~ oM ICHIGAN STATE UNIVERSITY LIBRARIES EET 3 1293 00627 1047 La paetbrtee ate TS 1 Nee ge wey i ba = » = ae “oe ee S a Nea 2 : se i ae hag “ +4 be. La’ a Le Oe oo? $. 7 a ek | CHIGAN STATE UNIVERSITY LIBRARIES TTT 3 1293 00627 1047 a wet tes BF Ae “7 - ° A STUDY OF THE EFFECT OF TIME AND TEMPERATURE UPON THE SWELL OBTAINED ICE CREAM. A Study of the Effect of Fime and Temperature Upon The Swell Obtained Ice Cream. Thesis for Degree of M. 8. Hohei Funayama, B. 8. fokyo Agricultural College, Japan. 1921 THES!S CONTENTS Introduction. Historical discussion Reason for making study Disoussion of swell Review of literature Outline of experiment Bffeot of freesing temperature Effect of time for freesing Preparing the mixture Method of freesing Method of taking test Experimental work. Experiment charts Correlation time, temperature and swell Experimental tables Summary Bibliography 96339 INTRODUCTION Ice cream is a term applied to a variety of frozen products, but commonly means a frozen mixture of crean, suger, whole milk, skim milk, condensed milk, evaporated milk or skim milk powder and flavoring substances. Ice cream is usually agitated by a dasher in the freesing process to make it smooth and of uniform consistency. Historical: Ice cream is usually used today as a food although in the past it was considered and used only as a delicacy or dessert. In ancient times "Cream Ice" was used on the table in England and France, which cream ice preceded the use of ice cream of today. That cream ice being of relatively modern origin. "Milk ice"and "Cream ice”™ were introduced into Emrope from Asia by Marcopolo and cream ice wag served at the Court of Charles the First of England, In 1776 English cream ice was made from milk, sugar . eggs, arrowroot or flour and flavoring extract. In the United States Ice cream was first prepared in New York by Mr. Hall. Ice cream was served at a dinner in Washington, at which dinner President Washington partook. The first wholesale ice cream business was launched in 1861 by Jacob Frussell of Baltimore. Ice cream made in this country is in great demand in other countries and consequently, steamers loading in New York take on this commodity for such distant countries as India, Japan, China and Australia. ~o5a= At the present time in U. S. ice cream consumption is greatly increasing and is important branch of the dairy industry. | Oriental countries never had tried ice cream making except only a few home made ice creams. There was an old record that ice cream was introduced by an American. For this reason, China and Japan have retained the custom of "no use milk, no use meat to eat™ because of the Buddist doctrine (religion) until about 10 years age. Reason for making study : Im Japan commercial ice cream was first made about seven years ago in Tokio by freesing by hand process. Since that time ice cream con- sumption has consequently increased during these few years. In 1920 the first ice cream manufacturing plant wag built in Tokie by the Oriental Condensed Milk Ce. At the present time in Japan ice cream making is changing from the hand process to the factory method used in the dairy industry. There have been very few investigators who have studied the technique and soience of ice cream making in China and Japan, This is very regretable for dairying in the Eastern Countries. For this reason the writer has taken up the study ef modern ice oream making at the Michigan Agricultural College in United States, America. He expects to introduce American ice cream making into China and Japan and carry en further studies of ice cream making under conditions prevailing in Eastern Countries. | , _Discussion ef Swell in Ice Cream: The swell is an important item in commercial ice cream making. The swell ef ice cream is due chiefly to the air which is inoorporated « . :- pap a t~ during the freesing process by the violent agitation, s0 that the finished product eccupies a larger space than the original mixture. The larger the swell obtained the more air there is incorporated in the ice cream and the more open will be the texture of the product. A certain amount of swell is necessary in a high grade ice cream to give desirable texture and smeothness. If too little swell were obtained the ice cream weuld be icy, seggy and heavy and more solid, that is more Webght per volume. It would have to be sold at @ proportionately higher price and the consumers would either be paying more for their dishes er receive a smaller serving for their money of a coarse and oold product and not generally relished. The swell should be properly done. If the swelling igs not preperly done the results is a loss in both quality and quantity of ice cream. Usually best results are obtained With 90 to 100 or 110 percent,swell depending upon the compesition ef the nix. fhe temperature while freezing in the machine is a most important factor influencing the swell. Other principal causes of variation in swell are total time te freese which has a noticeable effect on the amount swell and the quality, kind of material used, pasteurized of cream, homegenization of cream, amount ef sugar and total solid, spped ef dasher and type ef machine, Im pasteurized cream, the pasteurization temperarily destroys the viscosity of the cream and milk and as a result pasteurized cream must be aged longer to restore the aw = ap viscosity. Homogenizing cream breaks the solid of cream and milk into smaller particles. The whole mix is homogenized before going to the freeser. This increases the viscosity and because ef this and of the smaller particles more swell is pessible without sacrificing quality. The amount of sugar is imporéant enly because ef its bulk, and the rate of freezing is also affected by amount of sugar and solid in ice cream, The mae sugar added the more selids in ice cream, that is ebtained more swell. The total solid in the mix have a decided influp ence en the amount ef swell that can be obtained without imjury te the quality of the ice cresm. REVIEW OF LITERATURE. Phere is some published literature relative to the influence ef various facters to the swell in ice cream making. In 1910 a study ef the swell in ice cream making was published by (1) Washburn. Washburn states that swell commences to form at 34° F., and ceases to form at 27°#. The maximum is reached at 28.5° F., but the cream mix should not be removed from the freezer before the temperature has reached 28° F., etherwise some of the swell is lost by the loss of air. When the swell exceeds 80 percent of the mixture the kody ef the ice cream deteriorates. In 1916 (2) &. CG. Baer illustrated that five gallons ef 18 percent cream, enough to make 10 gallons of ice crean, after the sugar, vanilla, filler, ests. have been added amounts to 5.7 gallons of mix. This made into 10 gallons of ice cream gives an incvpease in volume of 4.35 gallons by swell. And alse (3) Dr. Heineman in 1920 shows that two gallons ice cream with an 80 percent swell or increase in volume can be made from one gallon of mixture. foo low a swell produced a heavy soggy ice crean, too high a swell produce a light and fluffy. These facts have been illustrated by many investigators. Time required for proper freezing. Too rapid freesing will make peor quality and quantity of ice cream. According te (4) J. N. Frandesen and Markbam in 1915 the time required for the swell will be governed by several factors. Time required for freesing ice cream mixture will depend somewhat upon the composition but more upen the temperature of the mix when put into the freeser. (5) Washburn showed that “time required for swell under normal conditions will be from 10 minutes to 14 minutes”. (6) A. C. Baer published that “usually the best results are obtained by freesing the mix in from 10 minutes to 15 minutes and this does not freeze it too rapidly and at the same time allows plenty of time to whip the cream into the smooth consistency which is desirable in a good ice cream. (¥%) E. Williams decreeé that it usually required 20 minutes time to complete the swell ef a 10 gallon batch of ice cream with a brine temperature vo F. and with a constant normal speed of the freezer. According to (8) Walter W. Fisk "time required for proper freesing should be take from 12 minutes to 20 minutes". When removing the ice cream from freezer to the ~-Joo cans, (9) Washburm shows it was found that when drawn off at 29° FP. the awell was 70 percent, the best temperature being 28° F. even though at this temperature product was thin. (10) W. W. Fisk shows that colder the cream mix when it enters the freezer the quicker the freezing time. For best control he advises a temperature of 40° F. He states that when ice oream is drown from freesing at temperature and 28° #. between 26° F./best results can be obtained.(11) Wisconsin Agricultural Experiment Station reported that cream should be removed from freezer at 27° Fe. and many other investi- gators published almost same results for this temperature. The factors affecting swell by material used were discussed by some investigators (12) Walter W. Fisk illustrated that (a) age, viscosity and fat content of milk and cream (b) size of fat globules (a) pasteurized milk (a) aging milk (e) use of emulser or homogenizer $2) Method of mixing (g) use of condensed milk (h) amount of sugar (i) different kinds of flavoring (j) fillers and binder (k) total solids in mix. | (13) Washburam gives the following as the influ- ence of material used on swell. The amount of fat in the cream has little or nothing to do with the amount of air whigh may be incorporated, but it has much to do with ths amount which remaing incorporated. Skim milk can be made to swell 100% er even more, but the product is coarse and the results only temporary for it quickly loses its air and falls or sinks in the can. A cream containing 35% to 40% is too soggy to whip well and affords an poor increase . Viscosity of cream mix is of considerably more importance. Viscosity increases after having been held cold for 24 hours. (14) According to Iowa Agricultural Experiment Station bulletin 180, the swell of ice cream is less with fresh cream than with cream which has been aged for 24 hours to 48 hours. When pasteurized cream 24 hours older was used swell was obtained than with fresh cream i. e. The aged cream produced an ice cream of a more perfect texture andi swell than is produced from the fresh cream. Influence filler: (15) Walter W. Fisk, (16) Washburn states that fillers have little affect on swell. (17) A. CO. Baer, (18) M. Mortensen shows that fillers do not affect swell. The foregoing literature is all that has been published upon the swell in ice cream but is not a comprehensive study of the subject. OUTLINE OF EXPERIMENT. Bffect of freezing temperature on swell: | Preezing is the process of coeling the mix and getting it in such condition that it is edible when frozen. The temperature in freezing and rate of freezing are important factors in this matter of increase in volume, for the reason that if the freezing be done too rapidly too little time elapses to admit of its through whipping or beating during the interval after the cream becomes oold enough to whip and before it becomes frozen and produces a course grained preduct in which case satisfactory swell could not be ebtained. Teo slew freezing may cause the cream to chum causing chunks of butter in the ice cream giving greasy and lumpy condition. Temperature: Ordinarily mixture of cream sugar and other materials used in ice cream is not in proper condition to retain air whipped into it before it reaches about 29 F. At this temperature it begins slewly to form up and gradually increases in volume as the temperature drops from about 29°F. to 29° F or 26° F which temperature is a little below the freezing point. See experiment chart. BFFECT OF TIME FREEZING ON SWELL: Pime required in preper swell the experiments show ugually when the mix of cream entered the freezer at from 44°F. to near 40 F, the swell began in about four minutes. For such cream total time freezing required from 12 minutes to 18 minutes. Usually the first in five or six minutes of that will have been consumed in extracting specific heat in mix, so that the aswell scarcely increases during this time; and in the next stage few minutes would be required to extracted part ef the latent the heat ani suitable whipping or beating done to incorporate air with mix so that in this time volume of mix increases quickly and last few minutes will generally be consumed increasing ever 100 percent and in smooth up of ice cream. The follewing experiments shows the relation between time and effectivity of bfine off and on should be not --120- dgnored. It should be done in suitable point of time and freezing temperature. This important relation will be discussed by following experiments. PRiPARING DEX MIX. The materials in the mix were prepared in accordance with the following formula for each experiment. The mix being standardized to 14% fat and 37% percent total solids. Total weicht of whole mix 350 lbs. 140 lbs. 35% cream 14 lbs. skthm milk powder 143 lbs. skim milk 45 lbse sugar 2 1bs. | relatine The mechanical mixture used was of oriinary starter can type. The first materials of cream and skim milk put into the mixer ané@ start mixin: by mechanical asitator. The second, added into the mixer sugar, gelatine and skim milk powder which were prepared well mixed together. After these materials into mixer was well mixed the whole mix was pasteurized then immediately cooled down 110° F. and visoolizea at a pressure of 2000 lbs. From the viscolizer the mix flowed over a surface coil cooler, the top Sec.ion of which was cooled with water and the bottom section cooled with brine. The mix was then held in a refrigerator for 24 hours before freezing. Method of Freezing. The same machine was used for each experiment. Type of freezing machine is horizon- =--]3-— al with constant normal speed of the dasher(state speed). Size of machine, ten gallons. Frzezing done by circulating brine cooled by ammonia refrigerating machine. The brine was kept between 5° and 10° F. Point of freezing temperature 27.869 F. in that freezing process. Method of Taking Tests The records of temperature were taken ev2ry minute by themometer inserted in peep hole of freezer. Swell was tested every other two minutes by over run tester scale and over run oup. The scale used very sensitive being graduated to one hundredth of a lb. Overrun cup was adjusted to hold exactly one pound of mix. The swell for the following experiments was calculated from the weight of mix as follows according to indicated weight by scale. Percent overrun- Weigcht of mix--Wt. of sample x 100 Weight of Sample Example: Used 1 lb. of mix for adjusting cup. Weight of sample of same volume of ice cream 0.52 lbs. 1-00--0.52 x 100 = 92 0.52 92 percent overrun. Chart Explanation: According to chart No. l. Let the figures on the lower straight line A-B represent minutes of time during freezing process. A-C line represents ~-]4—=— swell in percentage. B-D line represents temperature in degree F., and N. line represents temperature of ice cream in freezer. M. line represents percent swell. EXPERIMEN? 1. Wight of mix 45 pounds Temperature of mix when entered the machine 44°R, Viscosity not heavy. This experiment shows the mixture cooled down quickly during the first 3 minutes from 44 dersrees to 29°r,. From 4 minutes to 10 minutes it cooled down to 26°F. while the swell increased 80 percent. Brine Was turned off at 10 minutes. At this time the mim in frvezer increased air bable and beat up incorporateé ing with air the swell slowly increased. The temperature after the brine turned off the temperature was going up and the mix becomes warmer. The swell increased until the tem- perature reached 28° F. Maximum percent of swell increased 130 percent at 27.5° F. in 18 minutes. At 28°F. the brine was turned on the temperature cooled down to 26° F. in few minutes. During this time the temperature cooled down by brine being turned on the swell decreasing rapidly. The brine was turned off again at 26°F. The temperature raised again and the swell raised in proportion. The length of froezing time of this experiment was — 40 minutes. When the ice cream was removed from the freezer the swell was 120 percent, temperature 27.3°R., at 40 minutes. The ice cream obtained was very softe -15- Exp. I. Table for Time, Temp., Weight and Per Cent Swell. Time Temp. Wt. & Swell Time Temp. Wte 3 Swell 9:02 40 9:24 28 9:03 32 9:25 28 46 118 9:04 29 93:26 28 9305 29 674+ 46 9:27 28 47% 110 9:06 28% 9:28 28 9307 28 634 57 9:29 28 49% brinel02 9:08 27.5 9:30 28 °* ' 9309 27 57 69 9:31 27.7 492 101 9:40 27 9:32 27.5 9:11 264% 56 brine78 9:33 287 504 99 9:12 26 oft 9:34 26% 9:13 26 51 96 9:35 26 52 brine 92 9:14 26% 9:36 26 on 9:15 27 47 113 9:37 26 £48 108 9:16 27 9:38 26% 9:17 27 444 124 9:39 26.8 462 115 9:18 27.2 9:40 26.8 9:19 27+ 44 127 9:41 27. 452 119 9:20 274 9342 27.3 9321 28 44 127 9:43 27.53 46 118 9322 28 9:23 28 44% 124 | q | Chart Exp e de 1801. 45 lb. Batch Temperature of brine Temperature of mim 4: 140. ly, 120. a 10Q_.._ . _.\__-_ recent 8Q_ in 60. le Swell 4Q_ 128 20. pr ane on A Oo 118 O 2% £ 6 F fo 1h LE 16 100 | EXPERIMENT ll. Weight of mix 45 pounds Pemperature of mix 44.8 °F. Temperature of brine 10 F. Freezing process at keeping 27°F , temperature only, rate of freesing normal condition. fhe mix cold down quickly during first two minutes to 29°F.; cooled down to 27°F. in 6 minutes, Temperature held as near as possible at 27°F in the experiment by turning brine off and on several times. The swell increased gradually until it reached 120 percent in 20 minutes. The maximum percent swell was 128 percent in 24 minutes at reached 27°F. Exp. ll. Tabe for time, Temp. Weight and % Swell. Started 3:82 P. Me Time Temp. Wt. 4% Swell Fime Tem. Wt. % Swell 3:28 51 3:48 27 3:84 29 5:44 27 444 128 3:85 28.2 3:45 27 5:26 28 67 48 3:46 B7.2 44 brine on 5:27 274 5:47 27 brine brine 3:28 27 6l on 64 5:48 87 46 on 118 5:39 27 3:49 26.8 brine 35:30 27 55 on 6&2 3:60 26¢ 50 100 3:31 27 3:61 26 3:32 27 52 92 5:38 26.8 5334 27 48 108 el $255 5:37 5:38 5:59 3:40 5:41 5242 --18-- Continue Fable for Exp. ll. 27 27 46-1/8 116 B7 brine 27 45-2/8 on 119 27 27.2 44 brine on 87 brine off 27 45% 120 ae 160 1401 C e hart Exp. 11 P. 18 45 lbs. batch ah Temperature mix 44% degrees Temperature brine 10 degrees. 0112 4 6 8 10 12 14 16 18 20 22 24 26 28 45 # batch Temp. Mix 44% Temp. Brine 10° p, 30°F, | 296 » | g8°F 879, 26°p 30 31 25 degree s Experiment lll. 45 pounds batch of mix Femperature of cream 44°P. Temperature of brine 5°F. Rate of freesing normal condition. When mix was put into the freezer 44° F., then brine through the freeser and whipped the cream as experiment 1 ‘and ll, the mixture cooled down in three minutes to 29°F. At 10 minutes the temperature was 26°F., the swell 86 percent. The brine was turned off at 10 minutes; the temperature gradually going up while the swell gradually continous raising to 120 percent at 17 minutes and this point is the maximum swell point. at thés point the brine turned em the temperature cooled dowm and also the swell decreased. Again brine eff temperature going up, the swell also increasing. This experiment gives as following results: ~=20<0 Expe lll. Table for Time, Temp. Weight and Percent Swell. Time Temp, Wt. Swell ime Temp. Wt. % Swell. 2244 35 5:04 25.8 51 Ore 96 2:45 294 3:05 265.8 2:46 29 2 59 5:06 26 49k 102 2:47 28.3 3:07 26 2:48 28 64 57 3:08 26.2 402 105 2:49 27.8 3:09 26.5 2:50 27.5 S7 174 S:10 26.5 48 108 2:61 27 S:ll 26.7 2:62 26 suf off 85 $:12n 286.8 48 108 2:58 26 $:13 87 2:54 26 50 100 38:14 287 47% 110 2:55 26.2 5:15 «87k 2:86 26% 47 1138 8:16 «2% OATS 110 8:57 26% 2:58 264 46 118 2:59 26.8 brine 5:00 27 45 en 122 3:01 27 3:02 26.8 48-1/85 107 3:08 tw 160} 140. 120. 10@._ 20 Chart Exp. lll. °o Tempe mix 44 F. Brine Temp. 5° F. 465 lb. Batch of mix. Pe --21-= ee Lome ei i ee | SO 29 | BT 26 25 EXPERIMENT 1V Weight of batch 50 lbs. Temperature of mix 45° F, Temperature of brine 10° F. Rate of freezing normal condition. The mix cooled down 29°F in three minutes and at ten minutes the temperature dropped to 25.5°F. Teh swell being 80 percent. The brine was turned off at ten minutes, the temperature going up and at 18 minutes the swell reached its maximum eof 124 percent. This experiment results show almost the same results of Experiment No. lll. maPS ae Expe 1V. Table for Time, Weight and swell percent. Time __Femp. Weight Swell P.M. 5:56 50 5:57 £9 5:58 28% 5:59 274 4:00 27% 69 44 4301 27 4:02 26.8 61 64 4:03 26 4:04 26 55% 80 4:06 25.5 Brine off 4:06 25.8 52 92 4:3 07 4:08 26 47% 110 4:09 26 4:30 26 45 122 4:11 4:12 26¢ 4@;brine on 124 4:13 26.3 4:14 26 47 113 4:16 26 6:16 25.8 48 108 4:17 26 4:18 25.8 50 100 160 140] 1204 100; ._-. 801 60 | 40 201 Chart Exp. 1V.-: Temp. Mix 45°F. 50 lb. Batoh Temp. Brine 10°F, rine eff on. 50 - £9 | 28 | 27 26 2a ¥ G va Jaf ty so SF 26\xf WY rine off IG 25 Experiment V. Temperature of mix 47° FP, femperature of Brine 10°F, Weight of batch 45 lbs. Freezing temperature, hold low temperature. The mix cooled down te 89° F. in two minutes, the temperature reached 26° F. in nine minutes, the swell being 80 percent and rapidly cooled dow te 25° F. Then temperature hold between from 26° ¥. te 25°F. from ten minutes to 24 minutes. The swell because of two low temperature inoreased a little. At 15 minutes the swell obtained was 88 percent. At 24 minutes the swell was still 88 percent. After 24 minutes temperature was allowed to increase about 26° F., swell going up to 103 percent. It will be noted that too low temperature could not obtained proper swell however cream beat down and the ice cream frozen poorly. Air could not be incorporated into interval in mix crean. (1) Should never do freezing at too low temperature. (2) at 256° F. 2 swell over 90 percent could not be obtained. ~-26-- Exp. Ve. Table for Time, Temp. Weight and Percent Swell. Time Temp. Bt. G8well fime Temp. Wt, % Swell 9:48 29 10:08 9:49 28% 10:09 9:50 28 " 10:10 9:51 28 70 45 10:11 9:52 28 10:12 9:55 27.5 62 61 "10:18 9:54 27 10:14 9: 55 26¢0—Ois«éG 7 77 10:16 9:56 26 10:16 9:57 26 55 82 10:17 9:58 25.8 10:18 9:59 25.5 63¢ 87 10:19 10:00 25 10:20 brine 10:01 25 54 off 86 10:21 10:02 25.5 10:22 brine 10:08 26 52 on 92 10:23 10:04 25 10:24 10:05 253 0=— «BS 89 10:25 10:06 25 10:07 285 54 85 25 25 25.3 25.8 26.8 26.8 26.8 27 27 27 27 27 27 27 27.2 21% 27.5 27.5 Brine 54.5 off 83 524 90 512 95 50 100 50 100 494 102 494 101 51 96 55 89 Chart Exp. V. ° Tempe Hix 47 Fy Temp. Brine 10 F. 45 lbe _atch. —e - os — ——=e © oo © oe @ wwe © Cee oe 8 eee ee ee ~=27 -~ Je 28 BI wl S7 Se Chart Exp. Ve or i Fempe Hix a7°r 8 - Temp. Brine 10 F. 45 lb. -atch. fe IF GI BL fy Pe | EXPERIMENT Wl. A, Be Ae Weight of Mix 60 lbs. B. Weight of mix 43 lbs. femperature of mix 45° F. Temperature brine 10°F. femperature of brine 10°P. Femperature of mix 43°F. Ae Experiment result show the mix was cooled wery rapidly down te 29°F. at one minute, in five minutes cooled down to 27°F.; at nine minutes temperature was 25.5°F. At this point the swell was 84 percent and maximum swell 124 percent at 14 minutes. B. Experiment show the mix cooled down same as A» experiment point 29°F, at one minute; in five minutes cooled down 26.5°F, and cooled down to 85.5°F. at eight minutes and held at this point continuously for three minutes. Then temperature goes up to 26°F. again while the swell gradually increased to 108 percent at 11 minutes. Both A and B. Experiments seemed samewhat quickly cooled down during first few minutes but results obtained were almost near the proper swell and these experiments show almost identical graph in both swell and temperature. Total length of freezing time showed 13 minutes was best time in these 4A and B. Experiments. Exp.e Vl--A. Table for fime, Temp. Weight and Percent Swell. ime Temp. Weight YS Swell 4:25 89 4:26 28.5 4:87 28 4:28 21k 69 44 4:29 27 4:30 26.9 61 64 6331 26 4:32 26 554 80 4:38 25.5 Brine off 4334 25.7 52 92 4:36 25.8 4:36 26 49% 102 4:87 26 4:38 26 44% 124 4:39 26.2 4:40 26¢ 45 122 4:41 26.3 4:42 26 47 113 4:43 26 4:44 25.8 46 118 £ ee 4:43 | a750-- Exp. Vl--B. Tabse for Time, Weight, Temp. and Percent Swell. Tempe Weight & swell 29 20% 28 27 68 49 26.7 26.5 59 68 86 25.5 56 brine off 118 25.5 25.5 52 92 85.5 26 48 108 26 \ | on] wo | & DEPpe —___ ° re .+Pe------ a": rere mix 45 + Lenpe “in 4B fF. a iCl'De brine 10°. yer brine 10°, - 30 $0 ibe “atuh 43 lide ¢ tush | ' ‘ * . | vhurt 'XDe Vile | _ 140 | } } | | | | 120 | | + g9 ‘\ \ ( \ / / 200 | - Of ot \ i \ 4 \ \ \ 60 4 298 \ 1) y \ / é yy 60 i\ / _ \\. \ \y x / f 40 / 1 29 if { if \ 4 jj \ £0 J | \ \ \ \ \ 26 A ~ 25 Experiment Vill. Weight of mix 50 lbs. femperature of mix 44° F. Pemperature of brine 10° PF, fhe mix entered the freezer at 44° F, and cooled down to 29.2° FP. in three minutes. The mix was whipped while in this three minutes.#Brom eight minutes to 11 minutes the Temperature drepped from 28.5" F. to 27° F. after the brize was turned eff the temperature gradually went up to 28° F., the swell droppéng as this point was above the freezing point £7.86° F. fhe swell slightly increased during the first three minutes and from six minutes to 12 minutes the swell increased from 38 percent to 118 percent. The maximum swell 132 percent was obtained at the end of 18 minutes. After this the swell decreased due to raise in temperae ture at this point, 2-SS-- Exp. Vill. Table for Time, Temp. Weight, and Percent Overrun, Time Temp. Wt. “Swell Time Temp. Wt. ell $:11 44 3:31 = - 87.6 $:12 34 5:32 28 44.5 122 5:13 29.2 84 19 5:35 28 3:14 29 5:34 £8 46 118 5:15 28.6 §:16 28.8 75 353 S:17 28.6 3:16 28.5 61 64 8:19 £7.65 $:20 27.2 52 92 $:21 87 8:22 27 46 118 5325. RT 5:24 87 45 122 3:25 87 §:26 a7 44 127 3:27 27 3:28 27.2 43m 132 3:29 87.2 5:30 27.6 43.5 130 160 q 140 120} 6Ol 601 20- Chart Exp. Vil. onSgo= Temperature of mix 44°F. 50 pound batch Brine Temperature 10° F. 6 8 /0 72 I% (6 (8 20 22 24 26 50 29 27 26 --35-— Experiment V1lll. Temperature of mix 40°F. Temperature of brine 10°F. 50 lbs. of batch. The mix was oooled rapidly, from 40° F. to 28°F. in two minutes and then after a few minutes cooled down to 26° F. in eleven minutes. At this point the swell inoreased to 100 percent. When the brine was turned on the swell began decreasing at 15 minutes and then the swell quickly decreased . At 16 minutes the temperature cooled down to 25°F. > at the same time the swell de- oreased. This experiment shows results near the proper swell and at such freezing process. Yhe ice cream should be removed from the freezer at 14 minutes or 18 minutes. In this point would be good results obtained for quality and quantity of ice cream. Expe Vl1ll. Table for Time, Temp. Weight and Percent Swall. Time Temp. Wt. Swell Time Tempe Wt. Swell 3:26 30.5 3:45 26 3:27 28.2 3:46 25.9 55.2 80 3:28 £8 3:47 25.7 3:29 27.7 76 21 3:30 27.5 $331 27-1 75 34 3:32 26.8 3:33 26.8 65 64 3: 34 26.8 3:35 26.5 50 100 33356 R26 3:37 26.2 5:38 26.2 47 113 3:39 26.5 3340 26.5 46 118 3:41 26.5 3:42 26.5 49% 102 3:43 26.5 3:44 26.1 522 90 Chart Expe Vili. Pemperature of mix 40° F. 50 lb. batoh Oo Temperature of S5rine 10 bee ome ees @ Ee oS a eee ee eee oe eee eee eee ff. cee oe comm i es Fe ——- & <== oe sump © teweese 6 ooo @ ——— » oe £6 2 4Yy G6 S Jd fe Sy Lb foe a a ~=33—— Table le Relation oi Time, Temperature and Swell. The following table showing relation tine, temperature and swell percent in five minutes, ten minutes, 15 minutes and 18 minutes during freezing process of ice cream. The average percent of swell obtained in five minutes was 50.5 percent, average temperature 27.7. The averace percent ewell obtained in ten minutes was 85 percent and average temperature in ten minutes was 26.8°F. Averace swell and Temperature in fifteen minutes were 112.8 pe cent swell and 26.4° 7. Averace swell and temperature in eirnteen minutes were 116 percent swell and 26.5" FF. temperature. Time 5 mine 10 mine 15 mime 18 mine Expe Noe SWell Tempe Swell Tempe Swell Temp. swell Temp. 1 56 28.5 78 26.5 120 27 130 27 11 60 27.5 92 27 117 -27~—s«W2122 27 111 49 28 85 26 116 26.5 116 27 1V 40 27.5 80 25.5 106 26 126 26.5 v 44 28 82 26 92 26 92 26 V1 54 27.8 92 25.5 123. 26 114 26 Average 50.5 27-7 85 26.8 112.8 26.4 116 26.5 ~-39-— Table 11. Correlation of time and temperature at 80% and 1004 swell. p When reached ‘when reached to Rate trom condition Swell to 80, swell 100% swell 80 to 1005 Swell freezing process. ExXpe Noe Time Tompe Time Temp. Time Temp. 1 10 min. 26.5°F. 12 26°F. 2 min.0.5 Lormal. 11 8 27 ll 27 3 0 n 111 10 26 12 26.2 2 +0.2 " 1V 10 25.5 13 25.8 3 40.3 " VA 8 26 12 26 4 0 " V1B. 8 25.5 1l 25.5 3 0 " Averare 9 26.1 1-5/6 26.1 2-5/6 0.00 This table shows that the average temperature (26.1°F.) remained constant during the average increase in swell from 8Onpercent to 100 peroent. The time required to increase the swell from 80 percent to 100 percent was 2-5/6 minutes. This result show the swell from 80 percent to 100 percent could obtained at same temperature about 26°F. This result corresponds with experiment 11 showing that when the ice cream within the proper range of temperature the swell can be increased without chance of temperature. ~-40-— Effectivity of "Brine off and on" to the swell and the temperature. Table lll. Sffect within five minutes after brine was off and was turned on. Effect within five minutes after brine Was Offe Exp. No. Temp. Swell 111 26°R-26.5°R. 2t0.5°R 85-118=+33 1 265-27 =*0.5 88-124 =+36 1V 2525=-26 =+0.5 80-116 —336 V1 255-26 =#0.5 87-124 =+37 Averare 0.5 35 + sign shows going up +Sign shows increase Effect within five minutes after brine was on Expe Noe Tempe % Swell 1 28°F =26.6°F w-1.4°F, 102-96 » -6 11 26-25 =-1.0 92-88 = ~4 111 26.9-25.8 =x==1.1 122-96 = ~26 iv 26.526 a ~0.5 118-84na -34 Average -1.0 -17.4 - sign shows goins down - sign shows decrvase. From above table the following correlation could obtained. Effect to temperature: Effect of swell &: Brine off equal plus 0.5 Brine off equal pus 35 Brine on " -1.0 Bgine on " - 17.4 Now if effectivity by brine off and on assumed as 10. will obtained following equation. Effect to temperature: Effect to swell jp: Brine off effectivity w 5 Brine off effectivity # 10 Brine on effectivity =» 10 Brine on effectivity = 5 i.e. The brine on has twice effectivity of brine off for temperature in freezing process. The brine on has ¢ effectivity of brine off for the swoll in freezing process. The brine off has 4 effiotivity of brine on for the temperature in freezing process. The brine off has tweice effectivity of brine on for the swell in freezing process. The swell dropped when brine was turned on because the ice cream was frozen firmer causing it to become stiff and brittle and the additional whippine caused the air which had proviously been incorporated to be beaten out. The brine on and off should be done in conformity with effectivity of brine on and off. This factor is one of important factors to keep. overrun under proper control of ice cream freezing process. ~=42—— Usually when the brine turned off and on as soon effected to temperature, but the swell had effected few minutes later than the temperature. As satisfactory in "brine effectivity " of above discreption. Usually brine off in freezing process should be done between 26.5° and 26° ¥. at 8 to 10 minutes and brine on should be turned on if the temperature is going up near the 289 F. of temperature and let the temperature cool down. Table ly. Relation of Maximum percent swell, time and temperature. The following table shows that the average maximum percent swell 123 percent, temperature at about 27 desrees and time average 20 minutes takes to maximum swell. When reached maximum peroesnt swell Exp. Noe Time Tempe jo Swell Freezing condition 1 18 27.5 130 Normal 11 " 24 2702 128 27°F, only 111 17 27 122 Normal LV 18 26.5 124 Normal V 31 27 102 Low Temp. al 14 26 126 Low Temp. _ Vlim 18 271 132 Quickly freezing Averare 20 26.9 123-1 wm Aman It is noted that with this maximum point of swell the ice oream was forzen too thorough and very porous, light and fluffy because usually total lensth of freezing shoul be done in less than 20 minutes and the percent swell should not beyond 110 percent swell. SUMMARY Proper swell could not be obtained with too high temperature or too low temperature in freezing process. BSst freezing temperature from 25.5°F.- to 27 F. The experiment V. shows that too low temperature 25°F. the swell does not incrcase. In which case the ice cream is frozen too stiff and is rather brittle so that continued beating tends to break down the air cells which have already been formed. The experiment 1 and Vll show that at high temperature of 28° F. the swell does not increase and ice cream was soft. Too slow and too rapidly freezing should be avoided. If taken such freezing process it would obstruct keeping overrun under proper control and lose quality and quantity of ice oream The mixture temperature when entered the freezer should be taken aw near 40°R. as possible. It is better the control of temperature of freezing ice cream in Breezer. The temperature of ice cream when drawn from the freezer to cans should be from 26°F to 27°F, as at this temperature the ice cream has the proper consistency. if —_—44~— the temperature is higher the ice cream will be too soft and is liable to ocrystalize out in the harding room. Best result obtained at 2695 F. mixture in the freezer. In Experiment 1V the mix did not cool down to 29° R until four minutes had elapsed. 100% swell was obtained at the end of 13 minutes. In Experiment Vl A the mix Was cooled down to 29° F in two minutes and 100 percent swell Was obtained at the end of 11 minutes. This shows that the swell is dependent upon the length of time the ice cream whips at the proper temperature. In experiment 1V the extra two minutes during which the mix was above 29°F wis lost time in the freezing process so far as swell is concerned. Therefore the colder the mix before entering the freezer or the sooner it is cooled down after entering the freezer the more time is saved in the freezing process. In Experiment Noe 111 the brine was turned off at the end of 10 minutes when the temperature had reached 26°R. At the end of 17 minutes the temperature had raised to 27°, the swell increased during this time from 85 percent to 122 percent. At this point te brine was turned on for four minutes, tne temperature dropping to 25.8°T. and the swell decreasing to 96 percent. The brine was again turned off the temperature raising to 26.8°F in ei¢eht minutes. This temperature aurve follows very closely the first raise in temperature after brine was turned off. However, the swell during this 8 minutes increased only 12,5 while during the raise in temperature after the brine was turned off the first time for seven minutes the swell had increased 37 percent. ~-45-- The same result will be noticed in examining Chart Noe 1. Also in chart No. V when the temperature was allowed to raise after 24 minutes of time the swell did not increase as rapidly as it ddd in tve normal freezinss after 10 or 12 minutes had elapsed. This leads to the conclusion that after the ice cream has whipped in the machine for a long time (20 to 30 minutes) its consistency is such that air is not incorporated as readily as it is unier some conditions earlier in the freezing process. Total length of freezing time it should be from ten to eishteen minutes. An excessive swell should be avoided. An excessive swell in ice cream is alwags obtained at the expense of quality. Best percentaze of swell is from 90% to 100% or 110%. This is an important item in sommercial ive cream making. Temperature has direct relation to swell"the temperature by brine off" has twice effectivity of brine on to tho swell and "temperature by brine on" has 3 effectivity of brine off to the swell. The temperature should be c:ntol to the swell by brine off and on. See Experiment Table Noe lle Should have viscous milk and cream and age the milk Gream or mix. Without viscosity could not ottained desirable swell. Pasteurized cream and milk should be aged urtil viscous and the cream and milk or whole mix should be homogenized or emusified. (1) (2) (3) (4) (5) (6) (7) (8) (9( (10) muh G-— BIBLIOGRAPHY Washburn, Re lie Principles and practice of ice cream making Vermont Agricultural Experiment Station, Bul. 155. 1910. Baer, Ae Ce Ice Cream Making . Arricultural Experiment Station of University of Wisconsin. 1916 Paze 10. Heineman, Paul Ge Milk 1920 Page 632 Frandesen, J» H and liarkban, EA. _The Manufacture of Ice Cream and Ices. 1915 Page 152 Washburn, Re Nie Vermont Agricultural Experiment Station Bul. 155 1910 Baer, Ae Co Bulletin No. 262. Agricultural Experiment Station, Wisconsin February, 1916 Page 9 Williams, O. He The Creamery and Iiilk Plant Monthly Ice Cream Topics April. 1921 No. 4 Page 138 Fisk, Walter WwW. The Book of Ice Cream 1919 Page 138 Washburn, Re lie Principles and Practice of Ice Cream i.a_ing Vermont Agricultural Experiment tation Bul. 155 L910 Fisk, Walter WwW. The Book of Ice Cream 1919 Page 138 (11) (12) (13) (14) (15) (16) (17) (18) --47-- Bulletin 180. Asricultural sxperinent Station, Iowa 1918 Parse 262 Sisk, walter We “he Book of Ice Cream 1919 Pesce 140 Washburn, Re lie Bulletin 155. Vermont Agricultural Experirent Station 1910 Lortensen, lie factors which Influence the Yield and vonsistency of Ice Cream. Bulletin Noe 180. Acricultural Sxperime:.t Station Iova State College of Agricultural and iiechanics Arts. 1918 Page 261 Walter We ifisk “he Book of Ice Crzam Pace 141 Washburn PR. lie Vte EXPe Ste Rule 155 Baer, Ae Co. Wis. Arr. Expe Ste Bule 262. Pave 14. IM. Mortensen, Iowas Apr. Exp. Station Bul. 180 Pave 264-268 MICHIGAN STATE UNIV. LIBRARIES UNION PON 31293006271047