‘S‘HE EMPEDANCE MET'Hfib AM} ETS APPLICATIQN TO THE HETERMINATEQN Q53 Tfifi ACOUgTé‘Z [IMPEDANCE OF L§QL3§D MEDM Tlmés: 5M thee SW :35 My 32 MECHEGhN STATE iiN‘i-‘VERSETY Robert Richard Sfieaum W503 ° ’ "'9- 68““... Am,o_h"o-_w -——.“"‘ -.-. Mum” ~' ' .+_-_, J MICH|GAN STATE LIBRARIES ' W\\\\\\\\\\\\\\\\\\\\\\\\\\\\\\i\\\\\\\\\\\\\\\\\\\\\\i 3 1293 01774 5617 LIBRARY Michigan State University M: PLACE IN RETURN Box to remolee this checkput from your record. TO AVOID FINES returh ori orbefore date due. MAY BE RECALLED with earlier due date if requested. DATE DUE DATE DUE DATE DUE ma W14 TIE LIPMD’T'C“ IIZTIIOD- “.TLD ITS ATP LICATION TO TIE DETERM NATION CF TIE I‘COUSTI C IKFEDAHCE CF LIQUID MEDIA By Rebert Richard Slocum AN ABSIH ACT A Ti? ~SIS Submitted to the College of Science 51nd Arts of Michigan State University of Agriculture and Applied Science in partial fulfillment of he requirements fer the degree of TER OF SCIEICE Department of Physics 1956 Approved 2‘ A W HE IHPZD‘TCT "”“WPD AID ITS ATTLICA-IOI TO THE DITERNINATIOT OF THE MACOIST IC IMPE AT 3 OF LIQUID T-‘ED IA 0 The theory of electroacoustics has provided methods whereby analysis of tra11sducer performance may be carried out by measurements of the res ctive and resistive components of the electrical imped- ance offered to t‘1e terminals of the trfnsducer. From plots of t11e impedance components vs. free ucn- cy, quantities proportional to t”; 1e acoustic imped- ance of the wedium into which the transducer is operating can be derived. After empirically deter- mining the apprOpriate constants of the transducer, the acoustic impedance of the medium may be derived. ’5 Examples 0: t 1 as kind of in:_ormation ti 1at may be obtained about the transducer performance char- acteristics are given, and the results of meanu“e— f’) ments on liquids are presenter. The underlrirc .. \2 .134- .a'. theory is outlined, an a discussion 0- the general Lu utility of the impedance method is inclurei. Robert Richard Slocum THE IMPFDANCE METHOD AND ITS APPLICATION TO THE DFTTRMINATION OF THE ACOUSTIC IMPEDANCE OF LIO UID MFDIA BY Robert Richard Slocum A THESIS Submitted to the College of Science and Arts of Michigan State Universitv of Agriculture and Applied Science in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE Department of thsics 1956 AC 32101-552334: _- :2- I wish to mun: Dr. E. A. Modems; ‘1, wh suggested the development of this method, for his guidance and many sugfjostions duri ngf, tho develOp- mont of the equipm .71t, but more especially for his Lmdorstendirr; and encozuesgomont o R.SM II. III. IV. VI. VII. TABLE OF COKTEIT Page INTRODUCTION...... ..... ............ 1 THEORY...... ..... .................. 3 OBJECT OF EXPERIHLNT............... l4 EXPERIMENTAL SET-UP & APPARATUS.... l5 DATA............................... 21 CON LUSIONS AND SUG?TSTIONS........ 26 BIBLIO'GRi‘.PI—1Yooooooooo0000000000000. 28 I. INTRODUCTION The impedance method is a familiar one in the field of acoustics. The term 'motional impedance' was first introduced by A. E. Kennellv and G. W. Pierce in 1912, when they were studying the variation of impedance with freouency for a telephone receiver and discovered that the electric impedance could be influenced by the motion of the coupled mechanical svsteml. The impedance concept was introduced into mechanics and acoustics as a result of the similarity in form of the mathematical equations for acoustical and mechanical vibrations with those of oscillating electric circuits. Its introduction proved invaluable to the analvsis of transducer performance and facilitated improvements in transducers by leading to the develOpment of a compre- hensive theory of electroacoustics. The impedance concept carried over very directly into ultrasonics, where it continued to be of vital importance in transducer design and theory. Radiation resistance, motional impedance, and impedance matching are important considerations for anyone working with ultrasonic transducers. Pecause the motional impedance of a transducer is affected by the medium in which it is Operating as well as the manner in which the crystal is mounted, and since a change in the motional impedance in turn causes a variation in the electrical impedance offered to the generator at the input terminals of the transducer, observations of the electrical impedance lead to a knowledge of some of the important preperties of the media being irradiated. This studv utilizes the imped- ance method for the measurement of the characteristic impedance of various liquids. The theory will be outlined in Section II, and its Specific application to this problem and the apparatus, and some of the problems involved, including its limit- ations, will be considered subsequently. II. THEORY As has been pointed out, the study of equivalent circuits and the analogy between electrical and mech- anical oscillatory phenomena has led to the deveIOpment of the theory of electro-acoustics. By means of this theory it is possible to represent electro-mechanical transducers by a single form of equivalent circuit. Although such a representation by a single equivalent network allows maximum generality for application of theory to different cases, it has become common practice to use different types of circuits for different trans- ducers, on the assumption that some networks are physi- cally more meaningful than others. Here the discussion of transducers will follow the more general method, in which the transducer is considered as a four-terminal network. Following the theory given by Hunt2 , we consider a transducer as a four-terminal network, with two terminals representing the electrical input coupled through a "black box" element, which represents the general con- , version of electrical to mechanical energy, to a mech- anical circuit of a single degree of freedom (figure 1). 0n the electrical side, a current I flows through an electrical impedance 26, with a voltage E across the input terminals; on the mechanical side, there is a velocity v, a mechanical impedance Z , and a force F m across the output terminals. Two equations are needed to describe the behavior of this system: one in terms of the electrical quantities, including the reactions caused by the motion of the mech- anical system; the other in terms of the mechanical var- iables, as well as any mechanical reactions due to the currents and voltages in the electrical network. The symbols T.m and Tm, represent "transduction coefficients", denoting electromechanical coupling. Assuming a steady state, with time appearing in the form eiwt, the equations are E - 28.1 '. Tem'V (1) F - Tme'I + Zm°v Some important prOperties of the electromechanical interaction can be displayed by observing the driving- point impedance appearing at either pair of terminals. The electric driving-point impedance at a terminal pair is defined as the complex ratio of voltage across the terminals to the current in the terminal pair, when all other electromotive forces and current sources are suppressed. Putting F-O in Eqs.(l) and solving for I in terms of E, we get E’ (T' T’ ) The mechanical driving-point impedance is similarly found to be Equations (2) and (3) show the usual electrical and mechanical impedance with an additive term contain- ing the transduction coefficients. These extra terms represent a modification of the impedance caused by the presence of a bilateral electromechanical coupling. The additive term in Eq. (2) indicates the modification of the electrical impedance by the motion in the mechanical system; this term, (- TmeTgm) - Zmot, has been given the name of "motional impedange". Then Eq.(2) may be rewritten to include this defi- nition in the form Zee' Z. + zmoto where Z. is the "clamped" or "blocked” impedance, measured when the mechanical system has in some manner been prevented from vibrating. Since the motional impedance, Zmoto is directly proportional to the negative product of the transduction coefficients, its nature will depend on the size of these coefficients and whether they are real or complex. However, the general behavior of the motional impedance, especially its variation with fre- quency, may be studied by considering the behavior of the mechanical admittance ym, since Zmot'('Temee)/Ymo where ym - l/Zm. If the mechanical impedance Zm is written in the generalized form Zm - rm + j‘UIm * __l__ ' rm * 31m: jwcm where the quantities rm, 1m, and cm refer to the mechan- ical resistance, mass, and compliance, respectively, ~‘and xm denotes the mechanical reactance, we see that the variation of this impedance with frequency may be exhibited by expressing Zm as a vector from the origin in the complex xm-rm plane. In general both the length and phase of this vector will vary as the frequency changes, and the tip of the vector will trace out a curve which is Called an ”impedance locus". If rm is not a function of frequency the impedance locus will be a vertical straight line at a distance rmfrom the origin. The phase angle is zero at the angular frequency of mechanical resonance,CUO2 - l/lmcm. If a similar plot is made of the mechanical admit- tance, 7m! the admittance locus is a circle, which is just the geometrical inversion of the straight-line impedance locus. This admittance circle has a diameter of length l/rm. Since Z3, is real at mechanical reso- nance,ym is also real when.a)02 - l/lmcm (figure 2). If we call the frequencies for phase angles of7T/2 and -7T/2 radians al'and cu" (the quadrantal frequencies) I l -_ I [-0) 2 respectively, we may write rm --w 'm+w' cm' w 'm [(0.20 ] d - +-afW - —J——‘= T E F I ‘9—Tem— I C>* e~43 C>* C) <——i v——> Figure 1. General four-terminal network, valid for all transducer types. 9m D='/fm = 9m Ym = 9m +ibm= I/Zm Figure 2. Motional admittance circle for r independent of frequency (vertical straight-line impedance locus). 12 +Xee _k% Figure 3. Typical electrical impedance 100p (generally non-circular)for frequencies very near resonance. Figure 4. Universally accepted equiva- lent circuit for piezoelectric transducer. 13 III. O'3JTZCT .7 T’IT'J'I 7'13??? 9 Because of the rather general utility of the impedance method it was considered desirable to build up sufficient apparatus so that the technique would be available whenovor it might be noedod for studios in the ultra sonics lal)oro.tory, in conjunc- tion with both Optical and pulse methods. As an example of the knowlod3o that may be gained by this mothod, the do cision was made to undertake an investigation of several liquids to determine their acoustic impodonoos, from'which he sound velocities may be derived, if desirod. This wo also done with an eye toward dotcrminin: whether thoro mi3ht be a sufficio1t time-variation in the acoustic in~tdcwoo of 033 albumin to make Toss iblo tlzo development of a method for chockin3 the freshness of 0333 by ultrasonic radiation. In order to ill: 1stroto tao usof.ulnoos of his method a wioty of italics 10‘.lS are disployod. Toward this 0nd two impedance looms (a riot of reactnnos vs. resist nnco witl1 fr oquoncy as a nnra~ motor) have boon inc ludod. An impedance loop is useful bo ouso it ran ors immediately visible many important pfirform once charcctnriotlc of transducers. 14 Another interestin3 practical problem is the effect of the method of mountin3 on the transducer performance characteristics, for which the imped- ance method can give valuable infioreaticn. Dre to time limitations only one crystal was considered from this particular point of View. IV. EXPERIMENTAL SET-UP AND APPARATUS For all investigations in the vicinity of one megacycla 3 Brush Hypersonic Generator model BU-Zlh was used as a source of alternating current. This oscillator has an output frequency range from 300 to 1,200 kilocyclcs. This frequency rang. is covered in five stages, involving altcring the coil in the fre- quency-control tank-circuit. Within the five ranges the frequency is continuously variable by means of an auxiliary coil located insidc the main coil of the control tank circuit, causing small variations of inductance of the L-C tank circuit. The measuring instrument per so was a General Radio domesny R-P Bridge, Type 1606-A, in conjunction with a Hallicrafters General Communications Radio Receiver, Mbdsl 31-62 A, which functioned as a null detector for determination of bridge balance conditions. The type 1606-A Radio Frequency Bridge is a null instru- ment for use in measuring impedance at frequencies from #00 kc to 60 Me. The bridge is used with a series substitution method for meésuring an unknown impedance, Zx’ in terms of its series resistance compon- ent, Rx’ and series reactance comnonent, Xx. The Iresistance is read from a variable-condenser dial directly _ca1ihrated in reactance in ohms at a frequency of 1 Mo. 16 The resistance dial reading is independent of frequency, and reads from O to 1000 ohms; the reactance dial from O to 5000 ohms at 1 Me. The important characteristics required of the meas- uring apparatus are the following: (1) The oscillator must be as stable as possible in frequency, the output frequency and voltage being rela- tively independent of the load. It would be desirable to have one oscillator to cover the entire frequency range of interest to the experimenter, but it may be more convenient to use several oscillators of different frequency ranges, as was done in this case. The gener- ator must also be adequately shielded so as to avoid stray coupling between it and the detector. (2) The bridge must be a radio frequency type, capa- ble of a high degree of accuracy over the entire frequency range of interest, and well shielded against stray pick-up from either the generator or detector. It is strongly advisable that co-axial connectors be used for connections to both the source and the receiver. Obviously the reactance-resistance ranges must be commensurate with the corresponding impedance components being measured. (3) The detector must be of high sensitivity in order to enable very rrecise location of the balance point, since this is the quantity of major concern in this method. It must be well shielded, for the same 17 reasons mentioned in connection with the signal gener- ator and the 3-? bridge. It must possess a local oscil- lator capable of putting out a strong, clear signal, and should have an automatic volume-control switch. Frequently measurements were made with a U.S. Army Signal Corps Frequency ther 80-221 J, with a range from 125 to 20,000 kc. The prime requisite of the frequency measuring device in this application is accuracy. The meter used here was accurate to 1000 cycles per second. (see figure 1 for diagram of apparatus) The procedure for making measurements was the fol- lowing! The signal generator was set somewhere in the vicinity of the resonant frequency of the crystal, which was Operating into air, This frequency was measured on the frequency meter, and then recorded. Then the bridge was balanced with the crystal short- circuited. After connecting the crystal into the unknown arm of the bridge, a balance was again ob- tained using the reactance and resistance dials. The reactance and resistance were then recorded. This procedure was then repeated in its entirety for several different frequencies, until it was certain that the resonant peak in a plot of re- sistance vs. frequency had been located. Next the crystal was immersed in one of the liquids under consideration and the procedure outlined above was repeated, step by step. An example of these plots is shown for a general case (figure 2.) Lkasurements were made for several different crys- tals in each of the liquids investigated. Also some measurements at higher frequencies were made, using another oscillator that was available. In general reactance measurements were not made, since only the resistance and the resonant frequency were required for obtaining the acoustic imredance of the liquids. However, in order to obtain impedance loops, reactance data were measured in a few cases. As a rough indication of the effect of the crystal mounting, measurements were made on an unmounted barium titanite disc, and then again after the same crystal had been glued onto a phenolic resin composition board back- ing on one side. 19 Y FREQUENCY METER ’5 DETECTOR OSCILLATOR T T e e ’c BRIDGE 9 Q ‘c Figure l. RESISTANCE Block diagram of experimental apparatus. A O AIR FREQUENCY Figure 2. Typical curves of resistance vs. frequency in air, and with liquid load. 20 V. 0’ re > Figure (l) is a plot of moasurrd electrical resistance vs. frequency for a freely vibrating barium titanate orys ml with a resonant frequrncy of 1.0911 mogaoyolos por second. The broken curve is the one which applies to the unmounted crystal. The solid curve is the same plot for the crystal when mounted with air-backing in a brass crystal- holdor of the type commonly used for ultrasonic investigations of liquids. Figure (2) is a plot of the measured electrical resistance vs. the moasurod electrical reactance for the unmounted one mafiacycle barium titanato crystal, exhibiting the typical impedance loop form. Figure (3) is a plot of ‘ho motional resistance vs. the motional reactance. The plotted values are the difference betwoon the measured olcrtric l impwdu once components and the blocked impedance commononta, tho lattor boi 3 obtained by extrapolation, as discussed in roction II. Tho diameters of tho motional imp d 200 circles- are inversely froportionsl to ,ho losers of the P.) H cryst"l. fineo the lo its? mes ion was air for both cases, the decrees, in diameters inflicrtes cls“rly the losses coused by the mountinfl. Since ’ho quality factor, Q, is relotefl to the hol’-wifl it}; of the lac onant peaks, it is obvious tfint tko mounting e nsia rsbly lowers tho 2. By measuring tWo imoedo sore o? tho cr:,st .1 rqfiouqt:d, then “coin whcn in tho crystal holficr, sni tfien when Operatinfi into a liqull of known inpoicnce, it would be possiblc to fietrrni.o tho losses of tho holler. "‘"nre (4) is a graph of the ”ensure? electri- cwl scri cs ros istcnec st t? c rnti-resonont frequrncy $8. the known values-of tho acoustic inpcionco of two four liqzids in which e"érruueqcs Wrrc ordc. The eryo‘ol word for to so deto was s two—inch sdusre barium titocoto of nominol P“O”“Ufij of ono W{~~ cycle oer scoonfl. 4‘ 2511.511" to T'ir'nre (4-) 30:” L J- -- ~ ,, '7 4- wi‘uro (p) is a plot a ’- n n‘ ‘- V . Q ‘5 ‘ 1" " mJuSUPCJcnhB perforncd witd a one merocyclo nrr s conl emirtz crystal. .mmfipcsoe eoxomnucao 90% cmam use .Omao opmsmuap Esanmn oopcsoess poo zozcsoonm .m> mm %0 poam .H oksmfim 33x02. >ozuacmm h. 9; «9. no; so; mo; no; we; 1\\\\\\\l111 o ) on \“uth 3 OS. \Il‘! . ; flee. 8 S m on. on» muck ‘00» 91 ocao oozrcngH Hosefipoa Lsmfim mo mmoofi oSp Eong oo>apow .m mhzuam mozdhmhmmm m7. \\ I 0 is... r 2.1% Q\\..;, v w _ . x, thy m - ~ 4 v. i, \ o N I o MNLW\\ 3 \\ -. III/my l.|.|\ N- on. .Lae ma opwmrphu poo oomhpooop Hoodspooao .m oozwpmfimop HmoHspoon .m opzmam ESHLGQ > ooXl \. vnmmflrll. cnmL: Jr! ammo; 1// mwmQ. #024 0 cc . pric 1L0 nose. some; so; vaQ.o / 0.0 .— \ \\\ oo. ammo; _\\\\\uw\ a mo;. oox+ 9!. ISO ENZENE Q: B 50 \ OCCIA OI. \ANILINE ‘2 .0 ' POCOX IO”5 Figure 4. Comparison of measured values of the acoustic ' impedance of four liquids with their known values, taken with barium titanste crystal. "'5 Jean ENE -_ ‘ \} IO.5 \ a PiEANUT on?" m. I55 4\\\\i \ on.- x 200 L 1.275 L325 L575 ma 5 M75 1.523 pg 00 x 10" Figure 5. Same as Figure 4, using quartz 25 I45 '- r “'“',"f YYf'TP-Tv": " 5"", «'577r""-",'“"'T‘TP\"C" 1 . ‘ 1") .,x.‘.."'~'-/ 3' a n"I-“\.J‘-- I.’). ..‘-".’l’-.‘ H}! inc date shown in Section V, nnfl the experience coined in assembling eni using the nonsrctus, clearly point out several important conclusions. Firstly, the percentage errors in the measurement of the acoustic impedance of liquids ct s froeuency of onc megccycle with t' e nrcsoxt opporetuc are so hifin cs ten percent, rcnierinr; it impossible to determine the tim"-v"rilt on of eM‘ e.lbumin to better th.?n ten ncrcent. This cie”rly ca ms insufficiently s our to. tecer“y t operfornhnce of the no suronontc with tfie nresefit equipment is vrry leIr rni trou“lescre. It sIocsrs, however, that it will be possible in o compnro tivcly short t me, to inern“re the accuracy to within one or two percent. Chfly, in n p.coer for the Office of Ecvcl Tesecrchg, reinte'out thet similar m7 hoi, but oneroting at the much rrerter ”rcoucncy 0:? fifteen meter cycles n r second, is conn- hle of accuracies as hifh rs one fiercent. Prueticclly no chances are no sery for extension of the ccuip— cent reed for this study to the fifteen mcgccyclo rocion. For st lice in hip Ily vis~eus liouils w ich 1.1 6.0 "101-: s. M rtwd GLIJPPCHCG bstwrcn t*c 1.. 4- \ resistivc :nd rcactivs componcnts of the acoustic impcdfincc it will be necessary to csnstr~ ancncy Hf surin: drvicc ult: cnt qwcncy from air to liquid, is cxtrcmcly cyciMs pvr scconfi). 27 tann is proportioncl to the small (on the act a mcrc scnsitivc frc~ is now av liable in the ascnics laboratory, becsusc tic rcactivc ccmficn- chance in rcscnsnt fre- frcqucncy cWrnMc of a few hunsrcd 1. 3. 4. 5. 6. 7. 9. 10. 11. Hunt, F.V., "Electro cous tics," Rsrvsrd univer- sity Press, Csmoridgc, 1300., 1954. Cody, 'I.G.I" woclcctricity," McGrc w-Iill, Now York,l +6.11 Rsson, J.P "Pic: ocloc ric Cr"stcls and incir Application to Ultrasonics," D. Van Nostrc nd Co., Inc., New York, 1950. Vi"ouroux, P., "Cu rts V bro tors and Their Appli- cations, His Mojcsty' s Stationery Office, London, 1% line tor, T.F., and Richmrd! I. Bolt, "Sonics," JoEIn Iilcy 6: Sons, Inc., New York, 1955. Roson, J. P., "Tlcctrorccrcriccl Transducers and Rave Filters," D. Van Lo: trc nd 00., Inc., Row ,YOZQI. ' ., 1 3'2“- 0 mason, J.P., "Shear 310sticity osd Viscosity of liquids," Boll) mclophonc System Tech. Pulyli- cs.tions, Monogrcpll 3-145 7. CSdF. ~.G.. "II c.surcmcnts of Trcnsduccr Incut cod Output!" ORR, Contrc ct U6 014401, TcsI.: Order 1, 1:3 C11; #01, TGC1‘1. £0th 7:! 3’ 19149: Cody, W.G., "HcDSI Iromcrt of tlie Specific WPcousiic Resist an of Liquids," OIT, ControctI 36 ORR-262, Tos120rdcr 1, II’R 015401 Tech. cht. ! 4,1949. Cody, II.C., "A Capacitance Bridge for 315,11 Fro- quoncics," R.S.I., 21 (1950),1002—1009. Roth,J., "Tic: oclcctric Transducers, " chh. cht. Lo. 43, Resos.rch Lrsorctory of Eloctronics, Lc.ss. Inst. of Technology 1947. “ry,' M3 ., "low Loss Crystcl Systoflis, J.A.R.A., .23.. (1 9+9). 29. 28 .171. ”'55 ' HICHIGQN STQTE UNIV. LIBRQRIES 31293017745617