CONSTRUCTION OF A HELE-SHAW COMBUSTION APPARATUS AND EXAMINATION OF LOW-FLOW NEAR-EXTINCTION REGIME USING HIGH SPEED VIDEOGRAPHY By Jeffrey Stricker A THESIS Submitted to Michigan State University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE Mechanical Engineering 2012 ABSTRACT CONSTRUCTION OF A HELE-SHAW COMBUSTION APPARATUS AND EXAMINATION OF LOW-FLOW NEAR-EXTINCTION REGIME USING HIGH SPEED VIDEOGRAPHY By Jeffrey Stricker To ensure the safety of astronauts aboard the Space Shuttle and, more recently, the International Space Station, the propagation of fire in microgravity environments must be well understood, as it would be significantly different from fires on Earth. Thus, the National Aeronautics and Space Administration (NASA) Glenn Research Center in Cleveland, Ohio studies micro-gravity flame spread through its Analysis of Thermo-diffusive and Hydrodynamic Instabilities in Near-extinction Atmospheres (ATHINA) initiative. The facility has a drop tower, which can be used to demonstrate flame propagation in free-fall, but the drop tests are expensive and limited to the two to five second duration of the free-fall. To simulate a microgravity environment without using the drop tower, thus significantly extending the test time from a few seconds to several minutes, a device called the Narrow Channel Apparatus (NCA) was developed at MSU. In the NCA a thin solid fuel is burned in a channel with a vertical height small enough to suppress buoyant effects. In essence, the NCA allows us to study microgravity flame behavior that is anticipated in space using a test apparatus on Earth under 1-g conditions. The Michigan State University department of Mechanical Engineering is currently running its third iteration of the NCA. ACKNOWLEDGEMENTS First of all, I wish to thank my advisor, Dr. Indrek Wichman, for providing me access to his extensive references on combustion and for his continued guidance on this project. I wish to thank Dr. Sandra Olson and her colleagues at the NASA Glenn Research Center for their assistance in familiarizing me with the experimental apparatus and data analysis portion of this project. I also wish to thank Dr. Fletcher Miller and his students, Karen Hung and Jacob Pepper, for their support in this experiment. Finally, I must thank my parents for the financial and moral support that they have provided me throughout my graduate school experience. iii TABLE OF CONTENTS List of Tables ................................................................................................................................. vi List of Figures ............................................................................................................................... vii Chapter 1 – Introduction ..................................................................................................................1 Chapter 2 – Literature Review .........................................................................................................3 Chapter 3 – Experimental Setup ......................................................................................................7 Overview ..................................................................................................................................... 7 Test Section................................................................................................................................. 8 Plenum Chamber Pressure Relief ............................................................................................... 9 Flow Control ............................................................................................................................... 9 Sample Ignition ......................................................................................................................... 10 Data Collection ......................................................................................................................... 10 Apparatus Photos ...................................................................................................................... 12 Chapter 4 – Procedure....................................................................................................................18 Flow Controller Setup ............................................................................................................... 18 Channel Setup ........................................................................................................................... 18 Camera Setup ............................................................................................................................ 19 Running Test ............................................................................................................................. 19 Post-Test ................................................................................................................................... 20 Data Analysis ............................................................................................................................ 20 Chapter 5 – Verification and Calibration Tests .............................................................................22 Chapter 6 – Constant Flow Velocity burn Tests ............................................................................34 Chapter 7 – Fast Ramp Down Burn Tests .....................................................................................42 Chapter 8 – Slow Ramp Down Burn Tests ....................................................................................58 Chapter 9 – Lessons Learned .........................................................................................................81 Flow System ............................................................................................................................. 81 Sample Holder .......................................................................................................................... 81 Sample Ignition ......................................................................................................................... 82 Preliminary Apparatus Photos .................................................................................................. 83 Chapter 10 – Conclusions and Future Work ..................................................................................84 Appendices.....................................................................................................................................87 iv Appendix A – Stoichiometry Analysis ..................................................................................... 88 Appendix B – Pressure Relief Calculation ............................................................................... 91 Appendix C – Test Data............................................................................................................ 92 References ....................................................................................................................................129 v LIST OF TABLES Table 1. Flow Rate Test: Time Elapsed to Displace 1 L of Water ............................................... 23 Table 2. Overview of Test Data .................................................................................................... 92 Table 3. Flame Behavior ............................................................................................................... 94 vi LIST OF FIGURES Figure 1. Full View of Apparatus ................................................................................................. 12 Figure 2. View of Plenum Chamber with Top Removed, Highlighting Distribution Pipe and Flow Guide.................................................................................................................................... 13 Figure 3. View of Test Section Fully Assembled ......................................................................... 13 Figure 4. View of Test Section with Top Window Removed....................................................... 14 Figure 5. View of Test Section with Top Plate Removed ............................................................ 14 Figure 6. Close-up View of Test Section with Sample Holder Removed .................................... 15 Figure 7. Close-up View of Sample Holder Guide Pins ............................................................... 15 Figure 8. View of Pressure Relief System .................................................................................... 16 Figure 9. Close-up View of Igniter Wire and Tensioner .............................................................. 17 Figure 10. Full View of Test Setup, Highlighting Cameras and Mirror ....................................... 17 Figure 11. Water Displacement Test Setup .................................................................................. 23 Figure 12. Hot Wire Calibration, 2011-10-24 .............................................................................. 24 Figure 13. Hot Wire Calibration, 2011-10-25 .............................................................................. 24 Figure 14. Channel Exit Flow Velocities, 2011-10-25: z = 50 mm.............................................. 25 Figure 15. Channel Exit Flow Velocities, 2011-10-25: z = 0 mm................................................ 26 Figure 16. Channel Exit Flow Velocities, 2011-10-25: z = -50 mm ............................................ 26 Figure 17. Hot Wire Calibration, 2011-11-11 .............................................................................. 27 Figure 18. Channel Interior Flow Velocities, 2011-11-11: z = 50 mm ........................................ 28 Figure 19. Channel Interior Flow Velocities, 2011-11-11: z = 0 mm .......................................... 28 Figure 20. Channel Interior Flow Velocities, 2011-11-11: z = -50 mm ....................................... 29 vii Figure 21. Channel Interior Flow Velocities, 2011-11-18: z = 80 mm ........................................ 29 Figure 22. Channel Interior Flow Velocities, 2011-11-18: z = 0 mm .......................................... 30 Figure 23. Channel Interior Flow Velocities, 2011-11-18: z = -80 mm ....................................... 30 Figure 24. Hot Wire Calibration, 2011-11-21 .............................................................................. 31 Figure 25. Channel Interior Flow Velocities, 2011-11-21: z = 80 mm ........................................ 31 Figure 26. Channel Interior Flow Velocities, 2011-11-21: z = 0 mm .......................................... 32 Figure 27. Channel Interior Flow Velocities, 2011-11-21: z = -80 mm ....................................... 32 Figure 28. Test 2012-04-18_2, 70s, Flame Front (25 cm/s) ......................................................... 35 Figure 29. Test 2012-04-18_2, 180s, Flame Front (25 cm/s) ....................................................... 36 Figure 30. Test 2012-04-18_2, Burned Sample ............................................................................ 36 Figure 31. Test 2012-04-18_3, 70s, Flame Front (25 cm/s) ......................................................... 37 Figure 32. Test 2012-04-18_3, 170s, Flame Front (25 cm/s) ....................................................... 37 Figure 33. Test 2012-04-18_3, Burned Sample ............................................................................ 38 Figure 34. Test 2012-04-18_4, 75s, Flame Front (15 cm/s) ......................................................... 38 Figure 35. Test 2012-04-18_4, 200s, Flame Front (15 cm/s) ....................................................... 39 Figure 36. Test 2012-04-18_4, Burned Sample ............................................................................ 39 Figure 37. Test 2012-04-18_5, 70s, Flame Front (15 cm/s) ......................................................... 40 Figure 38. Test 2012-04-18_5, 180s, Flame Front (15 cm/s) ....................................................... 40 Figure 39. Test 2012-04-18_5, Burned Sample ............................................................................ 41 Figure 40. Test 2012-04-19_1, 70s, Flame Front (25 cm/s) ......................................................... 44 Figure 41. Test 2012-04-19_1, 190s, Weak Flame Front (10 cm/s) ............................................. 45 Figure 42. Test 2012-04-19_1, Burned Sample ............................................................................ 45 Figure 43. Test 2012-04-19_3, 85s, Flame Front (25 cm/s) ......................................................... 46 viii Figure 44. Test 2012-04-19_3, 265s, Weak Flame Front (10 cm/s) ............................................. 46 Figure 45. Test 2012-04-19_3, Burned Sample ............................................................................ 47 Figure 46. Test 2012-04-19_4, 80s, Flame Front (25 cm/s) ......................................................... 48 Figure 47. Test 2012-04-19_4, 240s, Weak Flame Front (10 cm/s) ............................................. 48 Figure 48. Test 2012-04-19_4, Burned Sample ............................................................................ 49 Figure 49. Test 2012-04-20_1, 85s, Flame Front (25 cm/s) ......................................................... 50 Figure 50. Test 2012-04-20_1, 225s, Weak Flame Front (9 cm/s) ............................................... 50 Figure 51. Test 2012-04-20_1, Burned Sample ............................................................................ 51 Figure 52. Test 2012-04-20_3, 70s, Flame Front (25 cm/s) ......................................................... 51 Figure 53. Test 2012-04-20_3, 240s, Flamelets (9 cm/s) ............................................................. 52 Figure 54. Test 2012-04-20_3, Burned Sample ............................................................................ 52 Figure 55. Test 2012-04-20_4, 80s, Flame Front (25 cm/s) ......................................................... 53 Figure 56. Test 2012-04-20_4, 230s, Flamelets (9 cm/s) ............................................................. 53 Figure 57. Test 2012-04-20_4, Burned Sample ............................................................................ 54 Figure 58. Test 2012-04-24_1, 80s, Flame Front (25 cm/s) ......................................................... 54 Figure 59. Test 2012-04-24_1, 210s, Flamelets (5 cm/s) ............................................................. 55 Figure 60. Test 2012-04-24_1, Burned Sample ............................................................................ 55 Figure 61. Test 2012-04-19_1 (High Speed Camera), 257s (286s in standard rate video), Flamelets Extinguishing (10 cm/s) ............................................................................................... 56 Figure 62. Test 2012-04-20_1 (High Speed Camera), 230s (346s in standard rate video), Flamelets Bifurcating (9 cm/s)...................................................................................................... 56 Figure 63. Test 2012-04-20_3 (High Speed Camera), 273s (300s in standard rate video), Flamelets Extinguishing (9 cm/s) ................................................................................................. 56 Figure 64. Test 2012-04-24_1 (High Speed Camera), 57s (98s in standard rate video), Flamelets Bifurcating (17 cm/s) .................................................................................................................... 57 ix Figure 65. Test 2012-04-26_1, 100s, Flame Front (25 cm/s) ....................................................... 60 Figure 66. Test 2012-04-26_1, 140s, Flamelets (10 cm/s) ........................................................... 61 Figure 67. Test 2012-04-26_1, Burned Sample ............................................................................ 61 Figure 68. Test 2012-04-26_2, 90s, Flame Front (25 cm/s) ......................................................... 62 Figure 69. Test 2012-04-26_2, 120s, Flamelets (10 cm/s) ........................................................... 62 Figure 70. Test 2012-04-26_2, Burned Sample ............................................................................ 63 Figure 71. Test 2012-04-26_3, 185s, Flame Front (25 cm/s) ....................................................... 63 Figure 72. Test 2012-04-26_3, 215s, Flamelets (10 cm/s) ........................................................... 64 Figure 73. Test 2012-04-26_3, Burned Sample ............................................................................ 64 Figure 74. Test 2012-04-26_4, 180s, Flame Front (25 cm/s) ....................................................... 65 Figure 75. Test 2012-04-26_4, 240s, Flamelets (10 cm/s) ........................................................... 65 Figure 76. Test 2012-04-26_4, Burned Sample ............................................................................ 66 Figure 77. Test 2012-04-26_5, 100s, Flame Front (25 cm/s) ....................................................... 66 Figure 78. Test 2012-04-26_5, 160s, Flamelets (10 cm/s) ........................................................... 67 Figure 79. Test 2012-04-26_5, Burned Sample ............................................................................ 67 Figure 80. Test 2012-04-26_6, 10s, Flame Front (25 cm/s) ......................................................... 68 Figure 81. Test 2012-04-26_6, 70s, Flamelets (10 cm/s) ............................................................. 68 Figure 82. Test 2012-04-26_6, Burned Sample ............................................................................ 69 Figure 83. Test 2012-04-26_7, 90s, Flame Front (25 cm/s) ......................................................... 69 Figure 84. Test 2012-04-26_7, 150s, Flamelets (10 cm/s) ........................................................... 70 Figure 85. Test 2012-04-26_7, Burned Sample ............................................................................ 70 Figure 86. Test 2012-04-27_1, 90s, Flame Front (25 cm/s) ......................................................... 71 Figure 87. Test 2012-04-27_1, 240s, Flamelets (10 cm/s) ........................................................... 71 x Figure 88. Test 2012-04-27_1, Burned Sample ............................................................................ 72 Figure 89. Test 2012-04-27_2, 90s, Flame Front (25 cm/s) ......................................................... 72 Figure 90. Test 2012-04-27_2, 240s, Flame Front (10 cm/s) ....................................................... 73 Figure 91. Test 2012-04-27_2, Burned Sample ............................................................................ 73 Figure 92. Test 2012-04-27_3, 80s, Flame Front (20 cm/s) ......................................................... 74 Figure 93. Test 2012-04-27_3, 180s, Flamelets (10 cm/s) ........................................................... 75 Figure 94. Test 2012-04-27_3, Burned Sample ............................................................................ 75 Figure 95. Test 2012-04-27_4, 80s, Flame Front (20 cm/s) ......................................................... 76 Figure 96. Test 2012-04-27_4, 180s, Flamelets (10 cm/s) ........................................................... 76 Figure 97. Test 2012-04-27_4, Burned Sample ............................................................................ 77 Figure 98. Test 2012-04-27_5, 80s, Flame Front (20 cm/s) ......................................................... 77 Figure 99. Test 2012-04-27_5, 180s, Flamelets (10 cm/s) ........................................................... 78 Figure 100. Test 2012-04-27_5, Burned Sample .......................................................................... 78 Figure 101. Test 2012-04-26_1 (High Speed Camera), 90s (141s in standard rate video), Flamelet Extinguishing (9 cm/s) ................................................................................................... 79 Figure 102. Test 2012-04-26_6 (High Speed Camera), 125s (83s in standard rate video), Flamelets Bifurcating (6.75 cm/s)................................................................................................. 79 Figure 103. Test 2012-04-27_2 (High Speed Camera), 117s (164s in standard rate video), Flamelets Bifurcating (17.6 cm/s)................................................................................................. 79 Figure 104. Test 2012-04-27_4 (High Speed Camera), 234s (257s in standard rate video), Flamelets Extinguishing (2.3 cm/s) .............................................................................................. 80 Figure 105. View of Plenum Chamber with Top Removed, Highlighting Old Seal Design........ 83 Figure 106. View of Test Section with Top Plate Removed, Highlighting Old Igniter Design ... 83 Figure 107. Steady State Flame Spread Rate vs. Oxidizer Flow Velocity for All Tests .............. 95 Figure 108. Steady State Flame Spread Rate Relative to Oxidizer Flow Velocity vs. Oxidizer Flow Velocity for All Tests .......................................................................................................... 96 xi Figure 109. Test 2012-04-09_1 Track .......................................................................................... 97 Figure 110. Test 2012-04-09_2 Track .......................................................................................... 97 Figure 111. Test 2012-04-18_2 Track .......................................................................................... 98 Figure 112. Test 2012-04-18_3 Track .......................................................................................... 98 Figure 113. Test 2012-04-18_4 Track .......................................................................................... 99 Figure 114. Test 2012-04-18_5 Track .......................................................................................... 99 Figure 115. Test 2012-04-19_1 Overall Track ........................................................................... 100 Figure 116. Test 2012-04-19_1 Initial Track.............................................................................. 100 Figure 117. Test 2012-04-19_1 Final Track ............................................................................... 101 Figure 118. Test 2012-04-19_3 Overall Track ........................................................................... 101 Figure 119. Test 2012-04-19_3 Initial Track.............................................................................. 102 Figure 120. Test 2012-04-19_3 Final Track ............................................................................... 102 Figure 121. Test 2012-04-19_4 Overall Track ........................................................................... 103 Figure 122. Test 2012-04-19_4 Initial Track.............................................................................. 103 Figure 123. Test 2012-04-19_4 Final Track ............................................................................... 104 Figure 124. Test 2012-04-20_1 Overall Track ........................................................................... 104 Figure 125. Test 2012-04-20_1 Initial Track.............................................................................. 105 Figure 126. Test 2012-04-20_1 Final Track ............................................................................... 105 Figure 127. Test 2012-04-20_3 Overall Track ........................................................................... 106 Figure 128. Test 2012-04-20_3 Initial Track.............................................................................. 106 Figure 129. Test 2012-04-20_3 Final Track ............................................................................... 107 Figure 130. Test 2012-04-20_4 Overall Track ........................................................................... 107 Figure 131. Test 2012-04-20_4 Initial Track.............................................................................. 108 xii Figure 132. Test 2012-04-20_4 Final Track ............................................................................... 108 Figure 133. Test 2012-04-24_1 Overall Track ........................................................................... 109 Figure 134. Test 2012-04-24_1 Initial Track.............................................................................. 109 Figure 135. Test 2012-04-24_1 Transient Track ........................................................................ 110 Figure 136. Test 2012-04-24_1 Final Track ............................................................................... 110 Figure 137. Test 2012-04-26_1 Overall Track ........................................................................... 111 Figure 138. Test 2012-04-26_1 Initial Track.............................................................................. 111 Figure 139. Test 2012-04-26_1 Transient Track ........................................................................ 112 Figure 140. Test 2012-04-26_2 Overall Track ........................................................................... 112 Figure 141. Test 2012-04-26_2 Initial Track.............................................................................. 113 Figure 142. Test 2012-04-26_2 Transient Track ........................................................................ 113 Figure 143. Test 2012-04-26_3 Overall Track ........................................................................... 114 Figure 144. Test 2012-04-26_3 Initial Track.............................................................................. 114 Figure 145. Test 2012-04-26_3 Transient Track ........................................................................ 115 Figure 146. Test 2012-04-26_4 Overall Track ........................................................................... 115 Figure 147. Test 2012-04-26_4 Initial Track.............................................................................. 116 Figure 148. Test 2012-04-26_4 Transient Track ........................................................................ 116 Figure 149. Test 2012-04-26_5 Overall Track ........................................................................... 117 Figure 150. Test 2012-04-26_5 Initial Track.............................................................................. 117 Figure 151. Test 2012-04-26_5 Transient Track ........................................................................ 118 Figure 152. Test 2012-04-26_6 Overall Track ........................................................................... 118 Figure 153. Test 2012-04-26_6 Initial Track.............................................................................. 119 Figure 154. Test 2012-04-26_6 Transient Track ........................................................................ 119 xiii Figure 155. Test 2012-04-26_7 Overall Track ........................................................................... 120 Figure 156. Test 2012-04-26_7 Initial Track.............................................................................. 120 Figure 157. Test 2012-04-26_7 Transient Track ........................................................................ 121 Figure 158. Test 2012-04-27_1 Overall Track ........................................................................... 121 Figure 159. Test 2012-04-27_1 Initial Track.............................................................................. 122 Figure 160. Test 2012-04-27_1 Transient Track ........................................................................ 122 Figure 161. Test 2012-04-27_2 Overall Track ........................................................................... 123 Figure 162. Test 2012-04-27_2 Initial Track.............................................................................. 123 Figure 163. Test 2012-04-27_2 Transient Track ........................................................................ 124 Figure 164. Test 2012-04-27_3 Overall Track ........................................................................... 124 Figure 165. Test 2012-04-27_3 Initial Track.............................................................................. 125 Figure 166. Test 2012-04-27_3 Transient Track ........................................................................ 125 Figure 167. Test 2012-04-27_4 Overall Track ........................................................................... 126 Figure 168. Test 2012-04-27_4 Initial Track.............................................................................. 126 Figure 169. Test 2012-04-27_4 Transient Track ........................................................................ 127 Figure 170. Test 2012-04-27_5 Overall Track ........................................................................... 127 Figure 171. Test 2012-04-27_5 Initial Track.............................................................................. 128 Figure 172. Test 2012-04-27_5 Transient Track ........................................................................ 128 xiv CHAPTER 1 – INTRODUCTION Combustion is a vital part of our everyday lives. While much of the current research in combustion involves improving the efficiency of our electric power generation, heating, transportation, and other such processes, it is equally important to study the detrimental aspects of combustion, such as pollutant formation and damage caused by uncontrolled fires, in order to improve the safety of our structures and vehicles. Combustion is a complex process involving several research disciplines, including chemistry, fluid mechanics, and thermodynamics, and all of its details are not yet fully understood. To ensure the safety of astronauts aboard the Space Shuttle and, more recently, the International Space Station, the Micro-gravity Science Division (MSD) team at the National Aeronautical and Space Administration (NASA) Glenn Research Center in Cleveland, Ohio studies micro-gravity flame spread through its Analysis of Thermodiffusive and Hydrodynamic Instabilities in Near-extinction Atmospheres (ATHINA) program. This initiative is necessary because combustion in micro-gravity environments is different from that on Earth due to the lack of buoyant effects, whereby flames tend to propagate upwards as a result of hotter gases rising above cooler gases due to gravity. Currently, NASA tests flammability of non-metallic solids using NASA-STD-(I)-6001A Test 1, but since this test consists of an upward flame spread in normal gravity, it is not representative of a fire occurring in microgravity conditions. The most ideal way to study micro-gravity combustion would be to actually conduct combustion tests in space, but while this will be done on a limited basis, it is very expensive and subject to scheduling constraints. To replicate a micro-gravity environment on Earth, the NASA facility has 2.2 and 5 second duration drop towers, which can be used to demonstrate flame 1 propagation in free-fall, but these tests are also expensive and are limited to the 2.2 and 5 second duration of the free-fall. Additionally, burn tests can and have been conducted aboard conventional aircraft flying parabolic trajectories, which provides about half a minute of microgravity testing conditions, but are also subject to substantial expense, scheduling constraints, and relatively high “g-jitter” (fluctuations in acceleration, particularly on the aircraft in parabolic flight but also to a lesser extent in the drop tower and aboard the space shuttle). To simulate a microgravity environment inexpensively and conveniently, an apparatus was developed in which a solid fuel could be burned in a channel with a vertical height small enough to suppress buoyant effects but not so small as to suppress the flame through heat loss to the chamber walls. Versions of this apparatus are being studied at NASA’s Glenn Research Center at Lewis Field (which subsequently shall be called NASA-Lewis), San Diego State University (SDSU), and at Michigan State University (MSU). Each team’s experimental apparatus is slightly different and is intended for different purposes. MSU’s Narrow Channel Apparatus (NCA) has evolved through three iterations. Details of the differences among these appear in the Literature Review and Experimental Setup sections. 2 CHAPTER 2 – LITERATURE REVIEW This project continues the previous experimental research done at Michigan State University by Oravecz [1] and Tanaya [2]. Prior to the research at MSU, theoretical analyses of thin solid fuel combustion were conducted by deRis [3] and Fernandez-Pello and Williams [4, 5]. Additionally, works by Wichman and Williams [6, 7] present a simplified model, based on the results of deRis, that applies to solid fuel flame propagation with an opposed oxidizer flow. Experimental research on diffusion flame spread over thermally thin solid fuels with opposed oxidizer flow in microgravity has been performed by Olson et al. at NASA-Lewis [8, 9, 10]. The results show that, as expected, at high flow velocities extinction occurs due to convective heat loss, but contrary to deRis’s model, at low velocities quenching occurs due to radiation and other heat loss. In the latter situation, the assumption by deRis of infinitely fast chemical kinetics becomes invalid. These results were not apparent until conducting simulated microgravity tests because achieving sufficiently low flow velocities in normal gravity is difficult due to buoyant effects, which tends to entrain oxidizer at speeds up to 30 cm/s near the flame front. Of interest in this project is combustion in this near-extinction limit of low oxidizer flow, where the flame front dissociates into narrow, finger-shaped flamelets. The studies by Zik et al. [11] show that the spacing between these “fingers” (flamelet paths) is determined by the Péclet number, which is the ratio of advection to diffusion, and that the width of the fingers is determined by heat loss. The research conducted by Oravecz consisted of the development of a narrow channel combustion chamber, also known as a Hele-Shaw apparatus, based on the preceding work and others [1]. Oravecz designed the MSU Flame Rig based on research that showed that buoyant 3 effects would be suppressed if the gap spacing, or the vertical height in the combustion chamber between the plates, is below a certain critical value. This critical value occurs where the Raleigh number, which is representative of the ratio of convective to conductive heat transfer, is no greater than 1708. Oravecz’s experiments showed that a Hele-Shaw apparatus can be an acceptable supplement to existing methods of studying microgravity flame spread, as indicated by the similarity of flame instabilities in the MSU Rig and the NASA Drop Tower tests. At sufficiently low oxidizer flow velocities, flames would disintegrate into flamelets that oscillated on the order of 1 Hz and spread slower than the flame front. They always propagated in the direction opposing oxidizer flow and would generally converge or auto-extinguish. Most importantly, these flamelets survived in flow velocities found on the Space Shuttle and International Space Station, indicating that such a fire could propagate in those environments. The discussion section in [1] includes a reminder that the Hele-Shaw apparatus is not a true zerogravity environment but rather just simulates one by suppressing buoyant flow, and it has the additional disadvantages of a large heat sink near the burning sample and a channel geometry that produces a viscous-dominated flow. However, it offers versatility that the true microgravity testing methods do not, specifically a long testing time, easy interchangeability of test samples, optical access, and variation of test geometry. The research conducted by Tanaya [2] continues the work of Oravecz. These tests utilized a new apparatus, called the Simulated Microgravity Flamelet Tunnel (SMFT). It had the same plenum and contraction chambers as the previous MSU Flame Rig but a different, although functionally similar, test section. Rather than standing on legs, it had a rolling cart to which it was mounted along its center axis (the axis in line with the flow) at each end, so that it could be rotated about that axis. By rotating the apparatus to the inverted (upside-down) position and 4 observing that the flame behavior is the same, it could be inferred that buoyant effects are in fact largely (but not totally) suppressed. Like the MSU Flame Rig, the SMFT test section contains a copper heat sink on one surface and a glass window for viewing on the other. The Flame Rig utilized shims to maintain gap spacing; to allow for rotating to the inverted position, the SMFT used bolts that secured to threaded holes in the sample holder, wall plate, aluminum base plate. The ignition system consisted of a straight wire across the sample mounted to tensioning clips at each end, unlike the old rig which initially used a rigid wire that was formed into many sinusoidal curves to ensure complete contact (later versions utilized the wire-tensioning concept). The SMFT had a stand secured to its top plate for mounting the camera and blocking excess ambient light. Tests conducted in the SMFT involved observing the flame breakup and convergence under linearly decreasing and increasing opposed flow velocities, respectively, which the paper called “ramping” flow. Test results indicated that flame stability in the opposed flow setup is strongly dependent on oxidizer flow rate and gap height; this is consistent with the previous tests. The ramp down tests showed that the number of flamelets formed is initially dependent on the flow deceleration rate but, after about 20 seconds, loses that dependency while also being bounded within a consistent range. The ramp up tests showed that the flamelets propagate slower than the flame front, but the ratio of flame spread velocity to oxidizer flow velocity is higher for the flamelets than the flame front, since the oxidizer flow is slower in the flamelet regime. For a steady flow test condition, the flame spread rate is nearly linearly proportional to the oxidizer flow velocity in the near-extinction (low flow) regime, then remains approximately constant and eventually decreases with increasing flow velocity. 5 Following Tanaya, Aditjandra [12] conducted numerous experiments using the SMFT. These tests focused on analyzing the number of flamelets formed and proportion of the sample burned in the low-flow near-extinction limit. Most were conducted in both the normal and inverted positions, which resulted in slight but statistically significant differences. The flamelet population tests showed that about half of the flamelets must be productive (that is, split into additional flamelets) in order to sustain the flamelet propagation (that is, for the rate of flamelet propagation to equal or exceed the rate of flamelet extinction). The rate of flamelet formation was slightly greater in the normal position than inverted and increased with increasing oxidizer flow. The study of burned area showed that about 40% to 70% of the fuel sample was consumed on average in the normal position versus 20% to 50% for the inverted position. Many of Aditjandra’s results [12] were summarized in a detailed article by Olson et al. [13]. Concurrently with the MSU NCA project are two projects at SDSU. A narrow channel similar to but smaller than the one at MSU is being used to test the effect of air pressure on the flame spread rate [14]. This setup utilizes bottled oxygen and nitrogen, along with a mass flow controller for each, to test different normoxic conditions (that is, varying the total air pressure and oxygen concentration while keeping the partial pressure of oxygen in the mixture constant), which mimics the conditions found on spacecraft. Another channel is being used to test an alternative fuel, trioxane (C3H6O3) [14]. Trioxane is physically thick but behaves as a thermally thin fuel because only a thin layer burns off the top surface of the fuel in each test. This fuel has the notable advantage that a single sample can be burned up to thirty times with no change in its behavior. 6 CHAPTER 3 – EXPERIMENTAL SETUP OVERVIEW The new setup discussed in this thesis is known as the Michigan State University Narrow Channel Apparatus (MSU NCA), to parallel the setup currently being studied at San Diego State University (SDSU), called the SDSU NCA. (SDSU actually has two narrow channels: one that resembles the NASA and MSU NCA’s, and another that utilizes a moving op wall to produce an opposed flow with a linear velocity gradient.) The MSU NCA employs the rolling stand and rotating shaft of its predecessor but has a new, wider channel mounted to it, as well as a greatly streamlined inlet plenum and a shorter outlet plenum section. See Figure 1 for a full view of the apparatus. The system consists of a ¼” inner diameter hose originating at the shop air supply (140 psi static pressure) and passing through a brass pressure regulator (reducing the air supply to 60 psi), a rotameter (to verify the flow rate), and Y-junction (to divide the flow evenly among two tubes), after which the tubes are fed into opposite ends of a distribution pipe in the plenum. The distribution pipe releases air toward the back of the plenum chamber, which reflects the airflow forward, effectively pressurizing the entire plenum chamber and driving a uniform flow out its exit. Just upstream of the plenum exit, the air passes through a plastic honeycomb, which has a 5 to 1 aspect ratio, and a fine metal screen, the combination of which should eliminate most turbulence and other flow nonuniformities associated with this setup. See Figure 2 for a view of the hardware in the plenum chamber. The air then traverses the test section where combustion of the sample is occurring and is finally released into the atmosphere through a converging exit chamber. 7 TEST SECTION An entirely new channel has been constructed for this experiment. Unlike its predecessor’s, the new test section now has quartz glass windows on both the top and bottom plates instead of a copper heatsink on the bottom plate, which allows simultaneous viewing from both directions (eliminating the need to rotate the channel to the inverted position to view the combustion from below) and ensures symmetrical heat loss. As mentioned in the overview, the test section is also wider than its predecessor’s in order to accommodate a larger sample, which can yield more flamelets. The new test section also has side windows for verifying vertical symmetry. The top window is now removable from the top plate for fast and easy sample reloading, identical to the NASA NCA. See Figure 3 for a view of the new test section and Figure 4 for the same view with the top window removed. Gap spacing is maintained using 1 mm thick shims (as in the original MSU Flame Rig) rather than threaded bolts (as in the SMFT) because the sample holder, which is made of 0.032inch (0.8 mm) thick stainless steel, is somewhat flexible, and so it takes many supports to keep it rigid. Shims are stacked in ten different places from the floor of the test section to the sample holder and then eight places from the sample holder to the ceiling. See Figure 5 for a view of the shims above the sample holder and Figure 6 for a view of the shims below it. The extra pair of shim locations below the sample holder accommodates pins that secure the sample holder in place when the top plate is removed, a detail of which is shown in Figure 7. Additional shims can be placed if the sample holder sags between supports. The channel plates are clamped to each other in two places along each side and secured by two bolts at each end, ensuring that neither plate deforms in the middle of the test section, which would cause a variation in the gap spacing. The apparatus overview in Figure 1 shows these clamps. 8 PLENUM CHAMBER PRESSURE RELIEF Unlike previous iterations of the narrow channel apparatus, the plenum chamber employs a U-tube manometer pressure relief system designed to prevent the static pressure in the test section from breaking the quartz windows. A detail of this setup can be seen in Figure 8. Dr. Fletcher Miller at San Diego State University, the Principal Investigator on this project, provided the P= formula for the maximum allowable pressure differential on the window M ⋅ T 2 (x2 − y2 ) , where M is the modulus of rupture (M = 7000 psi for quartz glass), T is x2 y2F the plate thickness (T = ¼ inch), x is the unsupported length (x = 17 inches), y is the unsupported width (y = 10 inches), and F is the desired factor of safety (F = 5). The result per these parameters was P = 1.178 psi, which corresponds to a 32.6-inch water column. There is additional safety in the fact that the pressure relief is in the plenum chamber, which is upstream and therefore at a higher static pressure than the test section. The appropriate height of the water column is marked on a ruler affixed to the manometer; the container should be checked and refilled periodically due to water evaporation. FLOW CONTROL The flow is metered by an Alicat model MC-100SLPM-D/5M flow controller with a 100 L/min capacity, which is controlled by a PC running an Igor Pro experiment written by Mr. Jacob Pepper at San Diego State University. The program calculates the necessary flow rate based on the desired flow velocity and channel geometry. It can also control separate oxygen and nitrogen flows to maintain a desired oxygen concentration. We cannot use this functionality since we are using shop air and only one mass flow controller. A portable hygrometer indicated that, with lab ambient conditions of 75.6oF and 70% relative humidity, the shop air was 74.9oF and 13.8% RH, which is dry enough that we do not require a dehumidifier or bottled air. 9 SAMPLE IGNITION Like its predecessor, the NCA igniter is a straight wire strung between two spring-loaded clips that maintain the wire tension as it stretches due to the temperature increase, and the sample is placed on top of the wire such that it is heated from below. See Figure 9 for a close-up view of the igniter wire and tensioner. The wire is 0.0071-inch-diameter (33-gauge) Kanthal A-1, whose resistance is 16.88 ohms/foot, so the 17-inch (1.42-foot) length of wire has a total resistance of 23.97 ohms. Current is supplied to the igniter wire by a Variac type W50M analog voltage controller with a 115 volt, 50-60 Hz AC input and 0 to 135 volt (RMS), 50-60 Hz AC output, up to 40 amperes. The sample ignites evenly when the voltage controller is set to 30 V, which corresponds to a current of about 1.25 A (which has been verified by a multimeter in series with the igniter circuit) and a power dissipation of about 37.6 W through the igniter wire. See Figure 9 for a close-up of the igniter wire and tensioner. DATA COLLECTION The camera mount has been retained from the SMFT to accommodate a lightweight, consumer-grade digital camcorder (recording approximately 30 frames per second) viewing the combustion from above. Additionally, a high-speed (200 frame per second) Basler camera views the combustion from below, in order to capture details of the flamelet dissociation process that are not detectable by standard rate video. Because of the high-speed camera lens’s long focal length, it must be placed far from the apparatus in order to view the entire sample, so a mirror has been placed at a 45-degree angle to the sample under the apparatus to reflect the image of the sample horizontally without any distortion (provided that the camera is perfectly level). The camera is positioned a suitable distance from the mirror to capture the image of the entire sample without much additional space around it (the tip of the camera lens positioned 23 inches from the edge of the sample cart has been found to be ideal), and at a suitable height to capture the entire 10 sample with the camera level (the tripod, with legs and neck fully extended, positioned 2 inches above the floor has been found to be ideal). See Figure 10 for camera position and mirror setup. Video recordings of the burn tests are objectively analyzed using NASA’s open-source Spotlight software, which can determine the flame propagation speed by tracking a specific point along the flame front. Previously the flame speed was estimated manually, but we are now employing Spotlight as suggested in Tanaya’s “Conclusions and Suggestions for Future Work” section [2] in order to increase the accuracy of our data. 11 APPARATUS PHOTOS Figure 1. Full View of Apparatus For interpretation of the references to color in this and all other figures, the reader is referred to the electronic version of this thesis. 12 Figure 2. View of Plenum Chamber with Top Removed, Highlighting Distribution Pipe and Flow Guide Figure 3. View of Test Section Fully Assembled 13 Figure 4. View of Test Section with Top Window Removed Figure 5. View of Test Section with Top Plate Removed 14 Figure 6. Close-up View of Test Section with Sample Holder Removed Figure 7. Close-up View of Sample Holder Guide Pins 15 Figure 8. View of Pressure Relief System 16 Figure 9. Close-up View of Igniter Wire and Tensioner Figure 10. Full View of Test Setup, Highlighting Cameras and Mirror 17 CHAPTER 4 – PROCEDURE FLOW CONTROLLER SETUP 1. Make sure air supply lines are connected (from shop air supply to pressure regulator to Alicat Mass Flow Controller). Turn on shop air supply valve (in fume hood). 2. Plug in the Alicat Mass Flow Controller and start up the PC to which it is connected. 3. Load the appropriate program into IGOR (located in the WaveMetrics folder in “My Documents”). CHANNEL SETUP 1. Verify that gap spacing is as desired (each shim is 1 mm thick, and sample holder can be approximated as zero thickness) and that test section bolts are tightened (such that there is no sagging of the top or bottom plates). 2. Remove top window and place rubber support shims. Each of these shims is also 1 mm thick, so there should be the same number of rubber shims as metal shims below the sample. Position the rubber shims using a paper clip or other tool in order to prevent fingerprints on bottom window. 3. Load sample (half sheet of 46 cm x 57 cm Whatman-44 filter paper) by placing it on top of the sample holder and igniter wire, sliding its edges under the paper clips that are attached to the sample holder. View through side windows to ensure sample is level and making even contact with the igniter. 4. Dry sample by running a high air flow rate (at least 80 SLPM) through loaded channel for at least 5 minutes. 18 CAMERA SETUP 1. Assemble high-speed camera, connect it to Ethernet port of PC, and start up PC. 2. Insert USB key and load StreamPix Single Camera program, then load “Basler Pylon GigE cameras” module (under “Camera” tab). 3. Position high-speed camera on floor facing mirror such that camera body is perfectly level (to prevent distortion of the reflected image) and image of sample is fully visible and occupies nearly the entire camera view (to minimize wasted space). This generally occurs when tip of lens is about 23 inches from edge of apparatus cart, and camera tripod (with legs and neck fully extended) is mounted approximately 2 inches above the floor. The ½-inch thick PMMA samples can be used as shims to place the tripod. Ensure aperture is set to fully open position (f-1.4), and adjust focus until rubber shims under the sample are clear. (Focusing the camera is easiest after the sample is loaded, as the sample blocks the view of background clutter.) 4. Place camera mount on top of test section with open side facing the channel exit. 5. Position consumer digital camcorder on top of camera mount such that lens is facing downward through viewing hole and igniter wire is at right edge of view (to match orientation of high-speed camera). Ensure sample is fully visible and level relative to edges of camera view. Focus camera manually if necessary. RUNNING TEST 1. Plug in LED lights in camera mount. 2. Set desired parameters in IGOR flow control program, start the flow, and wait for mass flow controller to stabilize at set point. 3. Begin video recording on both cameras. (For high-speed camera, create new sequence file in StreamPix before recording.) 19 4. Turn on power strip that feeds the igniter wire power supply, check its setting (with Kanthal A-1 33-gauge igniter wire, 30 volts RMS is appropriate), and turn on igniter wire switch (on desk next to multimeter). Multimeter can be used to verify current through igniter wire (1.25 amperes AC is appropriate). Check that igniter wire glows and sample ignites, then turn off igniter. 5. When sample autoextinguishes, stop the air flow in IGOR and turn on lights, then stop the video recordings. Ensure that both cameras have captured clear footage of the burned sample before stopping. (The spotlight connected to the igniter’s power strip can be used to illuminate sample if overhead lights are insufficient.) POST-TEST 1. Remove top window and discard sample fragments. The camera mount has Velcroattached removable curtains so that the clean-up and sample replacement process can be completed with the camera mount in place. 2. Remove rubber support shims, and then clean interior faces of both windows using glass cleaner and paper towels. DATA ANALYSIS 1. Collect the video footage of the combustion tests and convert to a usable format if necessary. (If analyzing high-speed video sequence captured by StreamPix, exporting to .avi using Cinepak Codec by Radius encodes fairly quickly, is a reasonable size and quality, and is readable by Spotlight 8 and Windows Media Player.) 2. Open video in Spotlight 8 and track using “Local Maximum Tracking”, with Area of Interest (AOI) centered on brightest area of light. Tracking in 0.1 to 0.5-second intervals is reasonable, depending on whether the combustion is in the flamelet or flame front 20 regime. Watch the tracking process to ensure AOI does not veer away from desired combustion area. (If this occurs, manual tracking may be used.) 3. Find tracking results file and import its data into Excel. Using an image editor (such as Microsoft Paint), determine the width (in pixels) of the viewable sample area, which is known to equal 43 cm. Based on that relationship, calculate each x-position from the tracking table in centimeters and determine the flame velocity between each reading, then calculate the overall flame spread rate for the test using the average of the individual velocities. 4. Save screenshots from the burn test footage as desired. 21 CHAPTER 5 – VERIFICATION AND CALIBRATION TESTS The system was checked for leaks by applying a soap bubble solution to the joints and seams of the apparatus between the mass flow controller and test section, which verifies by conservation of mass that the set flow rate is the same as the flow rate at the sample. When air was flowed through the channel, any leaks should have become visible by the escaping air creating bubbles in the applied solution. None were found. The height of the test section was measured. For a nominal gap height of 8 mm (4 shims above sample holder and 4 below it), the actual gap height was found to be 7 mm at the channel entrance, 8 mm at the sample, and 6 mm at the channel exit. The IGOR flow program should therefore be set to the nominal gap height since that is the height that corresponds to the sample location. Next, the flow rate of the mass flow controller was verified by running a water displacement test, as depicted in Figure 11. Flow originated from the clear plastic tube that ended at the throat of the soda bottle. As air floated up to the base of the soda bottle shown in the diagram, it displaced water from the bottle at a rate equal to the air flow rate. For this test, a beaker was used because the body of the soda bottle was too flexible. A stopwatch was used to time the displacement of 1 L of water. The flow rates were verified at 5 L/min and 10 L/min within the uncertainty associated with starting and stopping the timer. While higher flow rates will be used in the burn tests, they would cause the beaker to empty too quickly to be accurately timed, but since the mass flow controller is new and was calibrated at the factory, we can assume that it is accurate throughout its entire range. The complete data from this test are presented in Table 1. 22 Figure 11. Water Displacement Test Setup Set Flow Actual Flow Test # Rate (L/min) Time (s) Rate (L/min) 1 5 11.5 5.2 2 5 10.2 5.9 3 5 10.8 5.6 4 10 4.9 12.2 5 10 5.8 10.3 6 10 5.3 11.3 Table 1. Flow Rate Test: Time Elapsed to Displace 1 L of Water The preceding tests demonstrate that the total flow rate through the test section is as expected but not necessarily that the velocity profile is a fully developed parabola, as desired. A constant temperature hot wire anemometer was used to check the flow velocity profile at various average velocities, with probes placed at various points along the width (z axis) and height (y axis) of the channel. The hot wires were first calibrated using a known flow rate through a calibrator with a nozzle exit designed such that the velocity profile is uniform. The highest average flow velocity measured was 50 cm/s, for which the peak flow velocity would be 75 cm/s (1.5 times the average velocity for a parabolic velocity profile). Thus the peak Reynolds number is Re = V *D ν = (0.75m / s ) * (0.0172m) = 822 , which is well within the limit for laminar flow. 15.68 * 10 − 6 m 2 / s See Figure 12 and Figure 13 for the calibration curves from October 24 and 25, 2011, respectively. The raw data are in separate Excel files (not reproduced in this paper). 23 Figure 12. Hot Wire Calibration, 2011-10-24 Figure 13. Hot Wire Calibration, 2011-10-25 Note that while technically the voltage is dependent on the flow velocity, the axes are reversed on the calibration because we need a formula to calculate velocity as a function of voltage. For these two calibrations, the zero point and curve shapes are somewhat different, but 24 both fit strongly to second-order polynomials (R2 > 0.99). When the flow was tested, the second calibration curve was used since the tests were conducted on the same day as the calibration. The flow was tested at the channel exit in three locations across since the probe could be placed there easily, but the resulting data seemed unreliable, possibly due to interference from room air currents. Still, the calculated velocities from the channel exit flow tests are presented below. See Figure 14, Figure 15, and Figure 16 for data at the three z-axis positions. The raw data are in separate Excel files. Figure 14. Channel Exit Flow Velocities, 2011-10-25: z = 50 mm 25 Figure 15. Channel Exit Flow Velocities, 2011-10-25: z = 0 mm Figure 16. Channel Exit Flow Velocities, 2011-10-25: z = -50 mm These results are not as expected. The curves should be parabolic with maxima in the center (at y = 3 mm) and minima at the edges (y = 1 mm and 5 mm), which they are not. During tests at zero flow, the voltages were fluctuating significantly, and in some flow tests, the voltage 26 fell below the calibrated zero point, which suggests the data are unreliable. (In situations where the voltage was below the zero point, the calculated velocity was taken to be zero.) The hot wire failed unexpectedly, so another one was calibrated on November 11, 2011. Its results are below. Figure 17. Hot Wire Calibration, 2011-11-11 This calibration is not strongly parabolic because the voltages were different for a given flow velocity on the ramp-down test than for the ramp-up test. Still, this calibration curve was used because it was fairly similar to the others. This time the flow was tested above the sample holder (in the top half of the test section) just upstream of the cutout for the sample. The tests from November 18 onward were conducted at 80 mm left and right of center instead of 50 in order to measure closer to the edge of the sample. Results from flow tests on November 11 and 18, 2011, are presented below. 27 Figure 18. Channel Interior Flow Velocities, 2011-11-11: z = 50 mm Figure 19. Channel Interior Flow Velocities, 2011-11-11: z = 0 mm 28 Figure 20. Channel Interior Flow Velocities, 2011-11-11: z = -50 mm Figure 21. Channel Interior Flow Velocities, 2011-11-18: z = 80 mm 29 Figure 22. Channel Interior Flow Velocities, 2011-11-18: z = 0 mm Figure 23. Channel Interior Flow Velocities, 2011-11-18: z = -80 mm These results are also not as expected. The results on November 18 are considerably different from those of November 11 even though the configuration was the same. The hot wire was recalibrated on November 21, 2011. Its results are below. 30 Figure 24. Hot Wire Calibration, 2011-11-21 This calibration is much closer to expectations, so flow testing was then performed. One more data point in the vertical (y) direction was incorporated in this test. The results are below. Figure 25. Channel Interior Flow Velocities, 2011-11-21: z = 80 mm 31 Figure 26. Channel Interior Flow Velocities, 2011-11-21: z = 0 mm Figure 27. Channel Interior Flow Velocities, 2011-11-21: z = -80 mm These results are again not as expected. During this test (after the reading at z = 80 mm, y = 2.5 mm, and V = 50 cm/s), the probe failed. The next (and last remaining) probe was broken during calibration. 32 Unfortunately, the hot wire tests have not yielded useful data. All of these tests were conducted with the air distribution pipe facing the back of the plenum chamber, and the data indicate that the flow is lower than desired. The data were not accurate enough to derive a correction factor that would be used to generate the desired flow. Their measurements were inconsistent even for known conditions. The bulk of the probe bodies limited where they could be placed, and positioning them precisely was difficult with the equipment available in the lab. When they were placed, they exhibited random uncertainty that in some cases exceeded the expected range being measured, possibly due to other modes of heat transfer to nearby surfaces. As a result of these issues, combustion tests were performed despite the absence of channel flow data. 33 CHAPTER 6 – CONSTANT FLOW VELOCITY BURN TESTS The first set of burn tests was conducted with constant flow velocities in order to verify that the results were consistent with those from previous rigs. Data from all burn tests appear in Table 2. Four tests were conducted at 25 cm/s and two at 15 cm/s. The first two 25 cm/s tests were redone because the backlighting made it difficult to determine the proportion of sample area burned, though their results have still been included in the average flame speed calculation. The flame speed is determined as the slope of the linear regression curve for the flame track data, all of which have correlations (R2 values) greater than 0.997. In the 25 cm/s tests, the average flame spread rate is 0.216 cm/s, or 0.864% of the oxidizer flow velocity, and the flame front appears bright white, as shown in Figure 28, Figure 29, Figure 31, and Figure 32. In the latter two 25 cm/s tests, virtually the entire sample was consumed, as shown in Figure 30 and Figure 33. In the 15 cm/s tests, the average flame spread rate is 0.192 cm/s, or 1.28% of the oxidizer flow velocity. The flame appears dim and blue but is still a complete flame front, as shown in Figure 34, Figure 35, Figure 37, and Figure 38. During these tests only 80 to 90 percent of the sample was consumed, primarily because the sample ignited unevenly and required about one fourth of the sample length to stabilize, as shown in Figure 36 and Figure 39. In all of the constant velocity tests, the global mass air to fuel ratio was strongly fuel lean (between 21 and 27, which correspond to equivalence ratios of approximately 4 to 5.5), which is consistent with previous results. It should be noted that, while the flame front was not always uniform due to incomplete ignition and flow disruptions caused by the support shims, the flame spread rate was relatively 34 constant across the width of the channel; that is, even if the flame front was not uniform, it tended to propagate uniformly. Figure 28. Test 2012-04-18_2, 70s, Flame Front (25 cm/s) 35 Figure 29. Test 2012-04-18_2, 180s, Flame Front (25 cm/s) Figure 30. Test 2012-04-18_2, Burned Sample 36 Figure 31. Test 2012-04-18_3, 70s, Flame Front (25 cm/s) Figure 32. Test 2012-04-18_3, 170s, Flame Front (25 cm/s) 37 Figure 33. Test 2012-04-18_3, Burned Sample Figure 34. Test 2012-04-18_4, 75s, Flame Front (15 cm/s) 38 Figure 35. Test 2012-04-18_4, 200s, Flame Front (15 cm/s) Figure 36. Test 2012-04-18_4, Burned Sample 39 Figure 37. Test 2012-04-18_5, 70s, Flame Front (15 cm/s) Figure 38. Test 2012-04-18_5, 180s, Flame Front (15 cm/s) 40 Figure 39. Test 2012-04-18_5, Burned Sample 41 CHAPTER 7 – FAST RAMP DOWN BURN TESTS Ramp down tests were conducted in which the sample was ignited in a high, constant oxidizer flow velocity condition, and then, once the flame front stabilized, the flow velocity was decreased at a constant rate until reaching a low velocity steady state. The purpose of these tests was to examine the steady state flame behavior at high versus low flow velocities. The flame speed is determined as the slope of the regression curve for the flame track data (linear regression for steady state and second order for transient conditions). These quantities have correlations (R2 values) greater than 0.984. The first three tests were initiated at 25 cm/s and ramped down at the deceleration rate 5 cm/s2 for 3 seconds to a final velocity of 10 cm/s. The average initial flame spread rate was 0.214 cm/s, or 0.856% of the oxidizer flow velocity. Here, the flame front appears bright white, as shown in Figure 40, Figure 43, and Figure 46. The average final flame spread rate was 0.114 cm/s, or 1.14% of the oxidizer flow velocity. The flames appear dim blue and periodically flicker or dissociate into flamelets, indicating that they are at the lower limit of the flame front regime, as shown in Figure 41, Figure 44, and Figure 47. In these tests, two thirds to three fourths of the sample was consumed, as shown in Figure 42, Figure 45, and Figure 48. The next three tests were initiated at 25 cm/s and ramped down at 2 cm/s2 for 8 seconds to a final velocity of 9 cm/s. The average initial flame spread rate was 0.217 cm/s, or 0.868% of the oxidizer flow velocity, and the flame front appears bright white, as shown in Figure 49, Figure 52, and Figure 55. The average final flame spread rate was 0.0953 cm/s, or 1.06% of the oxidizer flow velocity, and as in the previous set of tests, the flames appear dim blue, as shown 42 in Figure 50, Figure 53, and Figure 56. In these tests, between two thirds and three fourths of the sample was consumed, as shown in Figure 51, Figure 54, and Figure 57. A final test was initiated at 25 cm/s and ramped down at 1 cm/s2 for 20 seconds to a final velocity of 5 cm/s, as an interim between the fast and slow ramp down tests. Its initial flame spread rate was 0.198 cm/s, or 0.990% of the oxidizer flow velocity. The flame front appears bright white, as shown in Figure 58. Its final flame spread rate was 0.0739 cm/s, or 1.48% of the oxidizer flow velocity, and the flames have dissociated into faint blue flamelets, as shown in Figure 59. The test was stopped when the first flamelet neared the end of the sample. About half of the sample was consumed, as shown in Figure 60. In this test, the ramping rate was slow enough that the transient behavior could be examined; the flame spread rate during the flow deceleration was found to be 0.720% of the oxidizer flow velocity. In all but the last of these tests, the ramping rate was fast enough that only the steadystate behavior could be examined; that is, the transient period was very short. As expected, the flame spread rate tended to be on the order of one hundredth of the oxidizer flow velocity (slightly lower for flame fronts and higher for flamelets), and the flame front showed signs of weakening and dissociation at flow velocities around 10 cm/s. In all of these ramping tests, the global mass air to fuel ratio was strongly fuel lean (between 28 and 43, which correspond to equivalence ratios of approximately 5.5 to 8.5), which is consistent with previous results. Note that the air to fuel ratios are much higher in the ramping tests than in the constant high velocity tests, indicating that the flamelets burn much more fuel lean than the flame front. Of interest in particular in these experiments was the behavior of the flame as it reaches the lower limit of the flame front regime and dissociates into flamelets. High speed footage was 43 recorded to capture this behavior, but due to the low lighting conditions and the small lens on the high-speed camera, little could be seen in these videos, though some screenshots are presented below. During the flow deceleration, the flame front initially decreases in intensity proportionally to the flow velocity and in the process changes hue from bright yellow to dim blue, as shown in the burn test figures below. Nearing the flamelet regime, the flame front begins flickering at a frequency that increases as the flow rate decreases. Finally, the flame again glows bright yellow immediately prior to bifurcating or autoextinguishing, as shown in Figure 61, Figure 62, Figure 63, and Figure 64. Note from the burned sample images that, at 9 and 10 cm/s flow velocities, small flamelets tended to propagate near the edges of the sample, whereas the flamelets in the center of the sample were larger, possibly due to locally lower air flow velocities around the edges. Figure 40. Test 2012-04-19_1, 70s, Flame Front (25 cm/s) 44 Figure 41. Test 2012-04-19_1, 190s, Weak Flame Front (10 cm/s) Figure 42. Test 2012-04-19_1, Burned Sample 45 Figure 43. Test 2012-04-19_3, 85s, Flame Front (25 cm/s) Figure 44. Test 2012-04-19_3, 265s, Weak Flame Front (10 cm/s) 46 Figure 45. Test 2012-04-19_3, Burned Sample 47 Figure 46. Test 2012-04-19_4, 80s, Flame Front (25 cm/s) Figure 47. Test 2012-04-19_4, 240s, Weak Flame Front (10 cm/s) 48 Figure 48. Test 2012-04-19_4, Burned Sample 49 Figure 49. Test 2012-04-20_1, 85s, Flame Front (25 cm/s) Figure 50. Test 2012-04-20_1, 225s, Weak Flame Front (9 cm/s) 50 Figure 51. Test 2012-04-20_1, Burned Sample Figure 52. Test 2012-04-20_3, 70s, Flame Front (25 cm/s) 51 Figure 53. Test 2012-04-20_3, 240s, Flamelets (9 cm/s) Figure 54. Test 2012-04-20_3, Burned Sample 52 Figure 55. Test 2012-04-20_4, 80s, Flame Front (25 cm/s) Figure 56. Test 2012-04-20_4, 230s, Flamelets (9 cm/s) 53 Figure 57. Test 2012-04-20_4, Burned Sample Figure 58. Test 2012-04-24_1, 80s, Flame Front (25 cm/s) 54 Figure 59. Test 2012-04-24_1, 210s, Flamelets (5 cm/s) Figure 60. Test 2012-04-24_1, Burned Sample 55 Figure 61. Test 2012-04-19_1 (High Speed Camera), 257s (286s in standard rate video), Flamelets Extinguishing (10 cm/s) Figure 62. Test 2012-04-20_1 (High Speed Camera), 230s (346s in standard rate video), Flamelets Bifurcating (9 cm/s) Figure 63. Test 2012-04-20_3 (High Speed Camera), 273s (300s in standard rate video), Flamelets Extinguishing (9 cm/s) 56 Figure 64. Test 2012-04-24_1 (High Speed Camera), 57s (98s in standard rate video), Flamelets Bifurcating (17 cm/s) 57 CHAPTER 8 – SLOW RAMP DOWN BURN TESTS Ramp down tests were conducted in which the sample was ignited in a high, constant oxidizer flow velocity condition, and then, once the flame front stabilized, the flow velocity was decreased at a slow constant rate until reaching zero flow. The purpose of these tests was to examine the transient flame behavior during slow ramping down flow. The flame speed is determined as the slope of the regression curve for the flame track data (linear regression for steady state and second order for transient conditions), all of which have correlations (R2 values) greater than 0.966. The first three tests were initiated at 25 cm/s and ramped down at 0.5 cm/s2 for 50 seconds. The average initial flame spread rate was 0.173 cm/s, or 0.692% of the oxidizer flow velocity, and the flame front appears bright white, as shown in Figure 65, Figure 68, and Figure 71. The average transient flame spread rate was 1.15% of the oxidizer flow velocity, and the flames appear dim blue and periodically flicker or dissociate into flamelets at around 10 cm/s flow, as shown in Figure 66, Figure 69, and Figure 72. In these tests, about half of the sample was consumed, as shown in Figure 67, Figure 70, and Figure 73. The next four tests were initiated at 25 cm/s and ramped down at 0.25 cm/s2 for 100 seconds. The average initial flame spread rate was 0.213 cm/s, or 0.850% of the oxidizer flow velocity, and the flame front appears bright white, as shown in Figure 74, Figure 77, Figure 80, and Figure 83. The average transient flame spread rate was 0.860% of the oxidizer flow velocity. The flames again appear dim blue and periodically flicker or dissociate into flamelets at around 10 cm/s flow, as shown in Figure 75, Figure 78, Figure 81, and Figure 84. In these 58 tests, about half of the sample was consumed, as shown in Figure 76, Figure 79, Figure 82, and Figure 85. The next two tests were initiated at 25 cm/s and ramped down at 0.1 cm/s2 for 250 seconds. Since flamelets in these tests reached the end of the sample before the flow velocity had reached zero, the next three tests were initiated at 20 cm/s and ramped down at 0.1 cm/s2 for 200 seconds. The average initial flame spread rate was 0.201 cm/s, or 0.806% of the oxidizer flow velocity, for the first two tests and 0.204 cm/s, or 1.02% of the oxidizer flow velocity, for the next three tests, and the flame front appears bright white, as shown in Figure 86, Figure 89, Figure 92, Figure 95, and Figure 98. The average transient flame spread rate was 1.04% of the oxidizer flow velocity, and the flames again appear dim blue and periodically flicker or dissociate into flamelets at around 10 cm/s flow, as shown in Figure 87, Figure 90, Figure 93, Figure 96, and Figure 99. In these tests, about half of the sample was consumed, as shown in Figure 88, Figure 91, Figure 94, Figure 97, and Figure 100. In all of these ramping tests, the global mass air to fuel ratio was strongly fuel lean (between 22 and 42, which correspond to equivalence ratios of approximately 4.5 to 8.5), which is consistent with previous results. The transient behavior of the flame in these tests was similar to that described in the previous chapter. During the flow deceleration, the flame front initially decreases in intensity proportionally to the flow velocity and in the process changes hue from bright yellow to dim blue, as shown in the burn test figures below. Nearing the flamelet regime, the flame front begins flickering at a frequency that increases as the flow decreases. And again, the flame glows bright yellow immediately prior to bifurcating or autoextinguishment, as shown in Figure 101, Figure 102, Figure 103, and Figure 104. Apart from the time scale, this behavior seems 59 relatively unaffected by the rate at which the flow is decelerated. Note from the burned sample images that the flamelets did not survive for very long, and very few of them bifurcated, which indicates that the range of flow velocities in which flamelets survive is very narrow. Figure 65. Test 2012-04-26_1, 100s, Flame Front (25 cm/s) 60 Figure 66. Test 2012-04-26_1, 140s, Flamelets (10 cm/s) Figure 67. Test 2012-04-26_1, Burned Sample 61 Figure 68. Test 2012-04-26_2, 90s, Flame Front (25 cm/s) Figure 69. Test 2012-04-26_2, 120s, Flamelets (10 cm/s) 62 Figure 70. Test 2012-04-26_2, Burned Sample Figure 71. Test 2012-04-26_3, 185s, Flame Front (25 cm/s) 63 Figure 72. Test 2012-04-26_3, 215s, Flamelets (10 cm/s) Figure 73. Test 2012-04-26_3, Burned Sample 64 Figure 74. Test 2012-04-26_4, 180s, Flame Front (25 cm/s) Figure 75. Test 2012-04-26_4, 240s, Flamelets (10 cm/s) 65 Figure 76. Test 2012-04-26_4, Burned Sample Figure 77. Test 2012-04-26_5, 100s, Flame Front (25 cm/s) 66 Figure 78. Test 2012-04-26_5, 160s, Flamelets (10 cm/s) Figure 79. Test 2012-04-26_5, Burned Sample 67 Figure 80. Test 2012-04-26_6, 10s, Flame Front (25 cm/s) Figure 81. Test 2012-04-26_6, 70s, Flamelets (10 cm/s) 68 Figure 82. Test 2012-04-26_6, Burned Sample Figure 83. Test 2012-04-26_7, 90s, Flame Front (25 cm/s) 69 Figure 84. Test 2012-04-26_7, 150s, Flamelets (10 cm/s) Figure 85. Test 2012-04-26_7, Burned Sample 70 Figure 86. Test 2012-04-27_1, 90s, Flame Front (25 cm/s) Figure 87. Test 2012-04-27_1, 240s, Flamelets (10 cm/s) 71 Figure 88. Test 2012-04-27_1, Burned Sample Figure 89. Test 2012-04-27_2, 90s, Flame Front (25 cm/s) 72 Figure 90. Test 2012-04-27_2, 240s, Flame Front (10 cm/s) Figure 91. Test 2012-04-27_2, Burned Sample 73 Figure 92. Test 2012-04-27_3, 80s, Flame Front (20 cm/s) 74 Figure 93. Test 2012-04-27_3, 180s, Flamelets (10 cm/s) Figure 94. Test 2012-04-27_3, Burned Sample 75 Figure 95. Test 2012-04-27_4, 80s, Flame Front (20 cm/s) Figure 96. Test 2012-04-27_4, 180s, Flamelets (10 cm/s) 76 Figure 97. Test 2012-04-27_4, Burned Sample Figure 98. Test 2012-04-27_5, 80s, Flame Front (20 cm/s) 77 Figure 99. Test 2012-04-27_5, 180s, Flamelets (10 cm/s) Figure 100. Test 2012-04-27_5, Burned Sample 78 Figure 101. Test 2012-04-26_1 (High Speed Camera), 90s (141s in standard rate video), Flamelet Extinguishing (9 cm/s) Figure 102. Test 2012-04-26_6 (High Speed Camera), 125s (83s in standard rate video), Flamelets Bifurcating (6.75 cm/s) Figure 103. Test 2012-04-27_2 (High Speed Camera), 117s (164s in standard rate video), Flamelets Bifurcating (17.6 cm/s) 79 Figure 104. Test 2012-04-27_4 (High Speed Camera), 234s (257s in standard rate video), Flamelets Extinguishing (2.3 cm/s) 80 CHAPTER 9 – LESSONS LEARNED FLOW SYSTEM The most significant issue with the flow system was air leaking out of the plenum chamber. The original design, shown in Figure 105, had a rubber gasket between the walls and top plate of the plenum chamber, but this gasket was never seated properly and allowed air to leak between it and the top plate. Additionally, the sudden contraction at the plenum chamber exit (in absence of the cardboard flow guide) likely created a significant constriction that worsened the leak. When a pressure test revealed the location of the leak, a layer of petroleum jelly (Vaseline) was used to seal the gap between the gasket and top plate, but this caused the rubber gasket to warp and ultimately exacerbated the problem. Finally the rubber gasket was discarded in favor of the bead of silicon adhesive sealant along the top of the perimeter walls of the plenum chamber; this was effective. Before the leakage issue was properly diagnosed, it was noted that the flow through the test section was stronger with the distribution pipe rotated 180 degrees (that is, facing the plenum exit instead of the back wall). Burn tests in this configuration produced flickering, unstable flame fronts, an indication of nonuniform and unsteady flow through the test section. The pipe was therefore returned to its original configuration when the flow issue was resolved. SAMPLE HOLDER The sample holder is currently not very rigid due to its thickness. The placement of the shims keeps it fairly level, but it sags in the middle of the channel since shims cannot be placed here due to the disruption they would cause to the flow. Shims were placed strategically to minimize sagging, but a new sample holder constructed of a different material would be ideal, as this issue has still not been fully resolved. 81 While the sample holder currently has paper clips attached to it for securing the sample in place, initially the sample was affixed using electrical tape. This method allowed for more tension across the sample, which could reduce the sagging due to gravity, but had the considerable disadvantage of not being adjustable after the sample was placed. Because of this issue, the sample was difficult to place uniformly, and so the paper clip method was found to be easier to set up. SAMPLE IGNITION The igniter wire was originally positioned forward of its current position such that it spanned the open region of the sample holder. Since the position of the tensioning clips was constrained by the chamber design, the wire was routed to its desired location by a pair of guides, as shown in Figure 106. This configuration was thought to be advantageous since it positioned the igniter within the viewing area of the window and in the path of the air flow (instead of adjacent to the sample holder), allowing for easier and more uniform ignition. However, it turned out that, without the backing of the sample holder, the igniter wire made very little contact with the sample. Furthermore, the igniter wire in this configuration would frequently slip out of place, and repositioning it required removing the top plate of the test section. Finally, the guides, which were made of rubber due to its insulating properties, were found to be scorched by the igniter wire after repeated tests. For these reasons, the igniter wire is now placed straight across the test section. 82 PRELIMINARY APPARATUS PHOTOS Figure 105. View of Plenum Chamber with Top Removed, Highlighting Old Seal Design Figure 106. View of Test Section with Top Plate Removed, Highlighting Old Igniter Design 83 CHAPTER 10 – CONCLUSIONS AND FUTURE WORK In constant velocity flows, the flame propagation rate was approximately 1% of the oxidizer flow velocity (slightly lower for the flame front and slightly higher for flamelets), which is consistent with previous experiments. The track is strongly linear, indicating that the flame speed is constant. In the ramping flows, the flame propagation rate was also approximately 1% of the oxidizer flow velocity but was variable, particularly in the faster ramp down tests. This behavior is possibly due to the lag time between the change in flow velocity and the response of the flame. The track is strongly second order, indicating that the flame speed decreases linearly with respect to the flow deceleration. Flamelets in the near-extinction regime tend to be a dim blue hue (which was often difficult to see in the video) and often flickered with increasing frequency as the oxidizer flow velocity decreased. However, immediately before bifurcating or extinguishing, the flamelet would glow bright yellow, possibly indicating that the flame is cooling. The flame front began dissociating into flamelets at oxidizer flow velocities of approximately 10 cm/s. The flamelets tended to extinguish at approximately 4 cm/s flow rate. Thus, the range of flow velocities that supports the propagation of flamelets is fairly narrow, as indicated by the short life span of the flamelets in the tests that ramped the flow down to zero. While the new Narrow Channel Apparatus is an improvement over its predecessor, the wider channel presents challenges that need to be addressed. The highest priority is a more effective sample holder and ignition system. Currently, the sample holder sags due to gravity in the center of the channel, and supporting it with shims is not an option as that would disrupt the flow. Thus, a new sample holder constructed of a more rigid material is needed. Furthermore, 84 the rubber shims that support the center of the sample disrupt the flame propagation and the uniformity of the sample, but leaving the sample unsupported in the center is not an option as the sample sags enough to touch the bottom glass, which severely disrupts the air flow and flame propagation. An ideal solution would be the use of thin, non-conductive and heat-resistant wire strung between the clips to uniformly and non-disruptively support the sample across its entire width. The next priority is improvements to the video recording technology. In particular, the high-speed camera is not very useful in its present state. At the very least, it needs a lens with a larger aperture for the flamelets to be visible in the video, as we are attempting to view very small points of light from a considerable distance. Ideally, the camera would also be higher resolution, as the flamelets currently appear pixelated due to their small size relative to the area being viewed. However, this would require a new camera, which would constitute a substantial expense. An alternative would be to install additional lighting in the camera mount, but too much light could overpower the light of the flamelets and render them invisible. Additional long-term upgrades include a second mass flow controller, equipment to measure the temperature at various points in the channel, and equipment to analyze the chemical content of the exhaust gases. With two mass flow controllers and bottled gases, the flow rate of oxygen and nitrogen can be controlled independently, allowing for testing the effects of varying oxygen concentrations. The IGOR program used to control the flow is already written to accommodate two MFCs. Accurate temperature measurements can verify the FLUENT models and the heat release formula derived by Aditjandra [12]. Accurate analysis of the exhaust gases can verify the oxygen consumption model derived by Aditjandra [12] and also provide real-time data regarding the combustion conditions. NASA-Lewis already has equipment to measure the 85 oxygen consumption rate. In the long-term future, a second high-speed camera and a PC with dual Ethernet ports and more processing power to run them would be ideal, as this setup would provide comparable video from both above and below the sample. Currently, the two videos are different speeds, different resolutions (with different aspect ratios), and offset from each other (due to the method of starting and stopping the video recording), which makes direct comparisons difficult. 86 APPENDICES 87 APPENDIX A – STOICHIOMETRY ANALYSIS The samples are Whatman-44 filter paper (cellulose) with chemical formula C6H10O5. Its combustion process in air is C6H10O5 + 6O2 + xN2  6CO2 + 5H2O + xN2 where coefficient x depends on the oxygen concentration. (In this case, x is the number of moles of nitrogen per six moles of oxygen.) Let n be the oxygen mole fraction. The nitrogen mole fraction is then 1 – n (assuming negligible concentrations of other gases in air). That makes the molar ratio of nitrogen to oxygen (1 – n)/n, which from the above formula is also equal to x/6. Therefore x = 6/n – 6 Then the general form of the combustion equation is C6H10O5 + 6O2 + (6/n – 6)N2  6CO2 + 5H2O + (6/n – 6)N2 For combustion in pure oxygen, n = 1, and so the formula simplifies to C6H10O5 + 6O2  6CO2 + 5H2O For the typical atmospheric molar oxygen concentration of 21% which was used in this experiment, n = 0.21, and so the formula simplifies to C6H10O5 + 6O2 + 22.57N2  6CO2 + 5H2O + 22.57N2 While the nitrogen is not part of the combustion process, its concentration is necessary to determine the oxygen flow rate based on the known total air flow rate. The air flow rate is reported as volumetric, and the volumetric concentration of oxygen in the air is equal to its molar concentration. 88 The stoichiometric mass ratio of air to fuel is then mair mF 6⋅ MW O2 +  6 − 6 MW n  N2   6⋅ 31.9988 MW F kg kmol +  6 − 6 28.0134 kg n  kmol   162.1402⋅ kg 0.1475 + 1.0366 n kmol For atmospheric air (n = 0.21), the stoichiometric mass air to fuel ratio is mair/mF = 5.08 The actual mass ratio of air to fuel can be approximated by the known air flow rate and elapsed time and the estimated mass of fuel burned. Let v be the average oxidizer flow velocity and h be the total gap height. The gap width is a constant 46 cm. The oxidizer flow rate is F = (46 cm)*v*h. The density of atmospheric air is approximately 1.225 kg/m3 (or 0.00125 g/cm3), and the gap height for all of the tests in this paper is 8 mm (0.8 cm), so the oxidizer mass flow rate for these tests is (0.04508 g/cm)*v. Then the total mass of air is ⌠ tf    v ( t) d mair 0.04508 t  cm  ⌡t  0  This integral simplifies to v*t for constant velocity flows or (vf + v0)/2*t for ramping g (constant acceleration) flows, where t is the elapsed time. The approximate mass of fuel burned is simply the estimated percentage of the sample area burned times the mass of the unburned sample, which is approximately 10.4 grams, as measured by the load cell in the lab’s cone calorimeter. (Each sample theoretically could have been weighed before and after the test to determine the mass burned, but as the sample tended to disintegrate into small pieces during the combustion process, determining the remaining mass post-burn would have been difficult.) 89 The approximate mass air to fuel ratio for atmospheric air and an 8 mm gap height is then mair mF tf 0.0043346 ⌠  Pb ⋅ cm ⌡t v ( t) d t 0 where Pb is the percentage of the sample area burned. The solved integral will have units of length, which cancels the length units in the denominator of the coefficient, resulting in a dimensionless quantity, as expected. 90 APPENDIX B – PRESSURE RELIEF CALCULATION Physical properties of quartz window - Length: x := 17in Plate thickness: T := M := 7000psi Modulus of rupture: Width: y := 10in Selected Factor of Safety - 4 in Unsupported surface area: A := x⋅ y F := 5 Properties of water - ρ := 1000 kg 3 P ρ⋅ g ⋅ h m P := ( M⋅ T x + y 2 2 x y F h := P ρ⋅ g P or h 2 2 Calculation using Dr. Miller's formula which corresponds to: 1 h = 32.601⋅ in 91 ρ⋅ g 2 ) P = 1.178⋅ psi A = 170⋅ in 2 APPENDIX C – TEST DATA Test Name 2012-04-09_1 2012-04-09_2 2012-04-17_1 2012-04-18_1 2012-04-18_2 2012-04-18_3 2012-04-18_4 2012-04-18_5 2012-04-19_1 2012-04-19_2 2012-04-19_3 2012-04-19_4 2012-04-20_1 2012-04-20_2 2012-04-20_3 2012-04-20_4 2012-04-24_1 2012-04-26_1 2012-04-26_2 2012-04-26_3 Initial v (cm/s) 25 25 25 25 25 25 15 15 25 25 25 25 25 25 25 25 25 25 25 25 Initial Initial Ramp Ramp Flame Flame Rate Time Final v Speed Speed / Transient Flame 2 Initial v Speed (cm/s) (cm/s ) (s) (cm/s) (cm/s) 0 N/A 25 0.2180 0.872% N/A 0 N/A 25 0.2369 0.948% N/A 0 N/A 25 N/A N/A N/A 0 N/A 25 N/A N/A N/A 0 N/A 25 0.2056 0.822% N/A 0 N/A 25 0.2053 0.821% N/A 0 N/A 15 0.1876 1.251% N/A 0 N/A 15 0.1963 1.309% N/A -5 3 10 0.2039 0.816% N/A -5 3 10 N/A N/A N/A -5 3 10 0.2231 0.892% N/A -5 3 10 0.2137 0.855% N/A -2 8 9 0.2205 0.882% N/A -2 8 9 N/A N/A N/A -2 8 9 0.2157 0.863% N/A -2 8 9 0.2161 0.864% N/A -1 20 5 0.1984 0.794% 0.0072*v + 0.0599 -0.5 50 0 0.1576 0.630% 0.0096*v + 0.0186 -0.5 50 0 0.1938 0.775% 0.0124*v - 0.0139 -0.5 50 0 0.1686 0.674% 0.0124*v - 0.0340 Table 2. Overview of Test Data (Red background indicates discarded tests.) 92 Final Flame Speed (cm/s) N/A N/A N/A N/A N/A N/A N/A N/A 0.1257 N/A 0.1066 0.1101 0.0995 N/A 0.0978 0.0887 0.0739 N/A N/A N/A Final Flame Speed / Final v N/A N/A N/A N/A N/A N/A N/A N/A 1.257% N/A 1.066% 1.101% 1.106% N/A 1.087% 0.986% 1.478% N/A N/A N/A 2012-04-26_4 2012-04-26_5 2012-04-26_6 2012-04-26_7 2012-04-27_1 2012-04-27_2 2012-04-27_3 2012-04-27_4 2012-04-27_5 25 25 25 25 25 25 20 20 20 -0.25 -0.25 -0.25 -0.25 -0.1 -0.1 -0.1 -0.1 -0.1 100 100 100 100 250 250 200 200 200 0 0 0 0 0 0 0 0 0 Table 2 (cont’d) 0.2053 0.821% 0.1908 0.763% 0.2320 0.928% 0.2223 0.889% 0.1885 0.754% 0.2148 0.859% 0.2082 1.041% 0.2049 1.025% 0.1996 0.998% 93 0.0072*v - 0.0005 0.0096*v + 0.0247 0.0064*v + 0.0424 0.0112*v + 0.0034 0.0080*v + 0.0324 0.0060*v + 0.0499 0.0120*v - 0.0192 0.0140*v - 0.0372 0.0120*v - 0.0072 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Test Name 2012-04-18_2 2012-04-18_3 2012-04-18_4 2012-04-18_5 2012-04-19_1 2012-04-19_3 2012-04-19_4 2012-04-20_1 2012-04-20_3 2012-04-20_4 2012-04-24_1 2012-04-26_1 2012-04-26_2 2012-04-26_3 2012-04-26_4 2012-04-26_5 2012-04-26_6 2012-04-26_7 2012-04-27_1 2012-04-27_2 2012-04-27_3 2012-04-27_4 2012-04-27_5 Initial v (cm/s) 25 25 15 15 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 20 20 20 Ramp Rate (cm/s2) 0 0 0 0 -5 -5 -5 -2 -2 -2 -1 -0.5 -0.5 -0.5 -0.25 -0.25 -0.25 -0.25 -0.1 -0.1 -0.1 -0.1 -0.1 Ramp Time (s) N/A N/A N/A N/A 3 3 3 8 8 8 20 50 50 50 100 100 100 100 250 250 200 200 200 Final v Number of Number of (cm/s) Bifurcations Extinctions 25 N/A N/A 25 N/A N/A 15 N/A N/A 15 N/A N/A 10 0 0 10 4 7 10 1 3 9 1 0 9 4 8 9 7 9 5 4 10 0 0 14 0 0 11 0 0 1 0 0 14 0 1 13 0 1 14 0 0 11 0 2 7 0 1 9 0 0 8 0 2 11 0 0 4 Table 3. Flame Behavior 94 Approx. Sample Area Burned (%)* 100% 100% 90% 90% 70% 60% 60% 70% 70% 70% 60% 40% 40% 50% 60% 40% 60% 60% 70% 80% 70% 70% 70% Approx. Mass Air/ Fuel Ratio 26.87 26.33 21.75 23.55 28.47 42.93 36.86 31.65 32.50 33.67 28.61 36.57 31.15 45.51 41.54 40.64 N/A 25.29 33.28 29.12 22.29 22.29 22.29 *In Table 3, the sample area burned was approximated visually. Tests 2012-04-09_1 and 2012-04-09_2 are not included because their burned sample area could not accurately be determined. Figure 107. Steady State Flame Spread Rate vs. Oxidizer Flow Velocity for All Tests 95 Figure 108. Steady State Flame Spread Rate Relative to Oxidizer Flow Velocity vs. Oxidizer Flow Velocity for All Tests 96 Figure 109. Test 2012-04-09_1 Track Figure 110. Test 2012-04-09_2 Track 97 Figure 111. Test 2012-04-18_2 Track Figure 112. Test 2012-04-18_3 Track 98 Figure 113. Test 2012-04-18_4 Track Figure 114. Test 2012-04-18_5 Track 99 Figure 115. Test 2012-04-19_1 Overall Track Figure 116. Test 2012-04-19_1 Initial Track 100 Figure 117. Test 2012-04-19_1 Final Track Figure 118. Test 2012-04-19_3 Overall Track 101 Figure 119. Test 2012-04-19_3 Initial Track Figure 120. Test 2012-04-19_3 Final Track 102 Figure 121. Test 2012-04-19_4 Overall Track Figure 122. Test 2012-04-19_4 Initial Track 103 Figure 123. Test 2012-04-19_4 Final Track Figure 124. Test 2012-04-20_1 Overall Track (Outliers have been deleted.) 104 Figure 125. Test 2012-04-20_1 Initial Track Figure 126. Test 2012-04-20_1 Final Track (Outliers have been deleted.) 105 Figure 127. Test 2012-04-20_3 Overall Track (Outliers have been deleted.) Figure 128. Test 2012-04-20_3 Initial Track 106 Figure 129. Test 2012-04-20_3 Final Track (Outliers have been deleted.) Figure 130. Test 2012-04-20_4 Overall Track 107 Figure 131. Test 2012-04-20_4 Initial Track Figure 132. Test 2012-04-20_4 Final Track 108 Figure 133. Test 2012-04-24_1 Overall Track (Outliers have been deleted.) Figure 134. Test 2012-04-24_1 Initial Track 109 Figure 135. Test 2012-04-24_1 Transient Track Figure 136. Test 2012-04-24_1 Final Track (Outliers have been deleted.) 110 Figure 137. Test 2012-04-26_1 Overall Track Figure 138. Test 2012-04-26_1 Initial Track 111 Figure 139. Test 2012-04-26_1 Transient Track Figure 140. Test 2012-04-26_2 Overall Track 112 Figure 141. Test 2012-04-26_2 Initial Track Figure 142. Test 2012-04-26_2 Transient Track 113 Figure 143. Test 2012-04-26_3 Overall Track Figure 144. Test 2012-04-26_3 Initial Track 114 Figure 145. Test 2012-04-26_3 Transient Track Figure 146. Test 2012-04-26_4 Overall Track 115 Figure 147. Test 2012-04-26_4 Initial Track Figure 148. Test 2012-04-26_4 Transient Track 116 Figure 149. Test 2012-04-26_5 Overall Track Figure 150. Test 2012-04-26_5 Initial Track 117 Figure 151. Test 2012-04-26_5 Transient Track Figure 152. Test 2012-04-26_6 Overall Track 118 Figure 153. Test 2012-04-26_6 Initial Track (Video recording was not initiated until after burn test had started.) Figure 154. Test 2012-04-26_6 Transient Track 119 Figure 155. Test 2012-04-26_7 Overall Track Figure 156. Test 2012-04-26_7 Initial Track 120 Figure 157. Test 2012-04-26_7 Transient Track Figure 158. Test 2012-04-27_1 Overall Track 121 Figure 159. Test 2012-04-27_1 Initial Track Figure 160. Test 2012-04-27_1 Transient Track 122 Figure 161. Test 2012-04-27_2 Overall Track Figure 162. Test 2012-04-27_2 Initial Track 123 Figure 163. Test 2012-04-27_2 Transient Track Figure 164. Test 2012-04-27_3 Overall Track 124 Figure 165. Test 2012-04-27_3 Initial Track Figure 166. Test 2012-04-27_3 Transient Track 125 Figure 167. Test 2012-04-27_4 Overall Track Figure 168. Test 2012-04-27_4 Initial Track 126 Figure 169. Test 2012-04-27_4 Transient Track Figure 170. Test 2012-04-27_5 Overall Track 127 Figure 171. Test 2012-04-27_5 Initial Track Figure 172. Test 2012-04-27_5 Transient Track 128 REFERENCES 129 REFERENCES 1. Oravecz, L.M. “Instabilities of Spreading Diffusion Flames in Microgravity and the Design and Construction of a Hele-Shaw Apparatus That Produces Flames in the Near Extinction Limit Regime Under Simulated Low Gravity Conditions.” M.S. thesis. Michigan State University, 2001. 2. Tanaya, Stefanus A. “Examination of a Simulated Micro-Gravity Device for Evaluating Flame Instability Transitions and Flame Spread Over Thin Cellulosic Fuels.” M.S. thesis. Michigan State University, 2004. 3. DeRis, J. N. “Spread of a Laminar Diffusion Flame.” Twelfth Symposium (International) on Combustion, The Combustion Institute, 1969, pp. 241-252. 4. Fernandez-Pello, A. C., and F. A. Williams. “Laminar Flame Spread over PMMA Surfaces.” Fifteenth Symposium (International) on Combustion, The Combustion Institute, 1975, pp. 217-231. 5. Fernandez-Pello, A. C., and F. A. Williams. “A Theory of Laminar Flame Spread over Flat Surfaces of Solid Combustibles.” Combustion and Flame, 1977, Vol. 28, pp. 251-277. 6. Wichman, I.S. and F.A. Williams. "A Simplified Model of Flame Spread in an Opposed Flow along a Flat Surface of a Semi-infinite Solid." Combustion Science and Technology, 1983, Vol. 32, pp. 91-123. 7. Wichman, I.S. and F.A. Williams. "Comments on Rates of Creeping Spread of Flames Over Thermally Thin Fuels." Combustion Science and Technology, 1983, Vol. 33, pp. 207-214. 8. Olson, S.L. "Near Limit Flame Spread over a Thin Solid Fuel in Microgravity." TwentySecond Symposium (International) on Combustion, The Combustion Institute, 1988, pp. 1213-1222. 9. Olson, S.L. "Mechanisms of Microgravity Flame Spread over a Thin Solid Fuel: Oxygen and Opposed Flow Effects." Combustion Science and Technology, 1991, Vol. 76, pp. 233-249. 10. Olson, S.L., and H.R. Baum, and Kashiwagi, T. "Finger-Like Smoldering over Thin Cellulosic Sheets in Microgravity." Twenty-Seventh Symposium (International) on Combustion, The Combustion Institute, 1998, pp. 2525-2533. 11. Zik, Ory, Zeev Olami, and Elisha Moses. "Fingering Instability in Combustion." Physical Review Letters, 2 November 1998, Vol. 81, #18, pp. 3868-3871. 130 12. Aditjandra, Karin Laksmi. “Population and Sample Burned Area Analyses for Near Limit Flames in a Simulated Low Gravity Environment Over Thin Cellulosic Fuels.” M.S. thesis. Michigan State University, 2005. 13. Olson, Miller, Wichman Olson, S. L., F. J. Miller, and I. S. Wichman. “A New Species of Fire: Characterizing Fingering Flamelets Using Biological Population Measures.” Combustion Theory and Modeling, 2006, Vol. 10, No. 2, pp. 323-347. 14. Pepper, Jacob M., and Fletcher J. Miller. “Characterizing the Narrow Channel Apparatus as a NASA Standard Material Flammability Test.” 2011 Fall Technical Meeting of the Western States Section of the Combustion Institute, The Combustion Institute, 2011. 15. Hung, Karen W., Sandra L. Olson, and Fletcher J. Miller. “Flame Spread Across Trioxane in a Narrow Channel Apparatus Simulating Microgravity Flow Conditions.” 2011 Fall Technical Meeting of the Western States Section of the Combustion Institute, The Combustion Institute, 2011. 131