No. 8). The calibration curve of the strain system is shown in Figure 3, page 16. The strain was then measured on the fatigue machine for the same loads and was compared to the static load calibration. The curves in Figure 3 show that a portion of the load applied through the machine was lost in the load-multiplier. This was probably due to frictional losses at the pivots and at the testing-head guides. The load on a sample to be tested and the load on the reciprocating platen could then be easily calculated by use of moments. The reciprocating Platen load was divided equally into two components, a static preload and a dynamic oscillating load. 15 Figure 2. Photograph of Sonntag Fatigue Machine used hi this research. The loadm multiplier‘ is nwunted on the platens of the machine. The oscilloscope was used to calibrate the loading system. 16 .mcaumofi osmflamm he use manned" chosen an eocueuno wo>uno ecupmunafleo cashew .n unease “coca eon mococauocofiev zHo a0 mmmzsz 000.0m . 000.01 .m oesmflm cog com com 0d: 00m 000 com ('lSd) ssauls HvaHs 20 and to increase the stress level after a certain number of cycles if failure did not occur. The stress level was elevated at 100,000 cycles. The data recorded for each sample were the maximum shear stress at failure, number of cycles to failure, and the position of the line of failure with respect to springwood and summerwood (Appendix 11, Tables d, e, and f). Any samples that exhibited evidence of grain deviation, pin knots, decay, accumulations of resin, or failure in clevage were eliminated from further consideration. This final inspection eliminated about fifteen percent of the original number of white fir samples and approximately five percent in Douglas- fir and western hemlock. DETERMINATION OF NDISTURE CONTENT All samples were weighed on a triple-beam balance (Appendix 1, No. 9) immediately after failure. The balance pan and pivots were cleaned and the instrument adjusted for zero before any measurements were made. The zero balance position was checked periodically during the course of the data collection. The weight immediately after failure was recorded for each sample. The samples were then placed in a drying-oven (Appendix 1, No. 10) and allowed to dry until no further loss of weight occurred. The drying temperature varied from 100 to 102 degrees Centigrade. 21 The constant weight that was eventually attained was recorded for each sample. The moisture content at the time of failure was computed on the basis of weight loss expressed as a percentage of the oven—dry weight for each samfie. This moisture content was then re- corded for each sample (Appendix II). DETERMINATION OF SPECIFIC GRAVITY The design of this research problem called for a measurement of specific gravity of the wood directly adjacent to the line of failure. Therefore, it was necessary that very thin chips or shavings be obtained from the failure line. Ideally the thickness of the sections should have been the diameter of a woody plant cell. This would have been very difficult to determine because the cell is characterized by decreaSing diameter from large springwood cells to very small summerwood cells. The average tangential diameter of a tracheid of white fir and Douglas-fir is from 35-145 microns while western hemlock tracheids, with an average tangential diameter of 30-140 microns, are somewhat smaller (1;). Micro-sectioning was not possible since the ‘lines of failure were usually anything but straight and flat. There remained the one method that was actually used; sections sliced with an exceedingly sharp knife. The sections varied from sixty to one-hundred microns in thickness and 22 usually contained two or three tangential rows of cells. The thickness measurements were made with a micrometer. Preliminary tests showed that ttm: usual methods for obtaining specific gravity were not suitable for very thin sections. The problenx was 'to determine the volume of the sections quickly and accurately to avoid error due to volume change resulting from intake or exodus of water. It was eventually decided to use the method of liquid mercury displacement. .A mercury' displacement volumeter (Appendix 1, No. 11) was de- signed with the aid of a prototype (Appendix 1, No. 12) loaned to the author. The volumeter was calibrated by measuring the displacement of precision ground ball bearings of varying diameters. The calibration curve for the volumeter is shown in Figure 6 on the following page. Before measurements were made for the specific gravity determination, the wood samples were again conditioned in a constant temperature-humidity room to a moisture content of approximately twelve percent. Thin sections were cut from each side of the line of failure and weighed on a grammatic balance (Appendix 1, No. 13). Material from one side of the failure was measured for weight and volume separately from material from the opposite side of the same line of failure. 23 .cmum85Ho> bamEmomHQmHv zusocms pom w>uso compounfifimo m.m AmcomeAmeu ownsov mzaqo> m." 0.“ m.o .0 shaman .\\ \\ \\ L\ :\ o~.o 00.0 05.0 (saqoux) 1N3W33V1JSIG HELSWOHDIN 21+ The sections were placed in the volumeter, the mercury was moved up to a reading-line on the sight tube, and the micrometer reading was recorded to the nearest ten-thousandths of an inch (Figure 7, page 25). The chips were extracted from the micrometer and the mercury was displaced up to the reading line, and the zero micrometer displacement was recorded. The difference between the two micrometer readings was converted directly into cubic centimeters. The specific gravity was then computed for each side of each line of failure in every sample. The average specific gravity at the line of failure was computed arithmetically and recorded (Appendix II). The specific gravity as referred to in this paper is based on weight and volume of the wood at about twelve percent moisture content. All samples were measured under the same conditions and the resulting specific gravity data were intended to show only the possible effect of this variable within one species. The average specific gravity figures in this paper should not be compared to Species averages from any source unless such measurements were made in exactly the same manner as in this research. 25 Figure 7. Mercury dISplacement volumeter. _ A indicates the reading-line on the sight tube, B is the micrometer and C is the mercury reservoir. 26 ANALYSI 8 AND RESULTS All portions of the analysis for this study were completed with the use of acceptable statis- tical systems. Computations were worked out and individually checked on an automatic calculator (Appendix I, No. ILL). Each species was analysed separately for variation in specific gravity at line of failure and moisture content at time of failure. In addition the relationship between specific gravity and shear stress at failure was explored for the statically loaded specimen. The data obtained from fatigue testing were used to determine the influence of the specific gravity and the shear stress at failure on the number of cycles to failure. SPECIFIC GRAVITY Analysis was conducted on each species to determine the variability in specific gravity that was observed between the statically loaded samples and the fatigue samples, The null hypothesis was assumed and simple group Comparison with the t test for significance was aPplied. The statistical results are summarized in Table 1. 27 Table 1. Summary cfi‘ the statistical analysis to test the mean difference of specific gravity between static and fatigue samples in each species. Western Species White Fir Hemlock Douglas-fir Testing Method Static Fatigue Static Fatigue Static Fatigue Mean 0.306 0.316 0.357 0.393 0.h28 0.h37 Variance 0.0891 0.0676 0.0h27 0.03h0 0.0372 0.0366 Pooled Variance 0.00h12h 0.002017 0.0019h3 Standard Error 0.0203 0.01ul9 0.0139h t 0.680 2.297% 1.000 *statistical significance at the 95 percent level. The t_values shown in Table I were interpreted to yield the results listed below: 1. The null hypothesis was accepted for white fir and Douglas-fir. It may be assumed that all the spe- cific gravity data were obtained from a common population and that the average specific gravity at the line of failure for the fatigue samples was not different from that of the static samples. 2. The null hypothesis was rejected for western hemlock. It may be assumed that the specific gravity at the line of failure for the fatigue samples was significantly greater than for that of the Static samples. MOISTURE CONTENT 28 An analysis was made in each species to study the variation in moisture content between the statically loaded samples and the fatigue samples. The null hypothesis was assumed and simple group comparison with the t test for significance was applied. The results are summarized below in.Table 2. Table 2. Summary of the statistical analysis to test the mean difference of moisture content between static and fatigue samples in each species. Western Species White Fir Hemlock Douglas-fir Testing .Method. {Static Fatigue Static Fatigue Static Fatigue Mean 10.88 10.23 13.h3 11.77 12.3h 11.13 Variance 1.821 7.300 2.989 22.207 0.827 1.071 Pooled Variance 0.2h00 0.6631 0.0h996 Standard - Error 0.15119 0.2575 0.0707 .E 11.18% 6.1.117“- 17.086” *fistatistical significance at the 99 percent level. The summary shown in Table 2 indicates that in all three species the moisture content at the time of 29 static failure was significantly greater than the moisture content at the time of fatigue failure. STATIC FAILURE vThe method of linear regression was employed to determine the effect of specific gravity on the shear stress at failure parallel to the grain in each of the species tested. This method was applicable since the variance was homogeneous, specific gravity was measured without error, and the shear stress was random. The results of the regression analysis are shown in Table 3. Table 3. Summary of regression analysis to demonstrate the effect of specific gravity on the magnitude of shear stress at failure. Species Regression Coefficient t-value White fir 2606.0 9.112** Western hemlock 3282.3 5.659** Douglas-fir 3581.5 6.707** Regression Equation White fir Y -336.6 + (2606.0) x 'Western hemlock Y = - 26.0 + (3282.3) x Douglas-fir Y = -460.0 + (3581.5) x 30 Table 3.-Continued. ** statistical significance at the 99 percent level. Y' estimated shear stress for any value of specific gravity. X any value of specific gravity. The _1_:_ values shown in Table 3 denote a statis- tically significant9 linear, positive regression of shear stress on the average specific gravity at the line of failure. Figures 8, 9, and 10 show the regres- sion and the 95 percent fiducial limits of estimated shear stresses for white fir, western hemlock, and Douglas-fir respectively. The regression line is based on the premise that the sum of squares of dev- iations from linear regression are minimum (27). The confidence interval of the stresses was determined by direct calculation over a range of specific gravity figures (29). In figure 11 the regression lines of all three species are shown on one graph. The greatest shear stress at the average specific gravity was developed in western hemlock, followed by Douglas-fir and white fir in that order. This successive relation- ship corresponds closely to published values of shear Parallel to the grain. The shear line of failure for western hemlock and Douglas-fir occurred at the point of maximum shear stress in all samples included in the analysis. In mm .hufi>Mum camaooam ummam>w 0:» mo bcfioq on» an mcfi~ codwmocmoa an» op anemofio can can mummoabm coumsfipmm mo muHEHH quoscfim acoopoa mo cab mgwoauca wmcfifi coxoub one .nfiu mafia: com >a~>mnm oaufiommm co mmwnpm human mo coammoawom .0 oasmfiu A.sna0 mammem mb«>mc0 ofimuooam ommco>m may go 0:000 one on 0:02 cofimmucmmu can on “mmmofio one new mommoaum cmbmsaamm mo mufisfi~ demoscfim bemocoa mm on“ obmofiecu mung“ cmxoab one .xoofism: ccmpmm3 pom zpfi>ma0 ofiuflomam co mmoupm ammcm mo couwmocmmm .0 opsufim A.sna0 mwmmem mammm oops cows com oo: o . \ . \ o\. \\ O \ .2 \ \ 0N.0 00.0 0:.0 om.o 00.0 AlIAVHD DIJIDHdS .zpm>mc0 oflmfiomam wmmco>m mo ucaoa meg um ocfifi coflmmocmou on» 60 “memofio one new mommmaum cmpmsflumo mo mpfisfifi dmfiosvfiu unmouom mo may upmowucw wmcafi :mxoaa use 3 3 .02 aasasa .c00immumsoa com hpfi>mu0 ofimwommm co mmouam cmunm no cofiwmonmmm A.sna0 mammew mammm coon comp com 00: o om.o on.o 0:.0 om.o i ALIAVHO OIJIDHdS 3h .cmumob mmqomam moan» ecu com >00>mcm ofihfiooam co uaafifimu um «macaw human 0o coumwucmum A.0mav mmmmhw mdmmw .Hfi musomm oops com" com co: .\ \ \\ \ \\ .V\ \ \ R\ \\. \\ \\ x \ \\ \\ \x\ xx \ \\ \\ \\ \_ .x\ =\\ x \ \ \ x \ \ \\\ caunmmdmaom 33350: 5.333 llll a: as}: .l-.l 0N.0 00.0 3.0 0m.0 00.0 ALIAVHD OIJIDHdS 35 addition, the line of failure was parallel to the grain direction in all samples. The line of failure character- istically occurred either in.the springwood or on the line between the summerwood cfi'an increment and the springwood of an adjacent increment. No failure took place entirely in the summerwood of the samples. The white fir samples were more variable than the other species with respect to the location of the line of failure. For the majority of the samples, shear failure began at the point of maximum shear and then migrated toward the early springwood. A photograph showing this phenomenon can be seen in Figure 12. page 36. The migration of the failure line always occurred at an angle to the grain and never progressed into a summerwood portion of a sample. The resulting oblique failure line was found only in samples that had summerwood at the point of maximum shear directly under the edge of the testinguhead. If the early springwood was at the point of maximum shear stress, the failure line was characteristically straight and parallel to the grain direction. This more normal type of failure is shown in Figure 13, page 37. Several samples in all three species exhibited another type of failure line when summerwood was at the point of maximum shear. The failure occurred between the summerwood of one increment and the springwood of the 36 Figure 12. Migration of the static failure line. The arrow indicates the failure line slanted towards low-density springwood. 37 Figure 13. Straight-line shear failure in static specimen. The failure in this specimen occurred at the plane of maximum shear. 38 Figure 14. Failure occurring in a statically loaded specimen away from the plane of maximum shear stress. 39 following increment at a plane removed from the point of maximum stress. This resulted in material being sheared from the side of the testing-head groove as shown in Figure 14, page 38. FATIGUE FAILURE The method of multiple regression was used to determine the effect of specific gravity and stress level on the number of loading cycles to failure. .A graph of the data on linear paper evidenced an exponential relationship between the three variables. Semi-logarithmic plotting and analysis did not yield significant results. Log-log plotting finally showed a relationship that could be subjected to analysis by the method of multiple regression. A search of the literature revealed that multiple logrithmic regres- sion can be appropriately used as a method of statis- tical analysis (26). In order to facilitate the use of this analysis, the data for specific gravity were converted from three-place decimals to three-digit, 'whole numbers. The purpose for the translocation of the decimal point was to avoid the use of negative loga- rithms in the subsequent analysis; All data were con- verted to logarithms and analysed with the standard multiple regression procedure. The results are summarized in Table 4. Table 4. 40 Summary of the results of the regression of number of cycles to failure on shear stress and specific gravity for white fir, western hemlock, and Douglas-fir. White Western Fir Hemlock Douglas-fir Mean specific 316' 393' 437' gravity Mean shear 315 psi 486 psi 480 psi stress Mean no. of cycles 1569 888 1175 byl°2 0.597 8.105 10.249 t for ‘5y1‘2 0.066 3.742** 3,034.. by2~l -7.424 -8.481 -10.625 t for ‘Byzoi 1.901 13.252** 7.601** R. 0.821** 0.942** 0.838** Species Equations of Multiple Regression White Fir Y Western Hemlock Y = (50828) X1 Douglas-fir Y R i - = (1.814)(10)20 x10'357 x2 7'35: 2 10.249 x -10.625 2 (31160) X1 the mean specific gravity figures are actually 0.316, 0.393, and 0.437. ** statistical significance greater than the 99 percent level. 41 Table 4.-Continued. by1°2 is the regression of number of cycles on specific gravity independent of shear stress. byZ-l is the regression of number of cycles on shear stress independent of specific gravity. R is the multiple correlation coefficient. Y is the estimated number of cycles to failure. X1 is specific gravity expressed as a three-digit whole number. X2 is shear stress at failure. The multiple regression of number of cycles on specific gravity and stress was significant for all three species. .A closer inspection of the partial regression coefficients reveal that in all three species the number of cycles to failure varies directly with exponential functions of specific gravity and varies inversely with exponential functions of shear stress. The equations of multiple regression define a curved, three-dimensional plane. In order to show the S-N curve graphically, it was necessary to hold one variable constant. Because it was the S-N curve that was desired, the relationships shown in Figures 15, l6, l7, and 18 were obtained for the average specific gravity in each species. The resulting two-dimensional curves are line intercepts on their respective three- dimensional, curved planes. The broken lines in Figures 15, 16, and 17 represent one standard deviation .cowbmfi>mc ccmucmpm sec upmoficca waned cmxonb one .A0Hn.0v 000 no zbfl>mnm onHomam ommco>m cm now vocsmbno mm: u>uso one .cfim 66023 060 m>nzo 2:0 .mH manage mmDAHo m0 mmmZDz mod 00d m0“ Jog no“ NOH 0“ H I I I I, 0 Ir, I [Y o J l I ll?! / 1.1 com 0 I [ill I I I I II 66 .l ./ J./ / l/nl ‘ / / .fi // / // / coo 000 0 r 000a 00N~ (“I“) 933313 mus h3 .cofium«>uc upmccwpm uco concave“ mesa“ auxocn one .Anon.00 non mo zufi>ma0 ommfiomam 60mpm>m cm pom cocsmbbo mm: o>nso one .xooflsun smegma: a00 m>pno 2:0 .0~ sesame mmDAH0 mo mmmZDz 50H 00H mofi do~ 000 . 0~ OH H 00m 1],, / l/ // /Z/w(/ oo: 6 1r 6 o / // o / // / Jw/ / /o/ c 000 000 000~ 00NH (’ISd) SSSHLS HVHHS .coabma>ma unmucmpm oco obwomucd macs“ cmxoub use .Amn:.0v we: mo zuu>mum ofimfiooaw emacu>m cm com cocsmbbo mm: o>pso och .cSMimmdmsoa com m>usu 2.0 .52 shaman mmDAH¢m Oh mMAQ>U m0 mmmzbz Nofi 00~ mod :0~ 00“ N0“ 0~ a .00N (l l l I a I 00.: I I 7 c 4] / oo o / o / o o l / / / O / > I! 0/ C A / 4]. 00¢ lo / / / / o 3 / I / / r / / /l e / OOQ 000d 00N~ ('Isd) ssauis evens 5 ifl. .cofibmmfibmm>cfl wasp c0 cmpmmp woaomaw swamp 000 com mm>pso Zsm .QH unamfim mquadx OH mmqu>u m0 mmmZDz Nos son mos :02 noa mod on a 0 com co: 000 000 a: 323 n // V / xooHEmn assume: lllll 0000 ufimammfimsom coma ('ISd) ssauis HVHHS 46 of estimated number of cycles. The magnitude of the deviation was obtained by the direct count of the number of logarithmic units separating the regression line from the plotted data points. The square root of the quotient of the sum of the deviations squared, divided by the degrees of freedom, yielded the logarithmic magnitude of the standard deviation. Inspection of Figure 18 reveals that the S-N curves are approximately the same shape for all three species. In addition the relationship between the stress levels for the three species at less than 100 cycles is about the same as under static loading. The failure line in fatigue samples occurred at the plane of maximum shear. The failure line was straight and parallel to the grain in all cases. Unlike the static samples9 no migration of the line of failure toward low density material occurred in the fatigue samples. It was extremely difficult to compare the shear stresses at failure obtained from static testing to those obtained from fatigue testing. The specific gravity dependence and the varying number of cycles to failure makes a direct comparison meaningless. The results indicated, however, that for samples in the same species with comparable specific gravity figures, the fatigue stress at failure was always 47 lower than the static stress at failure. The ratio of fatigue strength to static strength in shear parallel to the grain varied from 0.90 to 0.24 in Douglas-fir, 0.88 to 0.17 in western hemlock and from 0.95 to 0.36 in white fir. The above variations are averages and have no statistical significance between species. 48 DISCUSSION QE RESULTS The purpose of this section of the thesis is to review the sources of error with respect to the results obtained by the analysis. The results of this research are not in themselves the total answer to the questions probed during the course of the study. Careful examination must be made of the sources of error and of the underlying factors that occasion the variables that were measured as a portion of this research. To insure clarity, the origin of error in specific gravity and moisture content determination will be discussed in separate portions of this section. The relationship between specific gravity and shear stress at failure for the statically loaded specimens will also be covered in the discussion. Lastly, the factors that affected the regression of number of cycles to failure on the specific gravity and on the shear stress in the fatigue specimens will be reviewed. SPECIFIC GRAVITY To satisfy the purposes of this research, the sections of wood used to determine specific gravity were cut from both sides of the failure line. These sections were very thin. As a result, the volume of such sections was correspondingly small and the ratio 49 of surface area to volume decreased rapidly with an increase of thickness of the section. It was antici» pated that the percent possible error in specific gravity of a thin section would be many times greater than the percent possible error for a relatively thick section. In addition, it was obvious that any accurate control of thickness for the specific gravity sections was impossible. The percent possible error in specific gravity was estimated with the partial differential method and was found to vary from almost 100 percent for very thin sections to approximately one percent for the thickest sections. An effort was made to cut the specimens at a thickness that would yield an error of about fifteen percent. This figure allowed for sections thin enough to obtain material directly adjacent to the line of failure and of sufficient thickness to measure with an acceptable amount of error. The specific gravity at the line of failure was greater in the fatigue specimens than in the static specimens for all three species tested in this research (Table 1, page 27). This difference was caused by the tendency for the failure line to migrate toward low density springwood in the statically loaded samples. The average for a group of such samples would necessarily be lower than for the fatigue 50 samples in which failure occurred in the early spring- wood only if such material was at the plane of maximum shear stress. Because the western hemlock stock had a large proportion of summerwood, the specific gravity for fatigue samples was significantly greater than for the static samples. Douglas~fir and white fir stock had a greater proportion of springwood and, as a result, a nonnsignificant difference in specific gravity appeared between the static and fatigue samples. The physical sources of error in the determination of specific gravity were as listed below: 1. Thickness of sections. The thickness of each section was variable due to small deviations in the plane of the failure. It was not possible to cut a section so that the plane of the cut was equidistant from the plane of the failure at all points. The resulting error could be either positive or negative. 2. Roughness of failure plane. In many samples the plane of failure was characterized by alternating grooves and ridges. The size of the grooves limited the mercury contact since, at standard temperature and pressure, mercury will not pass through an opening 51 smaller than twowthousandths inches. The resulting error in specific gravity was negative in all cases. Fuzziness of failure_plane. The failure plane in western hemlock was characterized by a fuzzy appearance caused by the partial separation of some cells from the mass of material. These cells inhibited full contact by the mercury and induced a negative error in specific gravity figures. Change of moisture content. The time required for the measurement of the weight and volume of each section was approximately three minutes. Since this work was conducted under controlled temperature and humidity conditions, it was exceedingly unlikely that any large error was introduced by changes in weight or volume. Trapped air in mercury reservoir. Trapped air could be avoided by using the same mercury for only ten or twelve specific gravity measurements. Minute particles of wood caused air bubbles to appear in the volumeter sight-tube if more than a dozen determinations were made without changing or cleaning the mercury. In this research, the mercury was 52 changed when air bubbles began to appear. The presence of air bubbles induced either a positive or negative error in the specific gravity. 6. Change of temperature. The mercury volumeter was extremely sensitive to changes in temperature due to the relatively high coefficient of thermal expansion of mercury (13). The sources of error listed above were controlled as closely as possible during the experimental work and it may be said with assurance that the physical errors were relatively unimportant in the summation of their effect on the specific gravity of a specimen. The mercury displacement volumeter provided the writer with a useful, accurate instrument for the determination of volume for small, hygroscopic pieces of material. MOISTURE CONTENT The results of the moisture content determinations showed that in each species the average moisture content of the static samples was greater than that of the fatigue samples. The difference was caused by the time required for testing. Each static sample was tested over a time interval of one to two minutes in contrast to the fatigue samples that required from 53 several minutes to ten hours. The moisture conditions at the time of fatigue testing were such that water was lost from the wood. As the results in Table 2, page 28, point out, this loss of moisture was signifi~ cant for fatigue samples. The moisture loss was un- doubtedly accelerated by higher temperatures in the wood induced by friction of the testing=head against the wood. Despite the significance of the moisture content difference between static and fatigue samples, the mag- nitude of the difference was quite low. In western hemlock, where the difference was the greatest, the average moisture content of the fatigue samples was only 1.7 percent higher than that of the static samples. The physical sources of error in the moisture content determinations were as listed below: 1. Change in humidity. Static and fatigue testing were conducted day and night during the early summer months when the relative humidity differential can be unusually high. Samples that were tested and weighed at night exhibited a higher moisture content than those measured at mid-day. The resulting change in moisture content was either pos» itive or negative. 2. Balance inaccuracies. The samples were weighed on a triple beam balance before and after 54 oven-drying. Any inaccuracy intrinsic to the balance would produce an error in the moisture content. The balance was zeroed periodically to minimize error. The change in moisture content was either positive or negative. 3. Moisture movement during weighing. A small amount of error was introduced by the addition of moisture during the time required to obtain the ovenndry weight of the specimens. The error was the same for each sample and induced a negative effect on the moisture content. The maximum, possible, physical error was cal~ culated by the partial differential method at the exu tremities of the moisture content range. The percentage possible error due to physical measurement varied from seven percent to ten percent. Inspection of Table 2, page 28, shows that the moisture content variance for each test method in each species is relatively low. This indicates that the error due to physical measure- ment was insignificant and it can be assumed that all the moisture content figures for either test method in each species, were drawn from a common population. STATIC FAILURE The results summarized in Table 3, page 29, indicate that the stress level at shear failure under 55 a static load varies directly with the specific grav» ity of the wood at the line of failure. The variance of this relationship was influenced by error in speci- fic gravity (see page 50) and by errors made in the determination of stress level at failure for the statically loaded shear specimens. The sources of error for loading are listed below: 1. Stress concentration. The possibility existed that the specimen did not support the load evenly at all points of the contact area between the testing-head and the sample. This could occasion failure at a stress level considerably lower than was anticipated. The error due to stress concentration was minimized by the use of a rubber mat under the testing-head to distribute the load over the shear section of the sample. Loading. The testing machine was recalibrated previous to this research to give an error of about one percent at the load range for the static testing to be done as a portion of this problem. The error induced by loading could have been either positive or negative. Shear area. The shear area could not be measured exactly until after failure had occurred and could not be measured exactly 56 when the plane of failure was rough. The result was higher stress values than were actually present. The percent possible error for shear stress under static loading was computed by the method of partial differentials. The error in stress varied from six percent for the greatest load to nine percent for the smallest load. The scatter of the data shown in Figures 8, 9, and 10 was influenced more by error in specific gravity than by error in stress. Since the regression of shear stress at failure on specific gravity was significant for all three species, the combined experimental error may be considered unimportant. FATIGUE FAILURE The multiple regression of number of cycles to failure on specific gravity and stress level was influenced by physical error in the measurement of all three factors. The error contributed by specific gravity is discussed on pages 48 to 52 of this paper. The physical error involved in determining the number of cycles to failure was extremely small and may be ignored. The factors listed below are those that influenced the magnitude of the measurement error for shear stress at failure: 1. Stress concentration. The stress concentration factor for fatigue loading was the same as 57 for static loading (see page 55). Loading. The magnitude of the load at failure constituted the most significant source of error in the estimation of the fatigue strength in shear. The error was occasioned by the stress relaxation that occurred in the specimens and by the subsequent decrease in the static preload on the testing machine. The error was more pronounced at a relatively low number of cycles to failure because the reduction of the static preload was most pronounced at the early stage of loading. This source of error would have been virtually eliminated if the testing machine had an automatic preload adjustment. Unfortunately, such equipment was not available for this research. The decrease of static preload resulted in a negative error in shear stress and a positive error in the number of cycles to failure. Bending moment. The presence of a bending moment across the shear section produced error in the shear stress and, consequently, in the number of cycles to failure. Because the bending moment at the plane of maximum shear was 58 small, the error was small when the failure occurred at the plane of maximum shear. 4. Horizontal load components. The testing« head guides were designed to make the loado multiplier transfer only the vertical com~ ponent of the machine load. However it was unreasonable to assume that the horizontal loading component was zero. The horizontal components of load resulted in positive error in shear stress and negative error in the number of cycles to failure. This factor somewhat compensated for the error induced by the decrease in the static preload. The percent possible error for fatigue shear stress was determined for the highest and lowest values of load by the method of partial differentiation. The percent error varied from eight percent for the highest load to seventeen percent for the smallest load. Because change of stress is reflected directly in the number of cycles to failure, a small change in stress at the end of the S~N curve would yield a relatively unimportant change in the number of cycles to failure. The same change of stress at the beginning of the S—N curve could lead to an extremely significant change in the number of cycles to failure. 59 CONCLUSIONS THEORIES OF FATIGUE FAILURE The exact mechanism of fatigue failure in wood is an unknown quantity. This is not surprising since there exist many schools of thought concerning fatigue failure for materials that have received a great deal more attention than has wood. There is no doubt that the mechanism of fatigue in wood is similar in some respects to that for metals, plastics, and glass. This portion of the paper is devoted to a review of the more important theories of failure and a discussion of their utility for wood. The theories mentioned in this section are secondary stresses, hysteresis, and molecular slip. Secondary Stresses This theory states that a difference exists between the actual strengths of solid materials and the strengths they ought to possess by reason of molecular cohesive forces (6). All materials contain sub-microscopic defects that reduce the actual strength. These defects occur on both the interior and exterior of the material and furnish a position for failure to begin before the maximum stress can be developed. In addition, the 60 presence of internal stresses can reduce the magnitude of stress at failure. When applied stresses are imposed on pre-existing residual stresses. the resultant stresses are impossible to determine before failure actually occurs (12). The theory of secondary stresses appears at least partially significant to explain the mechanism of fatigue failure in wood. There are innumerable factors that can introduce microscopic defects and internal stresses to wood, both in the growing tree and in the preparation of wood for any particular use. In the growing tree, defects and internal stresses are occasioned by such factors as the weight of the tree, wind loads, snow loads, and frost action. In addition, all the many environmental conditions that influence the growth rate of a tree could also affect the amount and distribution of microscopic defects and residual stresses in the wood. These defects and stresses can be magnified and increased numerically by the logging and machining methods that are necessary to convert the tree into a wood product. The inevitable drying of the wood complicates the picture further by the addition of still more defects and residual stresses. If all the microscopic defects and residual stresses could be somehow eliminated, the natural morphology of wood itself contains factors that 61 account for increased stress. Some of the more important characteristics of wood that may be stress- raisers are listed below: 1. Specific gravity. Difference in specific gravity in adjacent portions of wood are a function of cell wall thickness. The relatively high specific gravity of summerwood in softwoods results from thick cell walls in contrast to the low specific gravity of wood resulting from thin-walled springwood cells. When the cells are supporting a load parallel to their long axis, there is a greater cell wall area sustaining the load in summerwood with a resulting lower stress. At the same load, the thin-walled springwood cells, with a smaller cell wall area, must withstand a greater stress. As a result, it may be theorized that the weakest portion of the wood is in the early springwood where the specific gravity is lowest. The results of the research reported here appear to substantiate this theory. Type of cells. The type and the amount of cells that are supporting or resisting a load on wood can have a pronounced influence on the stress at failure in shear parallel to 62 the grain. Some cell types are character- istically thin or thick walled in certain species. The number of cells of a particular kind will produce a specific gravity depen- dence as described above. Parenchyma cells, for example, are normally thin-walled in some species and, if present in a sufficient number, could introduce a source of stress concentration. Slope of fibrils. The secondary cell wall of woody plant tissue exhibits fibril ori- entation at an angle to the long axis of its cellular components (5). The fibril angles in the three layers of the secondary wall are generally totally different from one another, resulting in a complex stress formation inside the cell wall. Stress concentration could be expected to be maximum where the deviation of fibril alignment was greatest between adjacent layers of the secondary cell wall. In addition, the fibril alignment is variable from one cell to another. This could be a significant factor between summerwood and springwood where the difference in fibril alignment is maximum in adjacent cells. 63 4. Pits. Woody plant cells are characterized by the presence of pits between adjacent cells. These recesses in the secondary cell wall distort the normal fibril alignment in the cell walls and are effective stress raisers. The number, size, and distri- bution of the pits vary from one species to another and, as a result, may have a greater or lesser influence on the magnitude of the stress. 5. Sub-microscopic structure. The pattern of the cellulose in plant cell walls is not continuous. The long chain molecules of cellulose within the fibrils have alternate regions of parallel and non-parallel arrangement. The parallel regions are called crystalline and the disorganized regions are known as the amorphous areas (5). The discontinuity formed by the amorphous regions may serve as a stress raiser in shear parallel to the grain. Hysteresis Wood is not a perfectly elastic material. The slightest load on a wood member will induce some 64 permanent deformation too small to measure. In addition, if stress-strain diagrams are made for the loading and unloading of a sample, the points will not coincide exactly but will form a loop, called the hysteresis loop (16)(28). The area inside the loop is directly proportional to the amount of energy lost in the cycle, and the strain after one complete cycle is the permanent deformation. The energy loss is probably due to friction and is given off as heat. The hysteresis loops occur even within the elastic regions of wood. The hysteresis effect is very slight in wood for a single loading and unloading cycle at very low stress. However, if the stress is greater and if the stresses are repeated with sufficient rapidity, the strain can accumulate until failure eventually occurs. For very low, alternating stresses, ‘ the hysteresis loop may be a straight line. As the fatigue loading progresses, the hysteresis loop broadens more and more to eventual failure. Molecular glip Repeated stresses in metals result in the formation of "slip bands" in the crystals (9). These slip bands increase with the number of stress appli- cations until failure occurs when the bands cover the entire surface of the crystal. An analogous feature called 65 the slip plane, has been found in the cellulose of wood that has been subjected to mechanical stress (l4)(l7)(25)(30). There is some doubt regarding the origin of the slip planes in wood, but the possibility certainly exists that these planes represent minute failure in the crystalline region of the fibril. Continued fatigue loading would cause the formation of new slip planes and the enlargement of already existing slip planes to failure. APPLICATION OF FAILURE THEORIES This study has shown that wood appears to have a definite fatigue limit in shear parallel to the grain. The exact fatigue limit for a particular sample is difficult to determine in advance because of the strong influence of specific gravity at the plane of maximum shear. The fatigue strength of wood in shear parallel to the grain is different for different species and must be determined experimentally for each species. The exact mechanism of fatigue failure appears to be different from the mechanism of static failure. Previous research has shown that static failure of wood in compression occurs along a shear plane between the outer and central layers of the secondary cell wall and that the failure spirals along the length of the cell (3). This indicates that the maximum stress 66 position rotates as failure progresses. If this holds true for shear failure under static load, it partially explains the migration of the static, shear failure observed in this experiment. The maximum stress could be transferred through the isotropic compound middle lamella from a strong cell of high specific gravity to a weaker cell of lower specific gravity. This may have taken place since in all cases the migration was toward a region of low specific gravity. It is evident that investigation into the anatomy of shear failure under a static load is essential to the eventual solution of this portion of the problem. If it is assumed that the theory, postulated above, for the mechanism of static, shear failure is correct, then it is evident that the mechanism of fatigue shear failure is different. The evidence to support this contention lies in the fact that there was no migration of the shear line of failure in the fatigue specimens. Since the line of failure was straight there was little lateral transformation of shear stresses. This suggests several possibilities. First, the possibility exists that the stress occurred primarily in the isotropic region of the compound middle lamella. If this actually happened, then the mechanism of fatigue failure was probably a combination of secondary stresses and hysteresis. The hysteresis 67 loops would be progressively broadened by the energy loss attributable to failure by secondary stresses in the middle lamella. Another possibility for failure in fatigue is that it may occur within the cell wall. The mechanism of failure is then a combination of secondary stresses, hysteresis and molecular slip. In this study, as in many others in wood research, emperical equations were obtained through laboratory testing and statistical analysis. In orig- inal research it is important to first demonstrate the presence of a phenomenon; in this study the phenomenon was shear failure parallel to the grain in wood subjected to fatigue loading. This occurrence was shown to be inclusive by the method of testing and by the manner of failure. If the concent of fatigue in shear for wood is accepted, the next portion of the research should properly be an effort to determine the influence of various agencies on fatigue in shear. In this study, the influence of stress level and specific gravity were studied in an effort to estimate their contributiOn to variation in fatigue. When all the sources of variation have been explored, it should be possible to begin further research to learn the exact origin and mechanism of fatigue failure in shear for wood. Such research is not possible until all the sources of error have been estimated, 68 to enable the researcher to either elimate or account for them. Such errors may be occasioned by variables that have not been evaluated in this study. These include moisture content, temperature, residual stresses, presence of extractives, degree of lignifica- tion, damping capacity, and elastic and plastic defor- mation. All these variables, however, can be called superficial. They are merely outward manifestations of some internal change in the wood itself. The internal changes constitute the real failure due to fatigue loading. It is the author's intention to continue this research to its logical conclusion. 69 SUMMARY Wood can be made to fail by fatigue loading in shear parallel to the grain on a tangential plane. There is a linear relationship between shear stress and specific gravity at the line of failure for samples tested in static shear parallel to the grain on a tangential plane. There is a significant regression of stress level and specific gravity at the line of failure on the number of cycles to failure in shear parallel to the grain on a tangential plane. A linear relationship exists between shear stress and specific gravity at the line of failure in wood tested by fatigue loading in shear parallel to the grain on a tangential plane. The early springwood offers the least resistance to loading in shear parallel to the grain. The mechanism of fatigue failure in shear is different from that of static shear failure. The stress level at failure for fatigue shear samples is less than for samples tested under a static load for samples of the same species with comparable specific gravity values. 8. Additional research into the mechanism of fatigue failure in wood is necessary. 70 10. 71 W1 LIST OF.APPARATUS White fir stock from which samples were prepared contained about four and one-half growth increments per inch. western hemlock from which test samples were ‘prepared contained about twenty growth increments per inch. Douglas-fir stock from which test samples were prepared contained about twenty-one growth increments per inch. Band-saw. 36 inch band-saw, Model B-l8388, made by the Yates-American Machine Company, Beloit, Wisconsin. Static Testing Machine. Baldwin-Emery, SR-4 Testing Machine, Model F6T, manufactured by the Baldwin-Lima-Hamilton Corporation, Philadelphia. Fatigue Testing Machine. Sonntag Universal Fatigue Testing Machine, Model SF-OléU, designed by the Sonntag Scientific Corporation, Greenwich, Connecticut. Strain Gages. SR-4 Strain gages, Type AD-7 with a resistance of 120 ohms and gage factor of 1.95. Gages manufactured by the Baldwin- Lima-Hamilton Corporation, Philadelphia. Strain Amplifier. Baldwin SR-4, Type M, Portable Strain Indicator manufactured by the Baldwin-Lima-Hamilton Corporation, Philadelphia. Triple Beam Balance. Cenco Agate Bearing, Triple Beam Balance, made by the Central Scientific Company, Chicago. Drying Oven. Fisher Senior Forced Draft , Isotemp Oven, made by the Fisher Scientific Company, New York. 72 List of Apparatus.-Continued. 11. 12. 13. 14. Volumeter. Mercury displacement volumeter designed by the author from a prototype and made by the Metal Machining Company, Lansing. velumeter. Mercury displacement volumeter designed by Dr. Everett Ellis. Associate Professor, University of Michigan and made at the University of Idaho machine shop, Moscow, Idaho. Grammatic Balance. Gram-matic Balance made by E. Mettler, Zurich, Switzerland, and distributed in the United States by the Fisher Scientific Company. New York. Calculator. Friden Automatic Calculator Model STW, manufactured by Friden Inc. San Leandro, California. APPENDIX 1; DATA Table a. Data recorded for white fir samples tested in static shear parallel to the grain. Moisture Specific Shear Content Gravity Stress (7») (psi) 9.46 0.338 492 10.64 0.452 800 9.43 0.317 456 9.66 0.348 575 9.74 0.268 427 10.79 0.439 879 10.69 0.365 678 9.76 0.250 260 10.63 0.304 309 10.75 0.284 564 10.70 0.250 208 9.30 0.232 232 10.73 0.206 204 9.47 0.328 656 10.67 0.306 425 9.40 0.346 435 10.66 0.250 295 10.76 0.228 315 10.78 0.242 385 10.67 0.374 643 74 Table b. Data recorded for western hemlock samples tested in static shear parallel to the grain. Moisture Specific Shear Content Gravity Stress (%) (psi) 13.87 0.275 910 14.05 0.344 1130 14.06 0.368 1129 13.55 0.296 896 13.63 0.280 817 13.80 0.360 1234 13.77 0.420 1386 13.76 0.446 1498 13.59 0.323 1114 13.56 0.326 1057 13.43 0.338 1249 13.13 0.382 1212 13.09 0.412 1540 12.95 0.301 922 12.95 0.375 1407 12.84 0.398 1251 13.13 0.352 991 13.03 0.374 1084 12.89 0.372 1276 13.44 0.405 833 Table c. Data recorded for Douglas-fir samples tested in static shear parallel to the grain. Moisture (Specific Shear Content Gravity Stress (7») (psi) 12.27 0.441 1071 12.44 0.408 825 12.62 0.380 883 12.46 0.404 941 12.59 0.360 756 12.55 0.414 1022 12.27 0.454 1162 12.24 0.389 1263 12.55 0.470 1270 12.56 0.496 1307 12.55 0.391 1011 12.31 0.416 1023 12.01 0.449 1155 12.10 0.505 1397 12.26 0.464 1268 12.40 0.336 781 12.38 0.426 979 12.16 0.473 1323 12.04 0.448 1093 11.94 0.446 1050 76 Table d. Data recorded for white fir samples tested in fatigue. Moisture Specific Shear Cycles to Content Gravity Stress Failure (%) (psi) 10.66 0.306 340 1,000 10.56 0.324 448 100 11.11 0.313 294 1,000 10.74 0.285 347 200 10.66 0.338 170 1,650,000 10.93 0.310 429 200 10.67 0.279 242 4,000 11.22 0.297 190 1,250,000 11.32 0.363 225 1,000 11.25 0.282 219 190,000 11.09 0.384 656 50 11.11 0.281 500 300 10.83 0.542 400 10 11.00 0.318 400 40 11.04 0.322 300 400 10.69 0.306 225 4,000 10.71 0.279 200 49,000 10.67 0.294 300 2,000 11.29 0.313 400 5,000 10.08 0.268 350 300 77 Table e. Data recorded for western hemlock samples tested in fatigue. Moisture Specific Shear Cycles to Content Gravity Stress Failure (%) (psi) 12.60 0.347 544 100 12.17 0.380 657 175 12.67 0.390 876 5 12.55 0.420 706 500 12.82 0.340 716 10 13.06 0.436 384 10,000 12.81 0.366 604 30 12.84 0.370 439 1,000 11.78 0.366 414 1,000 11.85 0.368 268 200,000 11.66 0.422 334 98,000 11.22 0.410 450 5,000 11.68 0.448 450 2,000 11.74 0.342 450 1,500 9.84 0.358 450 1,000 9.53 0.380 450 3,000 10.74 0.326 634 30 9.65 0.486 734 100 11.69 0.394 782 50 12.33 0.444 450 16.000 11.77 0.384 453 100 11.82 0.350 . 564 10 12.24 0.354 763 100 12.19 0.379 572 50 12.11 0.512 500 3.000 10.63 0.410 217 750,000 11.69 0.409 466 100 12.47 0.412 784 10 11.33 0.380 191 3,000,000 11.05 0.491 268 3,000,000 78 Table f. Data recorded for Douglas-fir samples tested in fatigue. Moisture Specific Shear Cycles to Content Gravity Stress Failure (%) (psi) 11.50 0.532 536 2,000 10.86 0.424 660 50 11.32 0.493 442 9,000 10.55 0.471 847 20 10.91 0.450 454 100 11.35 0.444 511 1,000 11.28 0.386 581 20 11.00 0.432 505 2,500 11.02 0.394 700 10 11.55 0.418 408 5,000 11.19 0.390 404 1,000 11.21 0.442 358 52,000 10.83 0.456 520 200 11.20 0.449 367 1,250,000 11.14 0.402 824 10 11.09 0.420 514 400 11.28 0.491 392 1,200,000 11.06 0.384 464 300 11.22 0.530 602 2,500 10.98 0.439 253 1,500,000 10.87 0.466 428 1,500 10.67 0.440 495 60 9.68 0.396 706 40 10.82 0.430 565 50 10.95 0.504 378 22,000 11.11 0.382 307 2,200,000 11.32 0.313 349 500 10.92 0.520 505 1,000 10.87 0.418 381 21,000 11.13 0.485 498 500 79 LITERATURE CITED American Society for Testing Materials. "Testing Small Clear Specimens of Timber," Book of Standards, Pt. 4, Serial Designation D I43-52, Am. Soc. Test. Mat., Philadelphia, 1955. Baldwin-Lima-Hamilton Corporation. Instruction Manual for Universal Testing Machin . An Instructioananual Distributed By tfie Sonntag Scientific Corporation, Greenwich, Conn., 1951. Bienfat, L. J., "Relation of the Manner of Failure to the Structure of Wood under Compression Parallel to the Grain," Journal of A ricultural Research, Washington, D. C., p. 3:_l9§6. Brown, H. P., Panshin, A. J. and Forsaith, C. C., Textbook gf'Wood Technology, Vol. 1, McGraw-Hill Book Co., New Tork, . Brown, H. P., Panshin, A. J. and Forsaith, C. C., Textbook 2f Wood Technology, Vol. 2, McGraw-Hill Book Co., New York, . Cazaud, R., Fati ue of Metals, Philosophical Library Inc., New TOTE, I953. Coker, E. G. and Coleman, G. P., "Photoelastic Investigations of Shear Tests of Timber," Selected Engineering Pagers, Institution of Civil Engineers, 0. , Lon on, 1935. Dietz, A. G. H. and Grinsfelder, H., "Behavior of Plywood under Repeated Stresses," Transactions, American Society of Mechanical Engineers, April, 1943. Ewing, J. A. and Humfrey, J. C. W., "The Fracture of Metals under Repeated Alternations of Stress," Philosoghical Transactions, Royal Society, 0 o , 3. 80 Literature Cited.-Continued. 10. 11. 12. 13. 14. 15. 16. 17.‘ 18. 19. 20. Forest Products Laboratory. Wood Handbook, Agricultural Handbook No. 72, United States Government Printing Office, Washington, D. C., 1955. Freudenthal, A. M., "Planning and Interpretation of Fatigue Tests," Statistical Aspects of Fati ue-A Symposium, American Society of_Testing Materials, Stp. No. 121, 1951. Gilchrist, J., "On Wohlers Laws," Engineering, Vol. 90, 1900. Hodgman, C. D., Weast, R. C. and Selby, S. M., Handbook of Chemistry and Ph sics, Ed. 39, CEemicaI Rfibber Publishing Co., Cleveland, 1958. Hohnel, von P., "Ueber den Einfluss des Rinden- druckes auf die Beschaffenheit der Bastfasern der Dicotylen," Jahrbucher fur Wissenschaftliche Botanik, No. 15, Berlin, p.-3I1, 1884. HOPPG, 0., "Albersts Versuche und Erfindungen," Stahl und Eisen, Vol. 16, Berlin, 1896. Houwink, R., Plasticity Elasticity and Structure ‘gf Matter, Harren Press, Washington, D. C., I953. Kisser, J. and Steininger, A., "Makroskopische und Mikroskopische Strukturanderungen bei der Beigebeanspruchung von Holz," Holz gig RohéUnd Werkstoff, No. 10, p. 415, 1952. Kollmann, P., Technologie des Holzes und der Holzwerkstoffe, V01. 1, Springer-Verlag, Berlin, 1951. Kommers, W. J., "Effect of 5000 Cycles of Repeated Bending Stresses on Five-ply Sitka Spruce Plywood," United States Forest Products Laboratory, F. P. L. mimeo. 1305, 1943. , "Effect of Ten Repitions of Stress on the Bending and Compressive Strengths of Sitka Spruce and Douglas-fir," United States Forest Products Laboratory, F. P. L. mimeo. 1320, 1943. 81 Literature Cited.-Continued. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. 32. ,Jf, , "The Fatigue Behavior of Wood and Plywood Subjected to Repeated and Reversed Bending Stresses," United States Forest Products Laboratory, F. P. L. mimeo. 1327, 1943. Leggett, J. L.9 "Investigation of Fatigue Strength of Railroad Timber Bridge Stringers," Bulletin, American Railway Engineering Associ- ation, No. 510, 1953. Lewis, W. C., "Fatigue of Wood and Glued Joints used in Laminated Construction," Proceedin 8, Forest Products Research Society, p. 22!, I951. Marin, J., Engineering Materials, Prentice Hall Inc., Englewoo s,7NEwTJersey, 1952. Searle, G. 0., "The Microscopic Structure of‘ Tendered Fibers," gournal, Textile Institute, No. 15, p. 371, 19 . Severo, N. C. and Olds, E. G., "A Comparison of Tests on the Mean of a Logarithmico-normal Distribution with known Variance," Annals of Mathematical Statistics, v61. 27, N‘_36. T 1936. Snedecor, G. W., Statistical Methods, Ed. 4, The Iowa State College Press, Ames, Iowa, 1946. Timoshenko, S., Strength 2f Materials, Lancaster Press Inc., Lancas er, Penn., 1930. Walker, H. M. and Lev, J., Statistical Inference, Henry Holt and Company, New York, 1953. Wardrop, A. B. and Dadswell, H. E., Council of Scientific and Industrial Research, Bulletin 221, 1947. Weibull, W., "A Statistical Representation of Fatigue Failures in Solids," Transactions, Royal Institute of Technology, No. 22, 1949. Yavorsky, J. M., Cunningham, J. H. and Hundley, N. G.,"Survey of Factors Affecting Strength Tests of Glued Joints," Iournal, Forest Products Research Society, Vol. 5, o. , 1955. .rh.‘ «“5“ ”\f ....n{~?f-ti “5E- Ea“— “U .31“ 9 1:53.416 Jar-‘7 ... -. M ,1}? w- i“ H" M ' 7“"- IV ‘ . _. .1..- - -‘—= r O ‘- “a “ 1845 . Hirllllmimumn 31